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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2015

Scalable synthesis and post-modification of a mesoporous metal-organic framework called NU-1000

The synthesis of NU-1000, a highly robust mesoporous (containing pores >2 nm) metal-organic framework (MOF), can be conducted efficiently on a multigram scale from inexpensive starting materials. Tetrabromopyrene and (4-(ethoxycarbonyl)phenyl)boronic acid can easily be coupled to prepare the requisite organic strut with four metal-binding sites in the form of four carboxylic acids, while zirconyl chloride octahydrate is used as a precursor for the well-defined metal oxide clusters. NU-1000 has been reported as an excellent candidate for the separation of gases, and it is a versatile scaffold for heterogeneous catalysis. In particular, it is ideal for the catalytic deactivation of nerve agents, and it shows great promise as a new generic platform for a wide range of applications. Multiple post-synthetic modification protocols have been developed using NU-1000 as the parent material, making it a potentially useful scaffold for several catalytic applications. The procedure for the preparation of NU-1000 can be scaled up reliably, and it is suitable for the production of 50 g of the tetracarboxylic acid containing organic linker and 200 mg–2.5 g of NU-1000. The entire synthesis is performed without purification by column chromatography and can be completed within 10 d.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2021

Measurements of $\overline{\nu}_{\mu}$ and $\overline{\nu}_{\mu} + \nu_{\mu}$ charged-current cross-sections without detected pions or protons on water and hydrocarbon at a mean anti-neutrino energy of 0.86 GeV

We report measurements of the flux-integrated $\overline{\nu}_\mu$ and $\overline{\nu}_\mu+\nu_\mu$ charged-current cross-sections on water and hydrocarbon targets using the T2K anti-neutrino beam with a mean beam energy of 0.86 GeV. The signal is defined as the (anti-)neutrino charged-current interaction with one induced $\mu^\pm$ and no detected charged pion or proton. These measurements are performed using a new WAGASCI module recently added to the T2K setup in combination with the INGRID Proton Module. The phase space of muons is restricted to the high-detection efficiency region, $p_{\mu}>400~{\rm MeV}/c$ and $\theta_{\mu}<30^{\circ}$, in the laboratory frame. An absence of pions and protons in the detectable phase spaces of $p_{\pi}>200~{\rm MeV}/c$, $\theta_{\pi}<70^{\circ}$ and $p_{\rm p}>600~{\rm MeV}/c$, $\theta_{\rm p}<70^{\circ}$ is required. In this paper, both the $\overline{\nu}_\mu$ cross-sections and $\overline{\nu}_\mu+\nu_\mu$ cross-sections on water and hydrocarbon targets and their ratios are provided by using the D’Agostini unfolding method. The results of the integrated $\overline{\nu}_\mu$ cross-section measurements over this phase space are $\sigma_{\rm H_{2}O}=(1.082\pm0.068(\rm stat.)^{+0.145}_{-0.128}(\rm syst.)) \times 10^{-39}\,{\rm cm^{2} / nucleon}$, $\sigma_{\rm CH}=(1.096\pm0.054(\rm stat.)^{+0.132}_{-0.117}(\rm syst.)) \times 10^{-39}\,{\rm cm^{2} / nucleon}$, and $\sigma_{\rm H_{2}O}/\sigma_{\rm CH} = 0.987\pm0.078(\rm stat.)^{+0.093}_{-0.090}(\rm syst.)$. The $\overline{\nu}_\mu+\nu_\mu$ cross-section is $\sigma_{\rm H_{2}O} = (1.155\pm0.064(\rm stat.)^{+0.148}_{-0.129}(\rm syst.)) \times 10^{-39}\,{\rm cm^{2} / nucleon}$, $\sigma_{\rm CH}=(1.159\pm0.049(\rm stat.)^{+0.129}_{-0.115}(\rm syst.)) \times 10^{-39}\,{\rm cm^{2} / nucleon}$, and $\sigma_{\rm H_{2}O}/\sigma_{\rm CH}=0.996\pm0.069(\rm stat.)^{+0.083}_{-0.078}(\rm syst.)$.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2016

