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Guest Editorial for Nondestructive Testing and Evaluation (NDT&E) Special Section

Nondestructive testing and evaluation (NDT&E) are interdisciplinary fields that require a significant amount of interconnection between fundamental physics, measurement techniques, data processing, decision making, and reporting to have a significant impact on industry. NDT&E practitioners are challenged to keep up with the fast-paced evolution of materials, structures, processing, and manufacturing technologies. The development of engineered materials, complex structures and composites, and novel forming techniques require NDT&E to rapidly evolve to meet the needs of industry.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Narrow band photoacoustic lamb wave generation for nondestructive testing using candle soot nanoparticle patches

The generation of ultrasonic surface waves with a photoacoustic-laser-source has become useful for the noncontact nondestructive testing and evaluation (NDT&E) of materials and structures. In this work, a hybrid ultrasound based NDT&E method is proposed based on the photoacoustic-laser-source as a noncontact Lamb wave generator by incorporating a line-arrayed patterned candle soot nanoparticle-polydimethylsiloxane (CSNPs-PDMS) patch as the signal amplifier and with a narrow bandwidth. The CSNP-PDMS composite has been investigated as the functional patch for its laser energy absorption efficiency, fast thermal diffusion, and large thermoelastic expansion capabilities. The signal amplitude (in mW) from the CSNP-PDMS patch exhibits 2.3 times higher amplitude than the no patch condition and a narrower bandwidth than other conditions. Furthermore, improvement in the sensitivity is also achieved through the selection of the aluminum nitride sensing system. The overall combination of the Lamb wave generation and receiver-sensing system in this study is found to be very promising for a broad range of noncontact NDT&E applications.

Acoustic transducers↗

Nondestructive Testing Research and Capabilities at Pacific Northwest National Laboratory

Pacific Northwest National Laboratory (PNNL) is a United States Department of Energy (DOE) multipurpose laboratory operated by Battelle Memorial Institute. The laboratory maintains several technical and scientific capabilities to meet the diverse and challenging needs of sponsors. The Applied Physics Group maintains significant capabilities of interest to the nondestructive testing (NDT) community and regularly collaborates with other technical disciplines to form unique teams in response to specific challenges. This article provides a brief overview of the capabilities of the Applied Physics Group and highlights some activities to demonstrate the scope of capabilities that span from applied research aimed at improving existing NDT methods or processes to more fundamental research efforts that are focused on developing tools to facilitate future paradigms of structural condition monitoring and awareness.

Nondestructive Testing, NDE, Nuclear Power, Phased↗

Nondestructive Testing Research and Development Efforts at Argonne National Laboratory—An Overview

The Nuclear Engineering (NE) Division of Argonne National Laboratory (ANL) has been involved for many years with research and development efforts associated with the nondestructive testing/evaluation (NDT/NDE) of critical components and structures in power generation (nuclear and fossil plants), aerospace, defense, homeland security, medical, and scientific applications. A wide range of NDT methods including electromagnetic, thermal, radiographic, acoustic and ultrasonic methods have been used for a wide range of material evaluation applications. Argonne’s expertise in analytical and numerical modeling of thermal, acoustic and electromagnetic interaction with complex media as well as advanced signal processing and data analysis have been utilized extensively for NDT applications. Three active areas of research, all in connection with NDT of materials and systems utilized in nuclear energy applications, are discussed in detail in this paper.

Eddy current testing↗

A general nonlinear magnetomechanical model for ferromagnetic materials under a constant weak magnetic field

Weak magnetic nondestructive testing (e.g., metal magnetic memory method) concerns the magnetization variation of ferromagnetic materials due to its applied load and a weak magnetic surrounding them. One key issue on these nondestructive technologies is the magnetomechanical effect for quantitative evaluation of magnetization state from stress–strain condition. A representative phenomenological model has been proposed to explain the magnetomechanical effect by Jiles in 1995. However, the Jiles' model has some deficiencies in quantification, for instance, there is a visible difference between theoretical prediction and experimental measurements on stress–magnetization curve, especially in the compression case. Based on the thermodynamic relations and the approach law of irreversible magnetization, a nonlinear coupled model is proposed to improve the quantitative evaluation of the magnetomechanical effect. Excellent agreement has been achieved between the predictions from the present model and previous experimental results. In comparison with Jiles' model, the prediction accuracy is improved greatly by the present model, particularly for the compression case. A detailed study has also been performed to reveal the effects of initial magnetization status, cyclic loading, and demagnetization factor on the magnetomechanical effect. Our theoretical model reveals that the stable weak magnetic signals of nondestructive testing after multiple cyclic loads are attributed to the first few cycles eliminating most of the irreversible magnetization. Remarkably, the existence of demagnetization field can weaken magnetomechanical effect, therefore, significantly reduces the testing capability. This theoretical model can be adopted to quantitatively analyze magnetic memory signals, and then can be applied in weak magnetic nondestructive testing.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

