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Optical inspection probe permits remote inspection of combustion chambers through 360 degrees, and is fully controllable in terms of elevation, focus, and sweep. It eliminates the hazards of physically entering combustion chamber interiors and throats of rocket engines for inspection.
Improved fiber-optic probes developed for use in dynamic light-scattering measurements. Intended for measuring dynamic backscattering of laser light from concentrated suspensions of particles in liquids, for purpose of determining statistical distributions of sizes of particles. Offers advantages of compactness and ruggedness, and more suitable for industrial environments. Probes immersed in suspensions characterized. Associated lasers, photodetectors, and signal-processing circuits located remotely in safer environments, coupled to probes via optical fibers.
The Halley Optical Probe Experiment (HOPE) will furnish in situ photopolarimetric data on Comet Halley's coma dust cloud and atmosphere. The optical probe concept involves measurements of the polarized spectral radiance in the direction of motion at two points on the spacecraft trajectory, parallel to the direction of motion; their difference is the spatial derivative of the radiance along the line-of-sight, as well as of the light scattered by dust or emitted by gas in a tube along the trajectory. HOPE is proposed for the Giotto spacecraft's flyby of Comet Halley.
A new fiber optic probe is developed to study different parts of the eye. The probe positioned in front of an eye, delivers a low power light from a laser diode into the eye and guides the light which is back scattered by different components (aqueous humor, lens, and vitreous humor) of the eye through a receiving optical fiber to a photo detector. The probe provides rapid determination of macromolecular diffusivities and their respective size distributions in the eye lens and the gel-like material in the vitreous humor. We report alpha-crystalline size distributions, as a function of penetration depth, inside the lens and hyaluronic acid molecular size distribution in the vitreous body. In a clinical setting, the probe can be mounted on a slit-lamp apparatus simply by using a H-ruby lens holder. The capability of detecting cataracts, both nuclear and peripheral, in their early stages of formation, in a non invasive and quantitative fashion, has the potential in patient monitoring and in developing and testing new drugs or diet therapies to 'dissolve' or slow down the cataract formation before surgery is necessary. The ability to detect biochemical and macromolecular changes in the vitreous structure can be very useful in identifying certain diseases of the posterior chamber, e.g., posterior vitreous detachment.
A compact fiber optic probe developed for on-orbit science experiments was used to detect the onset of cataracts, a capability that could eliminate physicians' guesswork and result in new drugs to 'dissolve' or slow down the cataract formation before surgery is necessary. The probe is based upon dynamic light scattering (DLS) principles. It has no moving parts, no apertures, and requires no optical alignment. It is flexible and easy to use. Results are presented for excised but intact human eye lenses. In a clinical setting, the device can be easily incorporated into a slit-lamp apparatus (ophthalmoscope) for complete eye diagnostics. In this set-up, the integrated fiber optic probe, the size of a pencil, delivers a low power cone of laser light into the eye of a patient and guides the light which is backscattered by the protein molecules of the lens through a receiving optical fiber to a photo detector. The non-invasive DLS measurements provide rapid determination of protein crystalline size and its size distribution in the eye lens.
The research work presented in this report has established a new class of backscatter fiber optics probes for remote dynamic light scattering capability over a range of scattering angles from 94 degrees to 175 degrees. The fiber optic probes provide remote access to scattering systems, and can be utilized in either a noninvasive or invasive configuration. The fiber optics create an interference free data channel to inaccessible and harsh environments. Results from several studies of concentrated suspension, microemulsions, and protein systems are presented. The second part of the report describes the development of a new technology of wavefront processing within the optical fiber, that is, integrated fiber optics. Results have been very encouraging and the technology promises to have significant impact on the development of fiber optic sensors in a variety of fields ranging from environmental monitoring to optical recording, from biomedical sensing to photolithography.