Search for the rare decay $K^+\to\mu^+\nu\bar\nu\nu$

Evidence of the $K^+\to\mu^+\nu\bar\nu\nu$ decay was searched for using E949 experimental data with an exposure of $1.70\times 10^{12}$ stopped kaons. The data sample is dominated by the backgrond process $K^+\to\mu^+\nu_\mu\gamma$. An upper limit on the decay rate $\Gamma(K^+\to\mu^+\nu\bar\nu\nu)< 2.4\times 10^{-6}\Gamma(K^+\to all)$ at 90% confidence level was set assuming the Standard Model muon spectrum. The data are presented in such a way as to allow calculation of rates for any assumed $\mu^+$ spectrum.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2021

Measurement of charged-current $\nu_{\mu}$ and $\nu_e$ interactions with wire-cell in MicroBooNE towards a search for low-energy $\nu_e$ excess

This technote summarizes the existing work in searching for $\nu_e$ low-energy excess (eLEE) in MicroBooNE Booster Neutrino Beam (BNB) data stream based on the Wire-Cell event reconstruction paradigm. The charged-current $\nu_{\mu}$ and $\nu_e$ events are selected from the 5.3e19 POT data from the BNB beam and 2.06e20 POT data from Neutrinos at the Main Injector (NuMI) beam. The charged-current $\nu_e$ selection results from the BNB data that are sensitive to the eLEE search are not included. Various comparisons between data and Monte Carlo predictions are performed to validate the overall model and demonstrate the power of the analysis techniques.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2021

A Joint Measurement of $\nu_{\mu}$-Disappearance and $\nu_{e}$e-Appearance in the NuMI beam using the NOvA Experiment

The discovery of neutrino oscillations provides the first indication of a lepton flavor violating (LFV) process, one that isn't predicted by the Standard Model. As such, NOvA is part of a rich experimental program to constrain unknown parameters in the neutrino oscillation model, described for three neutrino flavors using the PMNS unitary matrix. It is a long baseline experiment utilizing two detectors, a Near Detector at Fermilab and a Far Detector in Ash River, Minnesota for a total baseline of 810 km. It receives a predominantly ${\nu_\mu}/\overline{\bar\nu_\mu}$ beam peaking at 1:8 GeV from the NuMI beam facility at Fermilab. There are four oscillation channels used in the analysis, ${\nu_\mu} \to {\nu_\mu}$, ${\nu_\mu} \to {\nu_e}$, ${\overline{\nu}_\mu} \to {\overline{\nu}_\mu}$ and ${\overline{\nu}_\mu} \to {\overline{\nu}_e }$. With a total exposure of 13:6_10$^{20}$ and 12:5_10$^{20}$ protons on target for the neutrino and anti-neutrino beam modes respectively, 82 candidates are seen in the ${\nu_\mu} \to {\nu_e}$ channel for a total predicted backgroundof 26:8 events. Similarly, 33 candidates are seen in the corresponding anti-neutrino channel for a total predicted background of 14:0 events. In the ${\nu_\mu} \to {\nu_\mu}$ $(\overline{\nu}_\mu \to \overline{\nu}_\mu}$ channel, 211 (105) candidates are seen with an expectation of 1156.1 (488.1) events at no oscillations.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2018

New $\nu_e + \bar{\nu}_e$ Appearance Results from NOvA [Slides]