Personnel Qualification and Certification Program in Pressure Decay Leak Testing on the RT-100 Type (B) Cask - 17229

The requirements for qualifications and certification of leak test personnel on Type (B) shipping casks have been more clearly defined with the recent release of ANSI N14.5-2014, Leak Tests on Radioactive Packages for Shipment. The latest version creates a standardized approach for qualifying and certifying personnel to conduct pre-shipment leakage tests on Type (B) packages. The U.S Nuclear Regulatory Commission (NRC) is currently updating the Regulatory Guide R.G 7.4, Leakage Tests on Packages for shipment of Radioactive Material, to endorse ANSI N14.5-2014. According to ANSI N14.5-2014, leakage testing shall be performed in accordance with written procedures by qualified and certified personnel in accordance with the requirements of ASNT SNT-TC-1A-2006, Recommended Practice for Personnel Qualification and Certification in Nondestructive Testing. This is a significant modification to the old standard, ANSI N14.5-1997, which simply states that pressure leak testing shall be conducted by trained and certified personnel without reference to any specific certification standards or regulations. SNT-TC-1A published by the American Society for Nondestructive Testing (ASNT) has several advantages to employers; namely, it allows for a Limited NDT Level II certification program. Limited certifications are especially valuable for personnel who possess limited experience and wish to become a certified Limited NDT Level II in a specific technique on a specific cask using a specific procedure and equipment. Robatel Technologies recently developed a comprehensive qualification and training program based on the recommendations of SNT-TC-1A for Exelon Corporation to certify their employees to a Limited NDT Level II in Pressure Decay Leak Testing on the RT-100 Cask. The project scope included the development of a training and qualification program (Written practice), writing a pressure decay leak test procedure, the design of a pressure decay leak test manifold, and the delivery of classroom training. The written practice outlines the requirements to ensure that personnel participating in the program have the necessary qualification, experience, and training to become certified in the leak test method. The program will give Exelon the liberty to conduct their own leak testing on the RT- 100 without the need to rely on outside resources for leak testing. When fully implemented, the program is expected to improve productivity and eliminate schedule delays, along with substantial economic benefits. Following the appropriate standards and industry best practices, the project was successfully completed and scheduled to be fully implemented by Exelon's Nuclear Stations by the end of 2016. (authors)

07 ISOTOPE AND RADIATION SOURCES↗

Sparse-Data Deep Learning Strategies for Radiographic Non-Destructive Testing

Radiography is an imaging technique used in a variety of applications, such as medical diagnosis, airport security, and nondestructive testing. We present a deep learning system for extracting information from radiographic images. We perform various prediction tasks using our system, including material classification and regression on the dimensions of a given object that is being radiographed. Our system is designed to address the sparse-data issue for radiographic nondestructive testing applications. It uses a radiographic simulation tool for synthetic data augmentation, and it uses transfer learning with a pre-trained convolutional neural network model. Using this system, our preliminary results indicate that the object geometry regression task saw an improvement of 70% in the R-squared value when using a multi-regime model. In addition, we increase the performance of the object material classification tasks by utilizing data from different imaging systems. In particular, using neutron imaging improved the material classification accuracy by 20% when compared to x-ray imaging.

convolutional neural networks↗

Comparative Study of 28 and 18 Years Field Aged Siemens-Arco M55 Modules in Temperate and Hot-Dry Climates

The primary objective of this research work is two-fold: (i) determine the degradation rates of Siemens-Arco M55 modules exposed over 18 and 28 years in a hot-dry climate of Arizona and a temperate climate of California, and; (ii) identify the potential modes responsible for these degradation losses. The degradation rates were determined based on the I-V data obtained on exposed modules and on the corresponding control modules which were not exposed in the fields. The degradation modes responsible for these degradations were determined using several nondestructive tests and destructive tests performed on these control and exposed modules. The nondestructive tests included: current-voltage, visual inspection, cell-module quantum efficiency, and module level reflectance spectroscopy. The destructive tests included: transmittance spectroscopy of glass superstrates, and FTIR, DSC and TGA of encapsulant materials.

