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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
NASA NTRS1993

Damage tolerance and arrest characteristics of pressurized graphite/epoxy tape cylinders

An investigation of the damage tolerance and damage arrest characteristics of internally-pressurized graphite/epoxy tape cylinders with axial notches was conducted. An existing failure prediction methodology, developed and verified for quasi-isotropic graphite/epoxy fabric cylinders, was investigated for applicability to general tape layups. In addition, the effect of external circumferential stiffening bands on the direction of fracture path propagation and possible damage arrest was examined. Quasi-isotropic (90/0/plus or minus 45)s and structurally anisotropic (plus or minus 45/0)s and (plus or minus 45/90)s coupons and cylinders were constructed from AS4/3501-6 graphite/epoxy tape. Notched and unnotched coupons were tested in tension and the data correlated using the equation of Mar and Lin. Cylinders with through-thickness axial slits were pressurized to failure achieving a far-field two-to-one biaxial stress state. Experimental failure pressures of the (90/0/plus or minus 45)s cylinders agreed with predicted values for all cases but the specimen with the smallest slit. However, the failure pressures of the structurally anisotropic cylinders, (plus or minus 45/0)s and (plus or minus 45/90)s, were above the values predicted utilizing the predictive methodology in all cases. Possible factors neglected by the predictive methodology include structural coupling in the laminates and axial loading of the cylindrical specimens. Furthermore, applicability of the predictive methodology depends on the similarity of initial fracture modes in the coupon specimens and the cylinder specimens of the same laminate type. The existence of splitting which may be exacerbated by the axial loading in the cylinders, shows that this condition is not always met. The circumferential stiffeners were generally able to redirect fracture propagation from longitudinal to circumferential. A quantitative assessment for stiffener effectiveness in containing the fracture, based on cylinder radius, slit size, and bending stiffnesses of the laminates, is proposed.

Ranniger, Claudia U.↗
NASA NTRS1974

Fabrication of a graphite/epoxy antenna for the Viking Orbiter spacecraft

A graphite/epoxy composite high-gain antenna has been developed for the Viking Orbiter 1975 spacecraft. A thin-skin honeycomb sandwich construction was used for the reflector structure. The antenna has been designed, and several have been fabricated and successfully tested and qualified under simulated launch and space environments. The graphite/epoxy material was used primarily because of the weight saving over a more conventional aluminum honeycomb construction and because of its low expansion characteristics. The low coefficient of thermal expansion of the graphite composite results in a dimensionally stable antenna structure under the extreme thermal environment to be encountered in this Mars mission.

Stonier, R. A.↗
NASA NTRS1971

The fabrication, testing and delivery of boron/epoxy and graphite/epoxy nondestructive test standards

A description is given of the boron/epoxy and graphite/epoxy nondestructive test standards which were fabricated, tested and delivered to the National Aeronautics and Space Administration. Detailed design drawings of the standards are included to show the general structures and the types and location of simulated defects built into the panels. The panels were laminates with plies laid up in the 0 deg, + or - 45 deg, and 90 deg orientations and containing either titanium substrates or interlayered titanium perforated shims. Panel thickness was incrementally stepped from 2.36 mm (0.093 in.) to 12.7 mm (0.500 in.) for the graphite/epoxy standards, and from 2.36 mm (0.093 in.) to 6.35 mm (0.25 in.) for the boron/epoxy standards except for the panels with interlayered shims which were 2.9 mm (0.113 in.) maximum thickness. The panel internal conditions included defect free regions, resin variations, density/porosity variations, cure variations, delaminations/disbonds at substrate bondlines and between layers, inclusions, and interlayered shims. Ultrasonic pulse echo C-scan and low-kilovoltage X-ray techniques were used to evaluate and verify the internal conditions of the panels.

Pless, W. M.↗
NASA NTRS1975

Design, fabrication, and test of a graphite/epoxy metering truss

A graphite/epoxy metering truss as applied to the large space telescope was investigated. A full-scale truss was designed, fabricated and tested. Tests included static limit loadings, a modal survey and thermal-vacuum distortion evaluation. The most critical requirement was the demonstration of the dimensional stability provided by the graphite/epoxy truss concept. Crucial to the attainment of this objective was the ability to make very sophisticated thermal growth measurements which was provided by a seven beam laser interferometer. The design of the basic truss elements were tuned to provide the high degree of dimensional stability and stiffness required by the truss. The struts and spider assembly were fabricated with Fiberite's AS/934 and HMS/934 broadgoods. The rings utilized T300 graphite fabricate with the same materials. The predicted performance of the truss was developed using the NASTRAN program. These results showed conformance with the critical stiffness and thermal distortion requirements and correlated well with the test results.