aNOvA (the NuMI Off-Axis $\nu_{e}$ Appearance Experiment) utilizes a near detector at Fermilab and a far detector 810 km away in Ash River, MN, to study the properties of neutrinos. Using a beam originating at Fermilab, NOvA studies neutrino oscillation via the disappearance of $\nu_{\mu}$, $\bar{\nu_{\mu}}$ in the beam and the corresponding appearance of $\nu_{e}$, $\bar{\nu_{e}}$. Prior results from NOvA have studied $\nu_{\mu} \rightarrow \nu_{e}$ with the accumulated neutrino interactions from approximately 9x10$^{20}$ protons on target (POT), full detector equivalent. In the time since, NOvA has accumulated anti-neutrino data to study $\bar{\nu_{\mu}} \rightarrow \bar{\nu_{e}}$ with approximately 7x10$^{20}$ POT. Though adding to the level of complexity in the analysis, this combined dataset provides enhanced sensitivity to important unresolved oscillation parameters, such as mixing angles, mass splitting and ordering, and the CP violating phase. Aspects of the appearance channel ($\nu_{e}$ and $\bar{\nu_{e}}$) analysis and results for NOvA's first study combining neutrino and antineutrino data will be discussed.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2023

Measurement of electroweak $Z\left(\nu \overline{\nu}\right)\gamma jj$ production and limits on anomalous quartic gauge couplings in pp collisions at $\sqrt{s}$ = 13 TeV with the ATLAS detector

The electroweak production of $Z\left(\nu \overline{\nu}\right)\gamma jj$ in association with two jets is studied in a regime with a photon of high transverse momentum above 150 GeV using proton–proton collisions at a centre-of-mass energy of 13 TeV at the Large Hadron Collider. The analysis uses a data sample with an integrated luminosity of 139 fb –1 collected by the ATLAS detector during the 2015–2018 LHC data-taking period. This process is an important probe of the electroweak symmetry breaking mechanism in the Standard Model and is sensitive to quartic gauge boson couplings via vector-boson scattering. The fiducial $Z\left(\nu \overline{\nu}\right)\gamma jj$ cross section for electroweak production is measured to be ${0.77}_{-0.30}^{+0.34}$ fb and is consistent with the Standard Model prediction. Evidence of electroweak $Z\left(\nu \overline{\nu}\right)\gamma jj$ production is found with an observed significance of 3.2σ for the background-only hypothesis, compared with an expected significance of 3.7σ. The combination of this result with the previously published ATLAS observation of electroweak $Z\left(\nu \overline{\nu}\right)\gamma jj$ production yields an observed (expected) signal significance of 6.3σ (6.6σ). Limits on anomalous quartic gauge boson couplings are obtained in the framework of effective field theory with dimension-8 operators.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2019

Extraction of Neutrino Oscillation Parameters using a Simultaneous Fit of $\nu_{\mu}$ Disappearance and $\nu_{e}$ Appearance data with the NOvA Experiment

This thesis presents the analyses and results of the $\nu_{\mu} \rightarrow \nu_{\mu}$ disappearance and $\nu_{\mu} \rightarrow \nu_{e}$ appearance due to neutrino oscillations using 8.85 $\times$ 10$^{20}$ protons on target (POT) equivalent of data collected by the NOvA experiment. The data analyzed in this thesis was collected from February 06, 2014 to February 20, 2017. NOvA is an accelerator-based, long-baseline neutrino oscillation experiment and uses the two detector set-up to study the phenomenon of neutrino oscillation using a beam of muon neutrinos produced at Fermilab. One NOvA detector is placed within the Fermilab campus, 100 m underground, at a distance of 1 km from the neutrino source and is called the Near Detector (ND). The ND is 300 ton in mass and smaller in size than the Far Detector (FD) which is 14 kton in mass and is placed 810 km away from the neutrino source in Ash River, Minnesota (MN). Both ND and FD are made of the same material and are functionally identical. The ND being closer to the neutrino source, analyzes the neutrino beam before the neutrinos oscillate and the FD analyzes the neutrinos after oscillations. The ND is used to predict the signal and background expectations in the FD. The similarity in the ND and FD help to reduce the systematic uncertainties in the FD prediction. The combined oscillation fit to the $\nu_{\mu} \rightarrow \nu_{\mu}$ disappearance and $\nu_{\mu} \rightarrow \nu_{e}$ appearance gives the best fit values of the $\Delta m^{2}_{32}$, $\sin^{2}{\theta_{32}}$ and $\delta_{CP}$ oscillation parameters and are presented in this thesis.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2018