14 SOLAR ENERGY↗

Bulk Electrical Cable Non-Destructive Examination Methods for Nuclear Power Plant Cable Aging Management Programs

This Pacific Northwest National Laboratory milestone report describes progress to date on the investigation of nondestructive test methods focusing particularly on bulk electrical test methods that provide key indicators of cable aging and damage. The work includes a review of relevant literature as well as hands-on experimental verification of inspection capabilities. As nuclear power plants consider applying for second, or subsequent, license renewal to extend their operating period from 60 years to 80 years, it is important to understand how the materials installed in plant systems and components will age during that time and develop aging management programs to assure continued safe operation under normal and design basis events (DBE). Normal component and system tests typically confirm the cables can perform their normal operational function. The focus of the cable test program, however, is directed toward the more demanding challenge of assuring the cable function under accident or DBE. The industry has adopted 50% elongation at break (EAB) relative to the un-aged cable condition as the acceptability standard. All tests are benchmarked against the cable EAB test. EAB, however, is a destructive test so the test programs must apply an array of other nondestructive examination (NDE) tests to assure or infer the overall set of cable’s system integrity. Assessment of cable integrity is further complicated in many cases by vendor’s use of dissimilar material for jacket and insulation. Frequently the jacket will degrade more rapidly than the underlying insulation. Although this can serve as an early alert to cable damage, direct test of the cable insulation without violating the protective jacket becomes problematic. This report addresses the range of bulk electrical NDE cable tests that are or could be practically implemented in a field-test situation with a particular focus on frequency domain reflectometry (FDR). The FDR test method offers numerous advantages over many other bulk electrical tests. Two commercial FDR systems plus a laboratory vector network analyzer are used to test an array of aged and un-aged cables under identical conditions. Several conclusions are set forth, and a number of knowledge gaps are identified.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Opportunities and challenges for structural health monitoring of radioactive waste systems and structures

Radioactive waste systems and structures (RWSS) are safety-critical facilities in need of monitoring over prolonged periods of time. Structural health monitoring (SHM) is an emerging technology that aims at monitoring the state of a structure through the use of networks of permanently mounted sensors. SHM technologies have been developed primarily within the aerospace and civil engineering communities. This paper addresses the issue of transitioning the SHM concept to the monitoring of RWSS and evaluates the opportunities and challenges associated with this process. Guided wave SHM technologies utilizing structurally-mounted piezoelectric wafer active sensors (PWAS) have a wide range of applications based on both propagating-wave and standing-wave methodologies. Hence, opportunities exist for transitioning these SHM technologies into RWSS monitoring. However, there exist certain special operational conditions specific to RWSS such as: radiation field, caustic environments, marine environments, and chemical, mechanical and thermal stressors. In order to address the high discharge of used nuclear fuel (UNF) and the limited space in the storage pools the U.S. the Department of Energy (DOE) has adopted a 'Strategy for the Management and Disposal of Used Nuclear Fuel and High-Level Radioactive Waste' (January 2013). This strategy endorses the key principles that underpin the Blue Ribbon Commission's on America's Nuclear Future recommendations to develop a sustainable program for deploying an integrated system capable of transporting, storing, and disposing of UNF and high-level radioactive waste from civilian nuclear power generation, defense, national security, and other activities. This will require research to develop monitoring, diagnosis, and prognosis tools that can aid to establish a strong technical basis for extended storage and transportation of UNF. Monitoring of such structures is critical for assuring the safety and security of the nation's spent nuclear fuel until a national policy for closure of the nuclear fuel cycle is defined and implemented. In addition, such tools can provide invaluable and timely information for verification of the predicted mechanical performance of RWSS (e.g. concrete or steel barriers) during off-normal occurrence and accident events such as the tsunami and earthquake event that affected Fukushima Daiichi nuclear power plant. The ability to verify the conditions, health, and degradation behavior of RWSS over time by applying nondestructive testing (NDT) as well as development of nondestructive evaluation (NDE) tools for new degradation processes will become challenging. The paper discusses some of the challenges associated to verification and diagnosis for RWSS and identifies SHM technologies which are more readily available for transitioning into RWSS applications. Fundamental research objectives that should be considered for the transition of SHM technologies (e.g., radiation hardened piezoelectric materials) for RWSS applications are discussed. The paper ends with summary, conclusions, and suggestions for further work. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Porosity detection in electron beam-melted Ti-6Al-4V using high-resolution neutron imaging and grating-based interferometry