Oken, S.↗
NASA NTRS1977

The effect of moisture on the dynamic thermomechanical properties of a graphite/epoxy composite

A study has been made of the effect of moisture absorption on the dynamic thermomechanical properties of a graphite/epoxy composite recently considered for building primary aircraft structures. Torsional braid analysis (TBA) and thermomechanical analysis (TMA) techniques were used to measure changes in the glass transition temperature (Tg) and the initial softening temperature (heat distortion temperature, HDT) of T-300/5209 graphite/epoxy composites exposed to room temperature water soak.

Sykes, G. F.↗
NASA NTRS1979

Electron and proton absorption calculations for a graphite/epoxy composite model

The Bethe-Bloch stopping power relations for inelastic collisions were used to determine the absorption of electron and proton energy in cured neat epoxy resin and the absorption of electron energy in a graphite/epoxy composite. Absorption of electron energy due to bremsstrahlung was determined. Electron energies from 0.2 to 4.0 MeV and proton energies from 0.3 to 1.75 MeV were used. Monoenergetic electron energy absorption profiles for models of pure graphite, cured neat epoxy resin, and graphite/epoxy composites are reported. A relation is determined for depth of uniform energy absorption in a composite as a function of fiber volume fraction and initial electron energy. Monoenergetic proton energy absorption profiles are reported for the neat resin model. A relation for total proton penetration in the epoxy resin as a function of initial proton energy is determined. Electron energy absorption in the composite due to bremsstrahlung is reported. Electron and proton energy absorption profiles in cured neat epoxy resin are reported for environments approximating geosynchronous earth orbit.

Long, E. R., Jr.↗
NASA NTRS1980

Effects of method of loading and specimen configuration on compressive strength of graphite/epoxy composite materials

Three test schemes were examined for testing graphite/epoxy (Narmco T300/5208) composite material specimens to failure in compression, including an adaptation of the IITRI "wedge grip" compression fixture, a face-supported-compression fixture, and an end-loaded-coupon fixture. The effects of specimen size, specimen support arrangement and method of load transfer on compressive behavior of graphite/epoxy were investigated. Compressive stress strain, strength, and modulus data obtained with the three fixtures are presented with evaluations showing the effects of all test parameters, including fiber orientation. The IITRI fixture has the potential to provide good stress/strain data to failure for unidirectional and quasi-isotropic laminates. The face supported fixture was found to be the most desirable for testing + or - 45 s laminates.

Clark, R. K.↗
NASA NTRS1980

Thermal expansion and swelling of cured epoxy resin used in graphite/epoxy composite materials

The paper presents results of experiments in which the thermal expansion and swelling behavior of an epoxy resin system and two graphite/epoxy composite systems exposed to water were measured. It was found that the cured epoxy resin swells by an amount slightly less than the volume of the absorbed water and that the swelling efficiency of the water varies with the moisture content of the polymer. Additionally, the thermal expansion of cured epoxy resin that is saturated with water is observed to be more than twice that of dry resin. Results also indicate that cured resin that is saturated with 7.1% water at 95 C will rapidly increase in moisture content to 8.5% when placed in 1 C water. The mechanism for this phenomenon, termed reverse thermal effect, is described in terms of a slightly modified free-volume theory in conjunction with the theory of polar molecule interaction. Nearly identical behavior was observed in two graphite/epoxy composite systems, thus establishing that this behavior may be common to all cured epoxy resins.

Adamson, M. J.↗
NASA NTRS1981

Strain rate, temperature, and humidity on strength and moduli of a graphite/epoxy composite

Results of an experimental study of the influence of strain rate, temperature and humidity on the mechanical behavior of a graphite/epoxy fiber composite are presented. Three principal strengths (longitudinal, transverse and shear) and four basic moduli (E1, E2, G12 and U12) of a unidirectional graphite/epoxy composite were followed as a function of strain rate, temperature and humidity. Each test was performed at a constant tensile strain rate in an environmental chamber providing simultaneous temperature and humidity control. Prior to testing, specimens were given a moisture preconditioning treatment at 60 C. Values for the matrix dominated moduli and strength were significantly influenced by both environmental and rate parameters, whereas the fiber dominated moduli were not. However, the longitudinal strength was significantly influenced by temperature and moisture content. A qualitative explanation for these observations is presented.

