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DOE OSTI2026

Comprehensive structural characterization of charged polymers involved in moisture-driven direct air capture

This study provides a comprehensive structural characterization of commercially available alkaline anion-exchange polymers (Fumasep FAA-3 and IRA 900) used in moisture-driven direct air capture (DAC) of carbon dioxide. Using X-ray diffraction, SAXS/WAXS, atomic force microscopy, FIB-SEM, and transmission electron microscopy, the authors identify nanoscale clustering, porosity, swelling behavior, and humidity-dependent structural changes that influence CO₂ adsorption and release. These findings establish structure–function relationships critical for designing more durable and energy-efficient DAC polymer materials.

36 MATERIALS SCIENCE↗

DOE OSTI2024

Downstream Separation of Formic Acid with Anion-Exchange Resin from Electrocatalytic Carbon Dioxide (CO 2 ) Conversion: Adsorption, Kinetics, and Equilibrium Modeling

The electrocatalytic carbon dioxide reduction reaction (CO 2 RR) that produces liquid formic acid (FA) is one potential route to minimize the CO 2 concentration in the atmosphere by utilizing CO 2 as a feedstock. However, one of the main disadvantages of this route is the high energy demand required for purification through conventional distillation. This method of purification has been shown to result in a large carbon footprint in life-cycle analysis (LCA). Therefore, finding an alternative purification technique that can integrate with an electrochemical CO 2 RR process with the potential to lower the carbon footprint would be of great interest. Under the experimental conditions of the CO 2 RR, FA remains in its basic form as the formate anion in the catholyte. Anion exchange resins with their basic properties can separate the formate anion from the catholyte mixture as an alternative to energy intensive distillation. In this work, three anion exchange resins with increasing basicity order: Amberlite IRA-96 < Amberlite IRA-910 < Ambersep 900 are tested to separate FA in the presence of aqueous solution of potassium bicarbonate catholyte with varying levels of resin and FA. Kinetics and equilibrium studies data for the FA adsorption are interpreted using several kinetics and isotherm models. The kinetics data fit well with a pseudo-first-order model at high initial FA concentrations and a pseudo-second-order model at low initial FA concentrations. The experimental data can be best explained with the Freundlich isotherm model. The fitted results show that strongly basic Ambersep 900 is more effective at separating FA, with a maximum adsorption capacity of 336.7 mg/g compared to Amberlite IRA-96 (275.2 mg/g) and Amberlite IRA-910 (209.2 mg/g) in neutral water. However, weakly basic Amberlite IRA-96 (110.8 mg/g) can separate FA more efficiently from potassium bicarbonate catholyte than Amberlite IRA-910 (99.9 mg/g) and Ambersep 900 (40.0 mg/g). As a result, competitive adsorption occurs in the presence of potassium bicarbonate catholyte, but the formic acid adsorption capacity is still sufficient for adequate separation.

20 FOSSIL-FUELED POWER PLANTS↗

NASA NTRS1984

The effect of radiation on the IRAS all-sky survey

The Infrared Astronomical Satellite (IRAS) is in a sun synchronous, 'near' polar orbit at an altitude of 900 km. The primary objective of IRAS is related to the conduction of an all-sky survey in the wavelength range from 8 microns to 120 microns. The present investigation is concerned with three components of the radiation environment encountered by IRAS, taking into account the high energy protons in the South Atlantic Anomaly, high energy electrons in the horns of the Van Allen belts, and cosmic rays. The effect of radiation on the returned data stream is studied, and attention is given to the steps which were taken to minimize the impact of radiation on the completeness of the survey.

