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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2026

Scintillation of liquid nitrogen

Liquid nitrogen is commonly used in cryogenic applications and is a promising medium for the direct immersion cooling of sensors used for nuclear and particle physics experiments. The scintillation properties of gaseous nitrogen are well-documented, but little is known about the scintillation of liquid nitrogen. If present, scintillation light from interactions of ambient radioactivity could produce backgrounds for rare event searches such as the direct detection of dark matter. Using a coincidence-tagged alpha decay, we demonstrate that liquid nitrogen exhibits measurable, albeit very faint, scintillation. Assuming the same scintillation wavelengths as gaseous nitrogen, we estimate a relative scintillation yield of $Y_{\liquidn}/Y^{\STP}_{\gasn} =$ \num[uncertainty-descriptors={stat,sys}]{0.0142(0.0005)(0.0030)} with respect to gaseous nitrogen at standard temperature and pressure. Considering the average scintillation yield from alpha decays in gaseous nitrogen, this implies a scintillation yield for alpha decays in liquid nitrogen of $Y_{\liquidn} = \qty[]{2.39(0.56)}{photons~per~MeV}$. To our knowledge this is the first measurement of scintillation in liquid nitrogen.

Pagani, Luca (ORCID:0000000234692581)↗
DOE OSTI2020

A high efficiency and low vibration liquid nitrogen cooling system for silicon crystal based x-ray optics

A compact low-cost cryocooling system has been designed, constructed, and tested at SLAC National Accelerator Laboratory. The cooling power is provided by natural convection and phase change of the liquid nitrogen. The initial application was to cool silicon crystal optics to the sub-100 K range. A silicon crystal of dimension (width × depth × height) 50 × 50 × 30 mm3 has been used with an electric heater on the top surface in this prototyping test. This system can effectively provide more than 80 W of cooling power to the optics with a consumption of liquid nitrogen less than 2.1 l/h. The vibration of the silicon crystal was monitored during the tests with added electric heater power on the crystal. We note the vibration of the silicon crystal due to liquid nitrogen boiling is negligible.

47 OTHER INSTRUMENTATION↗
DOE OSTI2024

Characterization of Silicon Photomultiplier Photon Detection Efficiency at Liquid Nitrogen Temperature

The detection of individual photons at cryogenic temperatures is of interest to many experiments searching for physics beyond the Standard Model. Silicon photomultipliers (SiPMs) are often deployed in liquid argon or liquid xenon to detect scintillation light either directly or after it has been wavelength-shifted. Maximizing the photon detection efficiency (PDE) of the SiPMs used in these experiments optimizes the sensitivity to new physics; however, the PDEs of commercial SiPMs, although well known at room temperature, are not well characterized at the cryogenic temperatures at which many experiments operate them. Here we present results from an experimental setup that measures the photon detection efficiencies of silicon photomultipliers at liquid nitrogen temperature, 77 K. Results from a KETEK PM3325-WB-D0 and a Hamamatsu S13360-3050CS silicon photomultiplier — of R&D interest to the LEGEND experiment — exhibit a decrease in photon detection efficiency greater than 20% at liquid nitrogen temperature relative to room temperature for 562 nm light.

Cryogenic detectors↗
DOE OSTI2020

A cantilevered liquid-nitrogen-cooled silicon mirror for the Advanced Light Source Upgrade

This paper presents a novel cantilevered liquid-nitrogen-cooled silicon mirror design for the first optic in a new soft X-ray beamline that is being developed as part of the Advanced Light Source Upgrade (ALS-U) (Lawrence Berkeley National Laboratory, USA). The beamline is optimized for photon energies between 400 and 1400 eV with full polarization control. Calculations indicate that, without correction, this design will achieve a Strehl ratio greater than 0.85 for the entire energy and polarization ranges of the beamline. With a correction achieved by moving the focus 7.5 mm upstream, the minimum Strehl ratio is 0.99. This design is currently the baseline plan for all new ALS-U insertion device beamlines.

47 OTHER INSTRUMENTATION↗
DOE OSTI2023

Experimental testing of a prototype cantilevered liquid-nitrogen-cooled silicon mirror

This report presents testing of a prototype cantilevered liquid-nitrogen-cooled silicon mirror. This mirror was designed to be the first mirror for the new soft X-ray beamlines to be built as part of the Advanced Light Source Upgrade. Test activities focused on fracture, heat transfer, modal response and distortion, and indicated that the mirror functions as intended.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
DOE OSTI2023