Lifshitz, J. M.↗
NASA NTRS1980

Fabrication of a graphite/epoxy composite leading edge for laminar flow control

Lockheed, under NASA contract, has recently completed the first phase of a program to evaluate laminar flow control concepts for transport aircraft. Achievement of laminar flow over a wing surface requires a system of slots, metering holes, ducts and pumps to be used to remove the turbulent air adjacent to the surface. This requirement poses severe restrictions on conventional metallic structure. Graphite/epoxy composite with its unique properties appears to be the material that might solve the very complex structural problems associated with a laminar flow control aircraft. A six-foot span graphite/epoxy test article incorporating provisions for leading edge cleaning, deicing and laminar flow control was designed, fabricated and tested.

Beall, R. T.↗
NASA NTRS1982

Requirements and design of the graphite/epoxy structural elements for the optical telescope assembly of the space telescope

The production of the Space Telescope's Metering Truss Structure (MTS) and Focal Plane Structure (FPS), which are of graphite/epoxy, is described. Graphite/epoxy laminates were chosen because of their high strength and stiffness, low weight, and a controlled coefficient of thermal expansion approaching zero. Photocopy masters, which are dimensionally accurate and stable photographic reproductions of full size engineering drawings, allowed the exact assembly of bonded or bolted parts by assembly mechanics, cutting costs and speeding production. While moisture absorption, high through-the-thickness coefficient of thermal expansion effects, and labor-intensive layup costs are potentially problematic in some cases, it is expected that solutions can be found through analytical and developmental programs.

Golden, C. T.↗
NASA NTRS1982

A model of the thermal-spike mechanism in graphite/epoxy laminates

The influence of a thermal spike on a moisture-saturated graphite/epoxy composite was studied in detail. A single thermal spike from 25 C to 132 C was found to produce damage as evidenced by a significant increase in the level of moisture saturation in the composite. Approximately half of this increase remained after a vacuum anneal at 150 C for 7 days, suggesting the presence of an irreversible damage component. Subsequent thermal spikes created less and less additional moisture absorption, with the cumulative effect being a maximum or limiting moisture capacity of the composite. These observations are explained in terms of a model previously developed to explain the reverse thermal effect of moisture absorption in epoxy and epoxy matrix composites. This model, based on the inverse temperature dependence of free volume, contributes an improved understanding of thermal-spike effects in graphite/epoxy composites.

Adamson, M. J.↗
NASA NTRS1984

Fracture surface characteristics of notched angleplied graphite/epoxy composites

Composite fracture surface characteristics and related fracture modes have been investigated through extensive microscopic inspections of the fracture surfaces of notched angleplied graphite/epoxy laminates. The investigation involved 4 ply laminates of the configuration + or - theta (s) where theta = 0 deg, 3 deg, 5 deg, 10 deg, 15 deg, 30 deg, 45 deg, 60 deg, 75 deg, and 90 deg. Two-inch wide tensile specimens with 0.25 in. by 0.05 in. through-slits centered across the width were tested to fracture. The fractured surfaces were then removed and examined using a scanning electron microscope. Evaluation of the photomicrographs combined with analytical results obtained using the CODSTRAN computer code culminated in a unified set of fracture criteria for determining the mode of fracture in notched angleplied graphite/epoxy laminates.

Ginty, C. A.↗
NASA NTRS1985

Profiles of fatigue damage in graphite/epoxy composites from ultrasonic transmission power spectra

Early fatigue damage in non-unidirectional multi-ply graphite/epoxy composites is manifested by a distribution of cracks and disbonds through the bulk of the material. Such damage is subtle and is difficult to detect with conventional ultrasonic technology. Consequently, a new ultrasonic measurement technique called phase-insensitive tone-burst spectroscopy has been developed. The new technique eliminates problems associated with phase cancellation and pulse shape artifacts inherent to conventional broadband ultrasonic spectral measurement systems and produces clean spectral information irrespective of specimen inhomogeneity or irregularities in surface geometry. Application of the new technique to measurements of graphite/epoxy composites has yielded frequency-domain profiles that show distinct differences in ultrasonic attenuation, attenuation slope, and velocity for each specimen experiencing a different level of fatigue damage.