This paper documents the design and development of the fiber-optic probes utilized in the flame detection systems used in NASA Langley Research Center's 8-Foot High Temperature Tunnel (8-ft HTT). Two independent flame detection systems are utilized to monitor the presence and stability of the main-burner and pilot-level flames during facility operation. Due to the harsh environment within the combustor, the successful development of a rugged and efficient fiber-optic probe was a critical milestone in the development of these flame detection systems. The final optical probe design for the two flame detection systems resulted from research that was conducted in Langley's 7-in High Temperature Pilot Tunnel (7-in HTT). A detailed description of the manufacturing process behind the optical probes used in the 8-ft HTT is provided in Appendix A of this report.
Electro-optical probe developed to perform noncontact, nondestructive, and relatively noninvasive measurements of electric fields over broad spectrum at millimeter and shorter wavelengths in integrated circuits. Manipulated with conventional intregrated-circuit-wafer-probing equipment and operated without any special preparation of integrated circuits. Tip of probe small electro-optical crystal serving as proximity electric-field sensor.
An optical probe was designed to measure radiation (from inside the arc heater) incident on a test sample immersed in the arc-heated stream. Currently, only crude estimates are available for this incident radiation. Unlike efforts of the past, where the probe line of sight was inclined to the nozzle centerline, the present development focuses on having the probe line of sight coincide with the nozzle centerline. A fiber-coupled spectrometer was used to measure the spectral distribution of incident radiation in the wavelength range of 225 to 900 nm. The radiation heat flux in this wavelength range was determined by integration of measured emission spectral intensity calibrated to incident irradiance from an integrating sphere. Two arc-heater conditions, corresponding to stream bulk enthalpy levels of 12 and 22 MJ/kg, were investigated in the 13-inch diameter nozzle of the Interaction Heating Facility at NASA Ames Research Center. With the probe placed at a distance of 10 inches from the nozzle exit plane, total radiative heat fluxes were measured to be 3.3 and 8.4 W/sq cm for the 12 and 22 MJ/kg conditions, respectively. About 17% of these radiative fluxes were due to bound-bound radiation from atoms and molecules, while the remaining 83% could be attributed to continua (bound-free and/or free-free). A comparison with spectral simulation based on CFD solutions for the arc-heater flow field and with spectroscopic measurements in the plenum region indicates that more than 95% of the measured radiation is generated in the arc region. The total radiative heat flux from the line radiation could increase by a factor of two through contributions from wavelengths outside the measured range, i.e., from the vacuum ultraviolet (wavelengths less than 225 nm) and the infrared (wavelengths greater than 900 nm). An extrapolation of the continuum radiation to these two wavelength regions was not attempted. In the tested configuration, the measured radiative heat flux accounts for only about 1.4% of the nominal heat flux on a flat face model and therefore is considered negligible. In the 6-inch diameter nozzle, on account of shorter path lengths, the radiation heat flux could be significant. Therefore, future tests in the 6-inch nozzle will have radiometers in addition to the optical probe.
An integrated fiber optic probe, comprising a monomode optical fiber fusion spliced to a short length of a graded-index multimode fiber, is fabricated for use as a coherent receiver in dynamic light scattering. The multimode fiber is cleaved to provide a gradient-index fiber lens with a focal length of 125 microns and an f-number close to unity. An integrated fiber receiver is used to measure the intensity-intensity autocorrelation data from a 0.05 percent by weight concentration of an aqueous suspension of polystyrene latex spheres. Analysis of 100 independent data sets indicates that the particle size can be recovered with an accuracy of +/- 1 percent.
This paper demonstrates the utility of a noninvasive backscatter fiber optic probe for dynamic light-scattering characterization of a microemulsion comprising sodium dodecyl sulfate/1-butanol/ brine/heptane. The fiber probe, comprising two optical fibers precisely positioned in a stainless steel body, is a miniaturized and efficient self-beating dynamic light-scattering system. Accuracy of particle size estimation is better than +/- 2 percent.