Studies of event burst phenomenon with SiPMs in liquid nitrogen

Silicon photomultiplier (SiPM) are used to collect scintillation photons in many cryogenic noble liquid detectors deployed around the world, such as DarkSide, nEXO, MEGII, ProtoDUNE and DUNE. An event burst phenomenon was observed during routine characterization on many models of SiPMs operated in liquid nitrogen. These bursts of consecutive pulses are initiated by an intense dark photoelectron pulse with an event rate much lower than the time-uncorrelated thermal dark pulse. Although the rate of these burst events is very low, it can potentially compromise some dedicated rare physics event searches which are also anticipated to be of extremely low rate. Here, we systematically studied the behavior of the event burst phenomenon and identified the probable cause of the phenomenon. Here, this investigation is important for the selection of SiPMs for use in noble liquid detectors, high energy physics experiments, and industrial applications where SiPMs are used in cryogenic environment.

47 OTHER INSTRUMENTATION↗
DOE OSTI2026

Long-term stability-degradation analysis of DUNE SiPMs in Liquid Nitrogen

We developed a cryogenic photon readout system to monitor arrays of DUNE SiPMs operating at various over-voltages in liquid nitrogen (LN2) for over three months. Photoelectron signals were read out simultaneously via weak capacitive coupling to the micro-FEMB, a 32-channel charge sensitive readout board designed for 77 K to 300 K operation in liquid argon time projection chambers (LAr-TPCs). A waveform snippet acquisition scheme was implemented to capture waveform signals whenever they exceeded a predetermined trigger level; consequently, empty waveforms were discarded. Selected SiPM parameters were monitored to detect any deviations beyond statistical fluctuations. While some parameters exhibited ~1σ variations over the 3-month test period, there was no evidence of drift being enhanced when operating at 4 V or 5 V compared to a 3 V over-voltage. However, a discernible PDE drop was observed across all channels, which warrants further investigation. In addition, we demonstrated that our system can simultaneously read out single photons from a selected group of SiPMs at room temperature.

Tsang, Thomas [Brookhaven]↗
DOE OSTI2023

First Experience with Liquid Nitrogen Cleaning

Field emission caused by microscopic particulate contamination is a limiting factor for the performance of superconducting RF (SRF) cavities. In an SRF based accelerator, particulates may be transported over the surface of an operational SRF cavity, becoming field emitters and consequentially degrading the performance of the SRF cavity. The most commonly used method for removing particulates from cavity surfaces is high-pressure ultra-pure water rinsing. We are developing a novel high-pressure liquid nitrogen cleaning technique that may possibly enable superior cleaning power and particulate removal from cavities in a cryomodule without taking apart the cryomodule components. This technique provides cleaning mechanisms beyond what are accessible by its high-pressure water rinsing counterpart and leaves no residues on the cleaned surface.

Ruber, R.J.M.Y.↗
DOE OSTI2024

LBNF/DUNE Nitrogen Refrigeration System Update

The Deep Underground Neutrino Experiment (DUNE) is supported by the infrastructure of the Long Baseline Neutrino Facility (LBNF). The central feature of DUNE is the liquid argon filled cryostats, which house the neutrino detector components. In order to maintain the argon in a liquid state, heat must be continuously removed. Argon condensers will remove this heat, and liquefy the argon, through the evaporation of liquid nitrogen. The supply of liquid nitrogen relies heavily on a near-industrial scale nitrogen refrigeration/liquefaction system. The nitrogen system will be a closed loop, in which the liquid nitrogen is supplied to users and, after being vaporized, is recycled to the nitrogen liquefaction units to be liquefied again. The system will also include nitrogen generation, to increase inventory in the closed loop, as well as to make up for losses. All of this will be installed nearly one mile underground (1.5km) on the 4850 level of the Sanford Underground Research Facility (SURF). The final DUNE vision requires 400kW of liquid nitrogen cooling capacity. Based on the operation modes and phased installation of the experiment, modularity of this cooling capacity is required. Nitrogen liquefaction will occur in four units which will afford a wide operational range of production (nominally 100kW each). Due to the experiment’s location deep underground in an inactive gold mine, there are unique and challenging constraints. These include limited access, footprint, and utilities. This poster describes the engineering effort, and provides an overview of the refrigeration system. The design includes a unique compressor arrangement which is covered in detail. Pictures and models are included where possible to help visualize the system.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2020

Characterization of high-purity germanium detectors with amorphous germanium contacts in cryogenic liquids

For the first time, planar high-purity germanium detectors with thin amorphous germanium contacts were successfully operated directly in liquid nitrogen and liquid argon in a cryostat at the Max-Planck-Institut für Physics in Munich. The detectors were fabricated at the Lawrence Berkeley National Laboratory and the University of South Dakota, using crystals grown at the University of South Dakota. They survived long-distance transportation and multiple thermal cycles in both cryogenic liquids and showed reasonable leakage currents and spectroscopic performance. Also discussed are the pros and cons of using thin amorphous semiconductor materials as an alternative contact technology in large-scale germanium experiments searching for physics beyond the Standard Model.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2020