Wolff, D. M.↗

NASA NTRS1989

Effects of ionizing radiation on cryogenic infrared detectors

The Diffuse Infrared Background Experiment (DIRBE) is one of three experiments to be carried aboard the Cosmic Background Explorer (COBE) satellite scheduled to be launched by NASA on a Delta rocket in 1989. The DIRBE is a cryogenic absolute photometer operating in a liquid helium dewar at 1.5 K. Photometric stability is a principal requirement for achieving the scientific objectives of this experiment. The Infrared Astronomy Satellite (IRAS), launched in 1983, which used detectors similar to those in DIRBE, revealed substantial changes in detector responsivity following exposure to ionizing radiation encountered on passage through the South Atlantic Anomaly (SAA). Since the COBE will use the same 900 Km sun-synchronous orbit as IRAS, ionizing radiation-induced performance changes in the detectors were a major concern. Here, ionizing radiation tests carried out on all the DIRBE photodetectors are reported. Responsivity changes following exposure to gamma rays, protons, and alpha particle are discussed. The detector performance was monitored following a simulated entire mission life dose. In addition, the response of the detectors to individual particle interactions was measured. The InSb photovoltaic detectors and the Blocked Impurity Band (BIB) detectors revealed no significant change in responsivity following radiation exposure. The Ge:Ga detectors show large effects which were greatly reduced by proper thermal annealing.

Moseley, S. H.↗

NASA NTRS1978

Infrared astronomical satellite

Design and mission characteristics of the Infrared Astronomical Satellite (IRAS) are reviewed with attention to the satellite/telescope configuration. The IRAS will be launched into a 900 km near-polar orbit (inclination 99 deg), with a cryogenically cooled 60 cm telescope capable of collecting 700 million bits of data per day. The telescope is expected to add from 6000 to one million new IR sources to the astronomical catalogs. Objects for study include stars, extended sources, asteroids, zodiacal light, artificial satellites, high energy protons, and dust.

Mclaughlin, W. I.↗

NASA NTRS1987

Diffuse infrared emission of the galaxy: Large scale properties

A quantitative analysis of Infrared Astronomy Satellite (IRAS) data in the galactic plane shows that: about 66% of the power radiated in the 100 micron band comes from the diffuse medium, the other 33% coming from well identified luminous sources. The diffuse emission has almost constant colors throughout the Galaxy, similar to the local cirrus colors. The sources have a much lower 12 micron/25 micron and a much high 60 micron/100 micron emission ratio than the diffuse component, giving a very striking anticorrelation in the color-color diagrams. The separation between one narrow and a second broader component shows that the molecular component does not provide much more than one half of the diffuse emission in the molecular ring: this implies a 4 pi nuI(nu) emissivity at 100 microns for the atomic component of about 2.4 x 10 to the minus 30th watts per H atom, 10 times higher than the emissivity of the molecular component at the same galactocentric radius. The atomic component emissivity measures the interstellar radiation field density. The temperature distribution of the 2 components is discussed comparing IRAS data with measures of the 900 micron emission of the galactic plane, which appears to be dominated by cold dust in the narrow component.

Puget, J. L.↗

NASA NTRS1984

IRAS cryogenic system flight performance report

It is pointed out that the Infrared Astronomical Satellite (IRAS) is the first telescope to perform observations in the far infrared from orbit. IRAS was launched on January 25, 1983 into a 900 km orbit. The use of the first large superfluid helium dewar in space makes it possible to provide a 2 K telescope environment for an anticipated period of one year. A description of the cryogenic system of IRAS is presented, taking into account the superfluid helium tank, the insulation system, the vacuum shell, the aperture cover, and the fluid management system. The dynamic performance of the cryogenic system is considered along with aspects of prelaunch preparations. Details of flight performance are also discussed, giving attention to transient performance, and steady state performance.

Urbach, A. R.↗

NASA NTRS1984

The IRAS minisurvey

Before the main Infrared Astronomical Satellite (IRAS) all-sky survey was started, a preliminary survey of 900 sq deg was carried out. Some results from this 'minisurvey' are given here. The completeness of the minisurvey at galactic latitudes from 20 to 40 deg drops sharply at flux densities below 0.4, 0.4, 0.5, and 2.5 Jy at 12, 25, 60, and 100 microns, respectively. The corresponding surface densities of point sources brighter than these flux levels are 1.1, 0.4, 0.65, and 1.25/sq deg, respectively. Outside the galactic plane, the majority of the sources at 12 and 25 microns are stars, while galaxies make up a significant proportion of 60 micron sources. The 100 micron band is dominated by emission from interstellar dust over much of the minisurvey area.