A Measurement of $\nu_e$ Appearance and $\nu_\mu$ Disappearance Neutrino Oscillations with the NOvA Experiment

NOvA is a two-detector, neutrino oscillation experiment on an 810 km baseline in the NuMI beam at Fermilab. NuMI is an off-axis, narrow-band beam centered near 1.8 GeV and is configurable to send a high-purity $\nu_\mu$ or $\bar{\nu}_\mu$ neutrino flux which passes through the NOvA far detector, sensitive to $\nu_\mu$ and $\bar{\nu}_\mu$ disappearance and $\nu_e$ and $\bar{\nu}_e$ appearance. The NOvA near and far detectors are functionally identical, liquid scintillator trackers. They are finely segmented relative to the radiation length in the detectors allowing for the detailed reconstruction of electromagnetic shower necessary to identify $\nu_e$ CC events. Through a joint analysis of the appearance and disappearance oscillation channels using neutrino and anti-neutrino data, NOvA constrains the allowed parameter space in $\delta_{CP}$, the neutrino mass hierarchy, $\sin^2\theta_{23}$, and $\Delta m^2_{32}$. We observe 58 and 18 appearance candidates on an expected backgr ound of 15.06 and 5.32 events in neutrino and anti-neutrino mode, respectively. This observation gives a $1.77\sigma$ preference for the normal mass hierarchy and $1.7\sigma$ preference for $\theta_{23} > \pi/4$. NOvA will maintain its position as a long-baseline oscillation experiment with leading sensitivity for several more years in which time analysis will further disambiguate the fundamental neutrino parameters that determine oscillation behavior.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2025

Observation of the ${K}^{+}\to {\pi}^{+}\nu \overline{\nu}$ decay and measurement of its branching ratio

A measurement of the ${K}^{+}\to {\pi}^{+}\nu \overline{\nu}$ decay by the NA62 experiment at the CERN SPS is presented, using data collected in 2021 and 2022. This dataset was recorded, after modifications to the beamline and detectors, at a higher instantaneous beam intensity with respect to the 2016–2018 data taking. Combining NA62 data collected in 2016–2022, a measurement $\mathcal{B} ({K}^{+}\to {\pi}^{+}\nu \overline{\nu}) = \large{(}13.0^{+3.3}_{-3.0}\large{)}$ x $10^{-11}$ of is reported. With 51 signal candidates observed and an expected background of $18^{+3}_{-2}$ events, $\mathcal{B} ({K}^{+}\to {\pi}^{+}\nu \overline{\nu})$ becomes the smallest branching ratio measured with a signal significance above 5σ.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2024

Observation of the semileptonic decays $$ {\textrm{D}}^0\to {\textrm{K}}_{\textrm{S}}^0{\pi}^{-}{\pi}^0{\textrm{e}}^{+}{\nu}_{\textrm{e}} $$ and $$ {\textrm{D}}^{+}\to {\textrm{K}}_{\textrm{S}}^0{\pi}^{+}{\pi}^{-}{\textrm{e}}^{+}{\nu}_{\textrm{e}} $$