Cryocooled cold trap system for the SuperCDMS dilution refrigerator

Operating 6,800 feet underground at the SNOLAB facility in Sudbury, Ontario, Canada, the dilution refrigerator-cooled SuperCDMS SNOLAB (Super Cryogenic Dark Matter Search at the Sudbury Neutrino Observatory Laboratory) experiment has been designed for maximum cryogenic up-time and remote operations. A key element in achieving these goals is a pair cold traps in the helium circulation stream of the dilution refrigerator; the first operating near liquid nitrogen temperatures and the second operating near liquid helium temperatures. Previous experience with the CDMS experiment, located underground at the Soudan Under-ground Laboratory, has given significant operational experience with dilution refrigerator cold traps and has solidified the demand of a system of dual cold traps. Unlike the CDMS-era system, the new SuperCDMS system will feature a cryocooler powered liquid nitrogen re-liquefying system (as opposed to regular under-ground re-filling of cold trap dewars using portable nitrogen dewars) and a cryogen-free 4 K cold trap, which eliminates the need for a bath of liquid helium.

43 PARTICLE ACCELERATORS↗
DOE OSTI2022

Analyzing BMP2, FGFR, and TGF Beta Expressions in High-Grade Osteosarcoma Untreated and Treated Autografts Using Proteomic Analysis

In the last few decades, biological reconstruction techniques have improved greatly for treating high-grade osteosarcoma patients. To conserve the limb, and its function the affected tumor-bearing bones have been treated using liquid nitrogen and irradiation processes that enable the removal of entire tumors from the bone, and these treated autografts can be reconstructed for the patients. Here, we focus on the expressions of the growth factor family proteins from the untreated and treated autografts that play a crucial role in bone union, remodeling, and regeneration. In this proteomic study, we identify several important cytoskeletal, transcriptional, and growth factor family proteins that showed substantially low levels in untreated autografts. Interestingly, these protein expressions were elevated after treating the tumor-bearing bones using liquid nitrogen and irradiation. Therefore, from our preliminary findings, we chose to determine the expressions of BMP2, TGF-Beta, and FGFR proteins by the target proteomics approach. Using a newly recruited validation set, we successfully validate the expressions of the selected proteins. Furthermore, the increased growth factor protein expression after treatment with liquid nitrogen may contribute to bone regeneration healing, assist in faster recovery, and reduce local recurrence and metastatic spread in high-grade sarcoma patients.

60 APPLIED LIFE SCIENCES↗
DOE OSTI2025

Integration and commissioning plan of Full Flow Purifier at Muon Campus

The Full Flow Purifier for Fermilab’s Muon Campus uses a charcoal bed surrounded by a liquid nitrogen jacket to purify up to 240 g/s of helium gas. Fabrication by Ability Engineering Technology Inc. has been completed and the purifier delivered to Fermilab. It is the largest purifier to be used at Fermilab based on both capacity and size. A previous paper discussed the design of purifier for various operational conditions and horizontal shipping. The purifier is designed to withstand 5g force in vertical and 2g force in lateral and longitudinal directions. Transportation experience from vendor to Fermilab and within site is discussed. Integration of the purifier involved design and fabrication of a liquid nitrogen transfer line, regeneration system, and helium piping to connect it to Muon Campus cryogenic system. It also involved establishing electrical, instrumentation and controls connections to the system. Integration of the purifier is discussed in detail. The purifier is to be commissioned using up to 4 MYCOM helium compressors to supply helium and liquid nitrogen supplied by a 15,000 -gallon tank. Actual effectiveness of the 3-stream heat exchanger is to be estimated based on measured temperatures and flow rate. Impurity levels shall be monitored at inlet and outlet of the purifier. Theoretical adsorption capacity of the purifier is calculated based on the measured temperatures and flowrates and is compared to actual adsorption capacity over time.