A fiber-optic probe employing two monomode optical fibers, one for transmitting a Gaussian laser beam to the scattering volume and the second, positioned at some backscatter angle, for receiving the scattered light is described. Performance and suitability of the system for a process control environment is assessed by studying a suspension of polystyrene latex particles over a wide range of sizes and concentrations. The results show that the probe is ideal for a process control environment in industrial and laboratory applications. Particle size is recovered, without any additional corrections for multiple light scattering, in concentrations containing up to 10 percent solids of 39-nm polystyrene latex spheres.
Size and weight of optics reduced considerably. Proposed fiber-optic probe in laser velocimeter smaller (and, therefore, lighter in weight and more maneuverable) than previous probe. Proposed configuration is product of calculations and experiments showing virtual waists serve same purpose. Laser-velocimeter lens brought close to transfer lenses to focus on virtual waists, thereby shortening probe head considerably.
The Halley optical probe experiment (HOPE) aboard the Giotto spacecraft has provided the first measurements of the optical properties of the dust and of some gaseous species (CN, C2, CO/+/ and OH) from inside the coma of comet Halley. The dust spatial distribution, inferred from sunlight scattering, obeys an r exp -2 law for distances from the nucleus r greater than about 2,000 km. The more rapid increase of dust density with distance observed in the innermost coma probably reflects the presence of a jet, or a surge of activity within a few hours before closest approach. The CN and OH signals increase more slowly than the dust signals, but faster than predicted by a simple model (of solar-excited resonance fluorescence) for the distribution of these species. This effect is probably caused in part by the dust contribution, as well as by the production from parent molecules of OH and CN in an excited state.
Multiple-fiber-optical probe developed for use in measuring light scattered at various angles from specimens of materials. Designed for both static and dynamic light-scattering measurements of colloidal dispersions. Probe compact, rugged unit containing no moving parts and remains stationary during operation. Not restricted to operation in controlled, research-laboratory environment. Positioned inside or outside light-scattering chamber. Provides simultaneous measurements at small angular intervals over range of angles, made to include small scattering angles by orienting probe in appropriate direction.
A new fiber optic probe developed for determining transport properties of sub-micron particles in fluids experiments in a microgravity environment has been applied to characterize particulate dispersions/suspensions in various challenging environments which have been hitherto impossible. The probe positioned in front of a sample delivers a low power light (few nW - 3mW) from a laser and guides the light which is back scattered by the suspended particles through a receiving optical fiber to a photo detector and to a digital correlator. The probe provides rapid determination of macromolecular diffusivities and their respective size distributions. It has been applied to characterize various biological fluids, protein crystals, and ophthalmic diseases.
Feasibility evaluation on optical probing of supersonic aerodynamic turbulence with statistical correlation
Protein crystals are experimentally grown in hanging drops in microgravity experiments on-board the Space Shuttle orbiter. The technique of dynamic light scattering (DLS) can be used to monitor crystal growth process in hanging droplets (approx. 30 (L)) in microgravity experiments, but elaborate instrumentation and optical alignment problems have made in-situ applications difficult. In this paper we demonstrate that such experiments are now feasible. We apply a newly developed fiber optic probe to various earth and space (micro- gravity) bound protein crystallization system configurations to test its capability. These include conventional batch (cuvette or capillary) systems, hanging drop method in a six-pack hanging drop vapor diffusion apparatus (HDVDA), a modified HDVDA for temperature- induced nucleation and aggregation studies, and a newly envisioned dynamically controlled vapor diffusion system (DCVDS) configuration. Our compact system exploits the principles of DLS and offers a fast (within a few seconds) means of quantitatively and non-invasively monitoring the various growth stages of protein crystallization. In addition to DLS capability, the probe can also be used for performing single-angle static light scattering measurements. It utilizes extremely low levels of laser power (approx. few (W)) without a need of having any optical alignment and vibration isolation. The compact probe is also equipped with a miniaturized microscope for visualization of macroscopic protein crystals. This new optical diagnostic system opens up enormous opportunity for exploring new ways to grow good quality crystals suitable for x-ray crystallographic analysis and may help develop a concrete scientific basis for understanding the process of crystallization.