Abstract By analyzinge + e − annihilation data corresponding to an integrated luminosity of 2.93 fb −1 collected at a center-of-mass energy of 3.773 GeV with the BESIII detector, the first observation of the semileptonic decays$$ {D}^0\to {K}_S^0{\pi}^{-}{\pi}^0{e}^{+}{\nu}_e $$ D 0 → K S 0 π − π 0 e + ν e and$$ {D}^{+}\to {K}_S^0{\pi}^{+}{\pi}^{-}{e}^{+}{\nu}_e $$ D + → K S 0 π + π − e + ν e is reported. In the hypothesis that all events correspond toK 1 (1270) decays, the branching fractions are measured to be$$ \mathcal{B}\left({D}^0\to {K}_1{(1270)}^{-}\left(\to {K}_S^0{\pi}^{-}{\pi}^0\right){e}^{+}{\nu}_e\right)=\left({1.69}_{-0.46}^{+0.53}\pm 0.15\right)\times {10}^{-4} $$ B D 0 → K 1 1270 − → K S 0 π − π 0 e + ν e = 1.69 − 0.46 + 0.53 ± 0.15 × 10 − 4 and$$ \mathcal{B}\left({D}^{+}\to {\overline{K}}_1{(1270)}^0\left(\to {K}_S^0{\pi}^{+}{\pi}^{-}\right){e}^{+}{\nu}^e\right)=\left({1.47}_{-0.40}^{+0.45}\pm 0.14\right)\times {10}^{-4} $$ B D + → K ¯ 1 1270 0 → K S 0 π + π − e + ν e = 1.47 − 0.40 + 0.45 ± 0.14 × 10 − 4 with statistical significance of 5.4σand 5.6σ, respectively. When combined with measurements of theK 1 (1270)→ K + π − πdecays, the absolute branching fractions are determined to be$$ \mathcal{B}\left({D}^0\to {K}_1{(1270)}^{-}{e}^{+}{\nu}_e\right)=\left({1.08}_{-0.13-0.10}^{+0.14+0.08}\pm 0.21\right)\times {10}^{-3} $$ B D 0 → K 1 1270 − e + ν e = 1.08 − 0.13 − 0.10 + 0.14 + 0.08 ± 0.21 × 10 − 3 and$$ \mathcal{B}\left({D}^{+}\to {\overline{K}}_1{(1270)}^0{e}^{+}{\nu}_e\right)=\left({1.70}_{-0.23}^{+0.26}\pm 0.13\pm 0.35\right)\times {10}^{-3} $$ B D + → K ¯ 1 1270 0 e + ν e = 1.70 − 0.23 + 0.26 ± 0.13 ± 0.35 × 10 − 3 . The first and second uncertainties are statistical and systematic, respectively, and the third uncertainties originate from the assumed branching fractions of theK 1 (1270)→ Kππdecays.

Physics↗
DOE OSTI2020

CPT violation sensitivity of NoVA, T2K and INO experiments using $\nu$ and $\bar{\nu}$ oscillation parameters

Charge-Parity-Time (CPT) symmetry allows only identical oscillation parameters for $\nu$ and $\bar{\nu}$. But,different mass and mixing parameters for $\nu$ and $\bar{\nu}$ can give us possible hint for CPT violation or new physics. Using, different oscillation parameters for $\nu$ and $\bar\nu$, we find sensitivity for ($\Delta m^{2}_{32}-\Delta\bar{m}^{2}_{32}$) and ($\sin^{2}\theta_{23}-\sin^{2}\bar{\theta}_{23}$) for long-baseline (T2K and NOvA) and atmospheric neutrino (INO) experiments in different possible combinations of octant for neutrinos and anti-neutrinos. We present the joint sensitivity of the T2K, NOvA and INO experiments to such CPT violating observables.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2017

Extracting Neutrino Oscillation Parameters using a Simultaneous Fit of the $\nu_{e}$ Appearance and $\nu_{\mu}$ Disappearance Data in the NOvA Experiment

NOvA is a two detector, long baseline neutrino oscillation experiment designed to study $\nu_{e}$ ($\bar{\nu}_{e}$) appearance and $\nu_{\mu}$ ($\bar{\nu}_{\mu}$) disappearance in a $\nu_{\mu}$ ($\bar{\nu}_{\mu}$) beam produced at Fermilab. The near detector (ND) is located 100 meters underground at a distance of 1 km from the target whereas the far detector (FD) is located on the surface, 810 km away from the beam source in Ash River, MN. The ND is used to measure the beam before oscillations and the FD measures the oscillated spectrum. The ND and the FD are functionally identical detectors and the ND spectra are extrapolated to the FD to predict the signal and background spectra expected in the FD. The extrapolation and data fitting techniques developed for these analyses within NOvA are presented.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2018

Systematic Uncertainties and Cross-Checks for the NOvA Joint $\nu_\mu$+$\nu_e$ Analysis

