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Lunar maria igneous rock compositions and magmatic liquid viscosity from samples 12021 and 12022, using microprobe analyses
Lunar samples are magnetic primarily due to the body centered cubic (BCC) iron and iron-nickel alloys they contain. Presented for the first time are results which demonstrate that the magnitude of the martensitic thermal remanence (MTRM) induced on quenching iron-nickel alloy in the geomagnetic field depends on the nickel content of the alloy. High magnetic stability is due to the increasing dislocation density and increasingly complex microstructures associated with increasing nickel content in the alloys. The results agree with the mechanical and structural properties of the alloys. The characteristic quench martensite microstructure observed on metallographic examination provides a recognition criterion for the MTRM mechanism. These results are important for lunar and meteoritic research intending to ascertain the paleofield responsible for the observed remanent magnetization.-
The flow characteristics of lunar compositions 15555 and 68502 have been determined over a wide range of viscosity. The temperature ranges covered by the measurements are 1201-1410 and 622-695 C for the 15555 composition and 1261-1515 and 725-840 C for 68502 composition. Reliable data could not be obtained over the intermediate ranges of temperature because of the occurrence of crystallization. The experimental data in the high temperature regions are found to be in close agreement with predictions of the semiempirical model of Bottinga and Weill. The results on these compositions are compared with previous data on other lunar compositions and on anorthite; and the importance of the flow behavior in interpreting lunar flows and phase morphologies is emphasized. Data are also reported on the kinetics of crystallization of the 15555 composition over the temperature interval from 700 to 1020 C.
Lunar compositional constraints are derived on the basis of geophysical data (in particular, the lunar seismic model as revised by Nakamura) and petrological arguments. Only in the case of extreme assumptions can critical aspects of bulk lunar composition be demonstrated to be equivalent to the present-day terrestrial mantle; specifically, the moon has an Mg number that is too low and an alumina abundance that is too high. Over a broad range of crustal densities the presence of a metallic core at least 150 km in radius is necessary to reconcile the upper mantle lunar seismic model with mass and moment of inertia constraints. A significant seismic discontinuity at 500 km depth may mark the lowest extent of early lunar differentiation, possibly representing a transition between highly fractionated upper mantle and less fractionated, perhaps even primordial, middle/lower mantle.
The evolution of major mineral compositions and trace element abundances during perfect fractional crystallization of a model lunar magma ocean was calculated. The minerals in the model lunar composition were olivine, orthopyroxene, clinopyroxene, and plagioclase. Lunar bulk composition data, major mineral/melt equilibria data, and trace element partition data were taken from published sources. The results show olivine beginning to crystallize at 1380 C. Approximately 50% of the system crystallizes as olivine. From 50 to 60% solidification, orthopyroxene crystallizes alone. During the final 40% solidification, Ca-rich clinopyroxene and plagioclase crystallize together. Various changes in composition of all these minerals are also noted during the process. Concomitant evolution of major element abundances in the melt is followed along with that of trace element abundances. Consequences of the results for constraints on some aspects of the composition of the lunar magma ocean and of the primitive moon are discussed.
Cooling rates required to form glassy or partly-crystalline bodies of 14 lunar compositions have been estimated using a previously introduced, simplified model. The calculated cooling rates are found to be in good agreement with cooling rates measured for the same compositions. Measurements are also reported of the liquidus temperature and glass transition temperature for each composition. Inferred cooling rates are combined with heat flow analyses to obtain insight into the thermal histories of samples 15422, 14162, 15025, 74220, 74241, 10084, 15425, and 15427. The critical cooling rates required to form glasses of 24 lunar compositions, including the 14 compositions of the present study, are suggested to increase systematically with increasing ratio of total network modifiers/total network formers in the compositions. This reflects the importance of melt viscosity in affecting glass formation.
The flow characteristics of lunar compositions 14310 and 14259 have been determined over a wide range of viscosity. The temperature ranges covered by the measurements are 1270 to 1440 C and 700 to 825 C for the 14310 composition and 1154 to 1431 C and 700 to 820 C for the 14259 composition. Reliable data could not be obtained over the intermediate ranges of temperature because of the occurrence of crystallization. The apparent activation energies for viscous flow in the high-temperature and low-temperature regions are respectively about 60 and 160 kcal/gm at for the 14310 composition and 60 and 170 kcal/gm at for the 14259 composition.
The simplified model of glass formation and the development of partial crystallinity in cooled bodies has been applied to lunar compositions 10060, 15028, 15086, 15101, 15286, 15301, 15498, 15499, 60255, 65016, 77017, Apollo 15 green glass and LUNA 24 highland basalt. The critical cooling rates for glass formation predicted by the simplified model are found to be in good agreement (to within an order of magnitude) with those predicted by the exact treatment of crystallization statistics. These predicted critical cooling rates are in even better agreement (a factor of 2) with measured values of the rates required to form glasses of the materials.
The kinetics of crystal growth have been determined over a wide range of temperature, from 800 to 1219 C, for lunar compositions 14259 and 14310. At all temperatures for both compositions the extent of crystal growth is found to be a linear function of time. For both materials, the growth rate versus temperature relations exhibit the form generally found with glass-forming materials. At all temperatures measured, the crystal growth rate of composition 14259 is smaller than that of composition 14310. The maximum growth rate for both compositions occurs at a temperature of about 1120 C. The growth rate data are combined with viscosity data obtained on the same compositions to construct the reduced growth rate versus undercooling relations.
