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Liquid scintillation counting technique is applied to the direct measurement of carbon-14 in carbon dioxide. This method has high counting efficiency and eliminates many of the basic problems encountered with previous techniques. The technique can be used to achieve a percent substitution reaction and is of interest as an analytical technique.
Liquid scintillation counting method with sonic oscillations, noting decreased preparation time and increased counting efficiency
Rapid technique for liquid scintillation counting of carbon-14-labelled barium carbonate
Soft betas, the internal conversion electrons, and unconverted gamma rays from lead-210 are efficiently detected in a liquid scintillation counting system with efficiency of 97 percent. The counter is interfaced with a multichannel pulse height analyzer. The spectra obtained is stored on paper tape and plotted on an x-y plotter.
Nuclear densitometer utilizing gamma radiation attenuation to measure liquid oxygen and hydrogen densities
Samples of various clays and minerals were ground or fractured and monitored with a liquid scintillation spectrometer in order to obtain triboluminescent decay curves. Kaolinite samples displayed several million counts/min after grinding, with a surface area emission estimated at tens of billions of photons/sq cm of surface. The photon production rates varied with the origin of the sample, and kaolinite continually yielded higher production rates than bentonite. The addition of water to the samples slightly increased the count rate of emitted light, while the addition of the fluorescent molecule substance tryptofan significantly enhanced the count rate. Freezing smears of kaolinite and montmorillonite in liquid nitrogen and in a salt ice mixture also induced triboluminescence in the montmorillonite. A possible connection between powdery triboluminescent materials formed in mining industries and respiratory disorders among miners is suggested.
A neutron detector sensitive from 2 to 100 MeV is described. The detector is designed for high altitude balloon flight to measure the flux, energy and direction of albedo neutrons from the earth and to search for solar neutrons. A neutron scatter from a proton is required in each of two liquid scintillator tanks spaced 1 meter apart. The energy of the recoil proton in the first tank is obtained from pulse height analysis of the scintillator output. The energy of the recoil neutron is obtained from its time of flight between the tanks. The detector has been calibrated with 15.3 MeV neutrons and mu mesons. The minimum detectable flux is 10(-4) neutron/sq cm/sec at a counting rate of one per minute; the energy resolution is 12% at 15 MeV and 30% at 100 MeV. The angle between the incoming neutron and the recoil neutron is measured to + or - 10 deg.
The results achieved with a 3.5 liter liquid xenon time projection chamber (LXe-TPC) prototype during the first year include: the efficiency of detecting the primary scintillation light for event triggering has been measured to be higher than 85%; the charge response has been measured to be stable to within 0.1% for a period of time of about 30 hours; the electron lifetime has been measured to be in excess of 1.3 ms; the energy resolution has been measured to be consistent with previous results obtained with small volume chambers; X-Y gamma ray imaging has been demonstrated with a nondestructive orthogonal wires readout; Monte Carlo simulation results on detection efficiency, expected background count rate at balloon altitude, background reduction algorithms, telescope response to point-like and diffuse sources, and polarization sensitivity calculations; and work on a 10 liter LXe-TPC prototype and gas purification/recovery system.