The physics goals of NOvA are the constraints of neutrino oscillation parameters such as the octant of $\theta_{23}$, $\delta_{\rm{CP}}$, and the neutrino mass hierarchy via a joint fit to $\nu_{\mu}$ and $\nu_{e}$ oscillation spectrum. We do this by propagating $\nu_{\mu}$ from the world's most intense neutrino beam at Fermilab, over a baseline of 810 km to northern Minnesota, USA, and measure the $\nu_{\mu}$ to $\nu_{e}$ oscillation probability. NOvA announced its latest oscillation results, based on 8.85$\times10^{20}$ (6.9$\times10^{20}$) protons on target neutrino (antineutrino) data. Preliminary results for the allowed values of oscillation parameters are: $\Delta m^2_{32}=2.51^{+0.12}_{-0.08}\times 10^{-3} \mathrm{eV}^2$, $\mathrm{sin}^2\theta_{23} = 0.58 \pm 0.03$ (upper octant), and $\delta_{\rm{CP}}=0.17\pi$ with preference to the normal hierarchy. Reliable constraints on these oscillation parameters require a rigorous treatment of systematic uncertainties and thorough cross-checks. In this paper, we present an overview of the treatment of systematic uncertainties as well as cross-checks using muon removed simulations and cosmic muon bremsstrahlung showers.

Gandrajula, Reddy Pratap↗
DOE OSTI2020

An investigation of the very rare ${K}^{+}\to {\pi}^{+}\nu \overline{\nu}$ decay

The NA62 experiment reports an investigation of the ${K}^{+}\to {\pi}^{+}\nu \overline{\nu}$ mode from a sample of ${K}^{+}$ decays collected in 2017 at the CERN SPS. The experiment has achieved a single event sensitivity of (0.389 ± 0.024) × 10 -10 , corresponding to 2.2 events assuming the Standard Model branching ratio of (8.4 ± 1.0) × 10 -11 . Two signal candidates are observed with an expected background of 1.5 events. Combined with the result of a similar analysis conducted by NA62 on a smaller data set recorded in 2016, the collaboration now reports an upper limit of 1.78 × 10 -10 for the ${K}^{+}\to {\pi}^{+}\nu \overline{\nu}$ branching ratio at 90% CL. This, together with the corresponding 68% CL measurement of (${0.48}_{-0.48}^{+0.72}$) × 10 -10 , are currently the most precise results worldwide, and are able to constrain some New Physics models that predict large enhancements still allowed by previous measurements.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2018

Combined quantum mechanical and molecular mechanical method for metal–organic frameworks: proton topologies of NU-1000

Metal–organic frameworks (MOFs) are materials with applications in catalysis, gas separations, and storage. Quantum mechanical (QM) calculations can provide valuable guidance to understand and predict their properties. In order to make the calculations faster, rather than modeling these materials as periodic (infinite) systems, it is useful to construct finite models (called cluster models) and use subsystem methods such as fragment methods or combined quantum mechanical and molecular mechanical (QM/MM) methods. Here we employ a QM/MM methodology to study one particular MOF that has been of widespread interest because of its wide pores and good solvent and thermal stability, namely NU-1000, which contains hexanuclear zirconium nodes and 1,3,6,8-tetrakis(p-benzoic acid)pyrene (TBAPy 4- ) linkers. A modified version of the Bristow–Tiana–Walsh transferable force field has been developed to allow QM/MM calculations on NU-1000; we call the new parametrization the NU1T force field. We consider isomeric structures corresponding to various proton topologies of the [Zr 6 (μ 3 -O) 8 O 8 H 16 ] 8+ node of NU-1000, and we compute their relative energies using a QM/MM scheme designed for the present kind of problem. We compared the results to full quantum mechanical (QM) energy calculations and found that the QM/MM models can reproduce the full QM relative energetics (which span a range of 334 kJ mol -1 ) with a mean unsigned deviation (MUD) of only 2 kJ mol-1. Furthermore, we found that the structures optimized by QM/MM are nearly identical to their full QM optimized counterparts.

Wu, Xin-Ping↗