Rowan-Robinson, M.↗

NASA NTRS1985

Design of the superfluid helium dewar for the Cosmic Background Explorer (COBE)

Design features of the 664-liter superfluid helium dewar to be used for the Cosmic Background Explorer (COBE) are described, with emphasis on the similarities and differences vis a vis the Infrared Astronomical Satellite (IRAS) dewar. The dewar (23 percent larger than the IRAS dewar) is intended to provide a 14-month operating lifetime (vs. 10 months for IRAS). A far infrared absolute spectrophotometer (FIRAS) and diffuse infrared background experiment (DIRBE) will conduct full sky surveys over the wavelength region from 1 micron to 1 centimeter. Launch into a 900-km sun-synchronous polar orbit is scheduled for the autumn of 1987.

Hopkins, R. A.↗

NASA NTRS1991

Molecular gas in luminous infrared galaxies

Radio observations of 60 bright IRAS galaxies with redshifts of 1500-25,000 km/sec are reported. Data obtained in the 1-0 line of CO using the 12-m NRAO radio telescope during 1985-1988 are presented in extensive tables, graphs, and line profiles and analyzed along with similar data on 29 less distant IRAS bright galaxies (Tinney et al., 1990). The galaxies are found to have H2 masses of (1-60) x 10 to the 9th solar mass and a mean ratio of H2 to warm dust of 540 + or - 290, corresponding to a total gas/dust ratio of 900-1100. The discrepancy between this value and that for the Galaxy (about 150) is tentatively attributed to the presence of undetected cold dust or errors in interpreting the IR data. The mechanisms which might be responsible for the high ratios of IR luminosity to H2 mass (2-220 solar luminosity per solar mass) are discussed.

Sanders, D. B.↗

NASA NTRS1984

The Infrared Astronomical Satellite (IRAS) mission

The Infrared Astronomical Satellite (IRAS) consists of a spacecraft and a liquid helium cryostat that contains a cooled IR telescope. The telescope's focal plane assembly is cooled to less than 3 K, and contains 62 IR detectors in the survey array which are arranged so that every source crossing the field of view can be seen by at least two detectors in each of four wavelength bands. The satellite was launched into a 900 km-altitude near-polar orbit, and its cryogenic helium supply was exhausted on November 22, 1983. By mission's end, 72 percent of the sky had been observed with three or more hours-confirming scans, and 95 percent with two or more hours-confirming scans. About 2000 stars detected at 12 and 25 microns early in the mission, and identified in the SAO (1966) catalog, have a positional uncertainty ellipse whose axes are 45 x 9 arcsec for an hours-confirmed source.

Neugebauer, G.↗

NASA NTRS1976

A telescope for the Infrared Astronomical Satellite /IRAS/

The Infrared Astronomical Satellite (IRAS) will be used to survey the 8 to 120 micron spectrum of the entire sky to the faintest flux levels possible by using state-of-the-art detectors and preamplifiers. As a result of a recently completed study of the telescope and focal plane, a concept has been devised that demonstrates the feasibility of using stored cryogen to cool the telescope for one year of operation in a polar twilight orbit at an altitude of 900 km. Predictions regarding noise equivalent flux density, cryogenic lifetime, and the number of noise spikes caused by Van Allen belt radiation are presented. The telescope is cooled both by supercritical and by superfluid helium. The on-board signal processing includes provisions for suppressing noise spikes.

Hedden, R. L.↗

NASA NTRS1991

Early results from the Cosmic Background Explorer (COBE)

Data obtained with the FIR Absolute Spectrophotometer, Differential Microwave Radiometers, and Diffuse IR Background Experiment (DIRBE) on the COBE satellite since its launch in November 1989 are briefly characterized. The COBE spacecraft and its 900-km 99-deg orbit are described; the scientific goals and capabilities of the instruments are reviewed; and sample DIRBE data are presented in a map and graph. Upper limits on the Comptonization parameter (y less than 0.001) and the chemical potential (mu less than 0.01 at the 3sigma level) are determined, and the spectrum of the dipole anisotropy is shown to be that of a Doppler-shifted blackbody. The DIRBE 100-micron sky brightness values at the ecliptic poles are found to be significantly lower than those measured by IRAS.

Mather, J. C.↗