Subedi, Jeewan [Fermilab]↗
DOE OSTI2025

Integration and commissioning plan of Full Flow Purifier at Muon Campus

The Full Flow Purifier for Fermilab's Muon Campus uses a charcoal bed surrounded by a liquid nitrogen jacket to purify up to 240 g/s of helium gas. Fabrication by Ability Engineering Technology Inc. has been completed and the purifier delivered to Fermilab. It is the largest purifier to be used at Fermilab based on both capacity and size. A previous paper discussed the design of purifier for various operational conditions and horizontal shipping. The purifier is designed to withstand 5g force in vertical and 2g force in lateral and longitudinal directions. Transportation experience from vendor to Fermilab and within site is discussed. Integration of the purifier involved design and fabrication of a liquid nitrogen transfer line, regeneration system, and helium piping to connect it to Muon Campus cryogenic system. It also involved establishing electrical, instrumentation and controls connections to the system. Integration of the purifier is discussed in detail. The purifier is to be commissioned using up to 4 MYCOM helium compressors to supply helium and liquid nitrogen supplied by a 60,000-liter tank. Actual effectiveness of the 3-stream heat exchanger is to be estimated based on measured temperatures and flow rate. Impurity levels will be monitored at inlet and outlet of the purifier. Theoretical adsorption capacity of the purifier is calculated based on the measured temperatures and flowrates and is compared to actual adsorption capacity over time.

Subedi, J. [Fermilab] (ORCID:0009000185837576)↗
DOE OSTI2022

Preliminary design of a helium cryogenic system for SAND detector at LBNF-DUNE near site

The Long-Baseline Neutrino Facility (LBNF) is providing a helium cryogenic system to support the superconducting solenoid magnet of the System for on-Axis Neutrino Detection (SAND) for the Deep Underground Neutrino Experiment (DUNE) Near Site at Fermilab in Batavia, IL. The design started in 2020 and construction is set to begin in the mid 2020‘s.The helium cryogenic system primarily consists of a helium refrigerator system, distribution valve boxes, vacuum-jacketed helium and nitrogen transfer lines, warm gaseous helium transfer system, instruments and control system, and gaseous helium storage tanks. It is designed to provide supercritical helium at around 3 bara and 5 K with expansion from 3 to 1.2 bara in the SAND cryostat and 70K forced cold gas helium to cool the thermal shields of the SAND cryostat. The SAND superconductive magnet is indirectly cooled through a liquid helium thermosiphon cycle. A pair of 3 kA leads is cooled by the gas helium vaporized from the liquid helium reservoir in the cryostat turret. The helium system will share the liquid nitrogen tank and liquid nitrogen phase separator with the Near Site Liquid Argon system. The helium recycle compressor system, GHe tanks and LN2 tank will be located on the Surface. The cryogenic facilities including refrigerator cold box, valve boxes and LN2 phase separator will be located on the shaft cryo-mezzanine in the underground cavern. The shaft connecting surface and cavern is more than 60 meter deep. The helium vacuum-jacketed transfer line between the cold box and the SAND magnet is more than 50 meter long. This paper presents the preliminary design of the helium cryogenic system including the design scheme, process flow diagram, heat load estimates, layout plan and so on.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2023

Understanding Interfacial Electrochemical Reactions through in situ ec-STEM and IL-Cryo-STEM

A major criterion in the design of next generation materials for electrical energy storage applications is a comprehensive understanding of interfacial electrochemical reactions as well as correlating the structure and chemistry across site-specific electrode/electrolyte interfaces with electron, charge, and mass transport processes as they govern performance characteristics. Scanning transmission electron microscopy (STEM) based techniques have emerged as an indispensable materials characterization tool that provides high spatial resolution imaging and chemical analysis and has been effectively utilized to obtain an atomic to nanoscale view of the interfacial structure before and after electrochemical cycling. More recently, there have been several advances that now allows us to obtain more detailed mechanistic insight into evolving reactions through in situ ec-STEM and electrical biasing platforms such as in the understanding of the mechanisms of solid electrolyte interphase formation, lithium dendrite nucleation and growth mechanisms and ionic transport mechanisms within intercalation, conversion, and alloying electrode materials. Several major advantages of the in situ ec-STEM approach is the quantitative electrochemical measurement of charge passed during cycling with simultaneous analysis of the electrochemical processes with STEM imaging and diffraction. Here, while spectroscopic analysis of the electrochemical reactions products has been performed, there is the issue of beam sensitivity and therefore, Cryo-STEM imaging combined with electron energy loss spectroscopy (EELS) techniques have been employed to analyze the chemistry of the SEI and Li dendrites. In this talk, we discuss the potential for combining identical location (IL) STEM techniques with Cryo-EM. The advantage of using this approach is that the sample is placed on a conventional TEM grid and the exact same location of the specimen can be analyzed before and after quantitative electrochemical measurements. Moreover, since the sample is on the TEM grid, the grid itself can be prepared for further Cryo-TEM experiments by plunge freezing in liquid nitrogen then transferred to the Cryo-TEM under liquid nitrogen. Results obtain from these experiments can be used to enhance our scientific understanding of interfacial chemistry at electrode/electrolyte interfaces and may be useful in the design of new materials.

36 MATERIALS SCIENCE↗