A high-resolution neutron tomography system and a grating-based interferometer are used to explore electron beam-melted titanium test objects. The high-resolution neutron tomography system (attenuation-based imaging) has a pixel size of 6.4 µm, appropriate for detecting voids near 25 µm over a (1.5 cm) 3 volume. The neutron interferometer provides dark-field (small-angle scattering) images with a pixel size of 30 µm. Moreover, the interferometer can be tuned to a scattering length, in this case, 1.97 µm, with a field-of-view of (6 cm)3. The combination of high-resolution imaging with grating-based interferometry provides a way for nondestructive testing of defective titanium samples. A chimney-like pore structure was discovered in the attenuation and dark-field images along one face of an electron beam-melted (EBM) Ti-6Al-4V cube. Tomographic reconstructions of the titanium samples are utilized as a source for a binary volume and for skeletonization of the pores. As a result, the dark-field volume shows features with dimensions near and smaller than the interferometer auto-correlation scattering length.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Nonstationary Infrared Testing of Coatings on Exterior and Interior Surfaces of Metal Shells

A new method for nondestructive testing of coatings on exterior and interior surfaces of metal shells is proposed that is based on video monitoring of the infrared radiation emitted from the shell excited by shortterm external heating. Computer processing of the measured nonstationary field of temperature distribution on the outer surface allows defects with lateral dimensions on the order of or greater than the shell thickness to be revealed on the inner (inaccessible to observation) surface. Geometric characteristics of these defects can be evaluated.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Post-irradiation Examinations of High Burnup PWR Rods - 18456

The High Burnup Spent Fuel Data Project (herein referred to as the 'project'), sponsored by the US Department of Energy (DOE) Office of Nuclear Energy (NE), is focused on experimentally evaluating the effects of long-term storage and transportation on high burnup (HBU) (defined as >45 gigawatt days per metric ton uranium) pressurized water reactor (PWR) spent nuclear fuel (SNF) [1]. To support this project, in the fall of 2017, an instrumented bolted-lid cask (project cask) at the North Anna reactor site was loaded with intact, HBU PWR fuel assemblies (project assemblies) having four different kinds of cladding and will be reopened in approximately 10-years for inspection. To support pre- and post-storage SNF rod characterization, 25 'sister rods' that are similar to the rods being stored in the project cask were extracted from seven different fuel assemblies at the North Anna nuclear power plant for post-irradiation examination (PIE). The sister rod testing program has multiple objectives, including: 1) Baseline testing to provide essential information on the physical condition and properties of the cladding and the fuel in the cladding prior to the loading, drying, and long-term dry storage process (analogous to an experiment control group). Similar tests are expected to be performed at the end of the 10-year storage period on rods extracted from the cask to identify any changes in the properties of the fuel rods that may have occurred during the dry storage period; and 2) Tests to provide material property and physical data using accelerated separate effects tests (SETs) and small-scale tests (SSTs) to explore a wide range of conditions that may occur for other dry storage systems and/or while the fuel is being transported after aging. Testing will be focused on understanding overall SNF rod strength and durability, and be comprised of both composite fuel and defueled clad testing with a focus on measuring cladding material and mechanical properties. Nondestructive testing is currently underway and plans are being updated to support the initial set of destructive tests that are expected to begin by early 2018. While the data generated can be used for multiple purposes, a primary goal of the sister rod PIE data and associated measured mechanical properties are expected to support existing fuel storage licensing and relicensing activities by addressing identified knowledge gaps, and enhance the technical bases for post-storage transportation, handling, and consolidation activities [1]. This paper presents results obtained from the sister rod testing to date, and describes some of the planned measurements, equipment, and procedures that will be implemented for the initial set of destructive examinations. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