An X-ray spectrometer carried in the Service Module of the Apollo 15 and 16 spacecraft were employed for compositional mapping of the lunar surface. The surface measurements involved observations of the intensity and characteristic energy distribution of the fluorescent X-rays produced by the interaction of the solar X-rays with the lunar surface as well as naturally occurring gamma-rays and cosmic ray produced gamma-rays. A large scale compositional map of approximately twenty percent of the lunar surface was obtained for the first time. It was possible to demonstrate differences between the highlands and the mare and to learn something about the composition of the moon's hidden side. Results obtained from the X-ray experiment and the gamma-ray experiment are consistent with those obtained from lunar sample analysis.
Several spectrometers carried in the Service Module of the Apollo 15 and Apollo 16 spacecraft were employed for the compositional mapping of the lunar surface. The observations involved the measurements of secondary (fluorescent) X-rays, gamma rays and alpha particle emissions. A large scale compositional map of over 20 percent of the lunar surface was obtained for the first time. It was possible to demonstrate interesting chemical differences between the mare and the highlands, to find specific areas of high radioactivity and to learn something about the composition of the moon's hidden side. Further the same devices were used to obtain useful astronomical data during the return to earth.
Several spectrometers carried in the Service Module of the Apollo 15 and Apollo 16 spacecraft were employed for the compositional mapping of the lunar surface. The observations involved the measurements of secondary (fluorescent) X-rays, gamma-rays and alpha particle emissions. A large scale compositional map of over 20 percent of the lunar surface was obtained for the first time. It was possible to demonstrate interesting chemical differences between the mare and the highlands, to find specific areas of high radioactivity and to learn something about the composition of the moon's hidden side.
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A minimally processed composite material derived from lunar soil and possessing tensile strength is described. Laboratory work and the direction of future work are discussed.
Space radiation is a complex mixed field of ionizing radiation that can pose hazardous risks to sophisticated electronics and humans. Mission planning for lunar exploration and long duration habitat construction will face tremendous challenges of shielding against various types of space radiation in an attempt to minimize the detrimental effects it may have on materials, electronics, and humans. In late 2009, the Lunar Crater Observation and Sensing Satellite (LCROSS) discovered that water content in lunar regolith found in certain areas on the moon can be up to 5.6 +/-2.8 weight percent (wt%) [A. Colaprete, et. al., Science, Vol. 330, 463 (2010). ]. In this work, shielding studies were performed utilizing ultra high molecular weight polyethylene (UHMWPE) and aluminum, both being standard space shielding materials, simulated lunar regolith/ polyethylene composites, and simulated lunar regolith mixed with UHMWPE particles and water. Based on the LCROSS findings, radiation shielding experiments were conducted to test for shielding efficiency of regolith/UHMWPE/water mixtures with various percentages of water to compare relative shielding characteristics of these materials. One set of radiation studies were performed using the proton synchrotron at the Loma Linda Medical University where high energy protons similar to those found on the surface of the moon can be generated. A similar experimental protocol was also used at a high energy spalation neutron source at Los Alamos Neutron Science Center (LANSCE). These experiments studied the shielding efficiency against secondary neutrons, another major component of space radiation field. In both the proton and neutron studies, shielding efficiency was determined by utilizing a tissue equivalent proportional counter (TEPC) behind various thicknesses of shielding composite panels or mixture materials. Preliminary results from these studies indicated that adding 2 wt% water to regolith particles could increase shielding of the regolith materials by about 6%. The findings may be utilized to extend the possibilities of potential candidate materials for lunar habitat structures, will potentially impact the design criteria of future human bases on the moon, and provide some guidelines for future space mission planning with respect to radiation exposure and risks posed on astronauts.
The viscous flow behavior of a 9.6-kg lunar rock containing 22.5 wt.% FeO was studied in the temperature ranges from 620 to 700 C and from 1215 to 1400 C. The material was synthesized under mildy reducing conditions to simulate the Fe(2+)/total Fe ratio of the lunar environment. The effect of iron oxidation state on flow behavior in the high viscosity region is studied for specimens of the 15555 composition with Fe(2+) concentration ratios of 0.94, 0.76, and 0.20. A change in ratio from 0.94 to 0.76 had no observable effect on viscosity, whereas a change from 0.76 to 0.20 was accompanied by a drastic increase in viscosity (some three orders of magnitude) at a given temperature, but without changing the form of the variation of viscosity with temperature. The flow behavior is analyzed as a function of the structural features of the glasses.
The goal of the current work was to develop an analytical framework for design of composite struts using various levels of model fidelity. An additional goal of this work was to perform an initial assessment of using automated fiber placement (AFP) and other advanced manufacturing methods to explore their feasibility for the fabrication of struts for lunar landers, strut-braced wings, and other aerospace components. In particular, designs were considered for fabrication at the Integrated Structural Assembly of Advanced Composites (ISAAC) facility at Langley Research Center (LaRC). The designs presented in this paper do not represent the exact geometry and material systems currently in use by the Artemis landing system, but they are considered to be representative. The designs produced during this study will be used to develop manufacturing demonstration units (MDU) that can be fabricated at ISAAC and tested in lab facilities at LaRC
The goal of the current work was to develop an analytical framework for design of composite struts using various levels of model fidelity. Rapid optimization trade studies were performed using low fidelity two-dimensional (2D) axisymmetric models with smeared composite properties. The optimum 2D model was compared with three-dimensional (3D) models with higher levels of fidelity in material property representation. Good agreement was found with all models. The buckling performance of the highest fidelity 3D model was found to be satisfactory for the intended loading conditions. An additional goal of this work was to perform an initial assessment of using automated fiber placement (AFP) and other advanced manufacturing methods to explore their feasibility for the fabrication of struts for lunar landers, strut-braced wings, and other aerospace components. The designs produced during this study are intended to be used to develop manufacturing demonstration units (MDU) that can be fabricated at the Integrated Structural Assembly of Advanced Composites (ISAAC) facility at Langley Research Center (LaRC) and tested in lab facilities at LaRC.