Cantrell, J. H., Jr.↗
NASA NTRS1986

Strength of graphite/epoxy bolted wing-skin splice specimens subjected to outdoor exposure under constant load and yearly fatigue loading

The results of an experimental study to provide long-term durability data on detailed full-scale graphite/epoxy wing-skin joint designs under environmental exposure and cyclic loading associated with commercial transport aircraft are reported. The specimens consisted of a single-row bolt configuration fabricated from T300/5208 and a double-row bolt configuration fabricated from T300/5209. The unpainted specimens were exposed to the outdoor environment under a sustained tensile load, and at yearly intervals, they were subjected to fatigue loading. Experimental results showed a slight reduction in residual tensile strength for both graphite/epoxy joints under the exposure times and fatigue loadings reported. A 7.5-percent decrease in residual strength was observed for the T300/5208 single-row joint after 5 years exposure and two lifetimes of fatigue loading. A 5.3-percent decrease in residual strength was observed for the T300/5209 double-row joint after 7 years exposure and 2.8 lifetimes of fatigue loading. The 5208 epoxy material was more susceptible to degradation by ultraviolet radiation than the 5209 epoxy material.

Wichorek, G. R.↗
NASA NTRS1985

Fracture of thick graphite/epoxy laminates with part-through surface flaws

Fracture behavior of tensile specimens containing through-the-thickness flaws and part-through semi-elliptic surface flaws was investigated. The material was T300/5208 graphite/epoxy, with a stacking sequence 0/+ or - 45/90 sub ns. Laminate thicknesses ranged from 8 to 120 plies. Fracture toughness for specimens with through-the-thickness flaws was a function of laminate thickness. Fracture toughness was also independent of crack size. Fracture toughness for the thick laminates was also independent of specimen geometry (center-cracked tension specimen, compact tension specimen, and three-point bend specimen). Using the asymptotic value of facture toughness and linear elastic isotropic fracture mechanics, the notched strength of tensile specimens with semi-elliptic surface flaws was predicted. The strength ratio is a function of the flaw depth (a/t) and flaw aspect (a/c) ratios. Comparisons between predicted and experimental strengths are good for large values of a/t. The notched strength of filament wound graphite/epoxy tensile specimens with part-through surface flaws was also predicted.

Morris, D. H.↗
NASA NTRS1985

Effects of strain rate on delamination fracture toughness of graphite/epoxy

The objective of this paper is to evaluate various experimental techniques and analysis methods for the characterization of interlaminar fracture toughness, and to determine the effects of strain rate on that property for a graphite/epoxy composite. Mode I interlaminar fracture was investigated by means of a double-cantilever beam (DCB) specimen for AS-4/3501-6 graphite/epoxy. Hinged tabs were used to insure unrestrained rotation at the free ends. Specimens were loaded at quasi-static deflection rates of up to 8.5 mm/s corresponding to crack extension rates of over 51 mm/s. Crack extension was monitored by means of strain gages mounted on the surface of the specimen, or a conductive-paint circuit attached to the edge of the DCB specimen. Continuous records were obtained of load, deflection, and crack extension for determination of the strain energy release rate. The latter was expressed as a power law of the crack extension velocity. Results indicate that the strain energy release rate increases with crack velocity by up to 28 percent for the range of rates considered.

Daniel, I. M.↗
NASA NTRS1986

Fracture of thick graphite/epoxy laminates with part-through surface flaws

Fracture behavior of tensile specimens containing through-the-thickness flaws and part-through semi-elliptic surface flaws was investigated. The material was T300/5208 graphite/epoxy, with a stacking sequence 0/+ or - 45/90 sub ns. Laminate thicknesses ranged from 8 to 120 plies. Fracture toughness for specimens with through-the-thickness flaws was a function of laminate thickness. Fracture toughness was also independent of crack size. Fracture toughness for the thick laminates was also independent of specimen geometry (center-cracked tension specimen, compact tension specimen, and three-point bend specimen). Using the asymptotic value of fracture toughness and linear elastic isotropic fracture mechanics, the notched strength of tensile specimens with semi-elliptic surface flaws was predicted. The strength ratio is a function of the flaw depth (a/t) and flaw aspect (a/c) ratios. Comparisons between predicted and experimental strengths are good for large values of a/t. The notched strength of filament wound graphite/epoxy tensile specimens with part-through surface flaws was also predicted.

Harris, C. E.↗