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N2SS2O5 crystallizes in the monoclinic P2_1/c space group. The structure is zero-dimensional and consists of eight ammonia molecules, four hydrogen sulfide molecules, and four sulfino hydrogen sulfite molecules.
S3(NO)2 crystallizes in the monoclinic C2/c space group. The structure is zero-dimensional and consists of four S3(NO)2 clusters. N5+ is bonded in a bent 120 degrees geometry to two S2- atoms. There is one shorter (1.55 Å) and one longer (1.64 Å) N–S bond length. There are two inequivalent S2- sites. In the first S2- site, S2- is bonded in a bent 120 degrees geometry to one N5+ and one O2- atom. The S–O bond length is 1.48 Å. In the second S2- site, S2- is bonded in a water-like geometry to two equivalent N5+ atoms. O2- is bonded in a single-bond geometry to one S2- atom.
(NO2)2S3O10 crystallizes in the monoclinic Cc space group. The structure is zero-dimensional and consists of eight hydroxylamine, n-hydroxy- molecules and four trisulfuric acid molecules.
ONS2 crystallizes in the triclinic P-1 space group. The structure is zero-dimensional and consists of four ONS2 clusters. In two of the ONS2 clusters, N2- is bonded in a bent 120 degrees geometry to two S2+ atoms. There is one shorter (1.55 Å) and one longer (1.67 Å) N–S bond length. There are two inequivalent S2+ sites. In the first S2+ site, S2+ is bonded in a single-bond geometry to one N2- atom. In the second S2+ site, S2+ is bonded in a bent 120 degrees geometry to one N2- and one O2- atom. The S–O bond length is 1.48 Å. O2- is bonded in a single-bond geometry to one S2+ atom. In two of the ONS2 clusters, N2- is bonded in a bent 120 degrees geometry to two S2+ atoms. There is one shorter (1.55 Å) and one longer (1.67 Å) N–S bond length. There are two inequivalent S2+ sites. In the first S2+ site, S2+ is bonded in a single-bond geometry to one N2- atom. In the second S2+ site, S2+ is bonded in a bent 120 degrees geometry to one N2- and one O2- atom. The S–O bond length is 1.48 Å. O2- is bonded in a single-bond geometry to one S2+ atom.
N2(SO2N)2 crystallizes in the monoclinic P2_1/c space group. The structure is zero-dimensional and consists of four 1,3,5,2,4,6-trithiatriazinane 1,1,3,3,5,5-hexaoxide molecules and twelve ammonia molecules.