CryoEM single particle reconstruction with a complex-valued particle stack
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59 BASIC BIOLOGICAL SCIENCES↗
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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
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Harmonic Slip-Stacking
Particle accelerators employ slip-stacking configurations to store two particle beams with disparate momenta within a single ring. Additionally, A novel slip-stacking configuration employing a harmonic RF cavity was proposed and studied. Anticipated benefits of the harmonic cavity include mitigating parametric resonances, minimizing emittance growth, and significantly expanding the stable longitudinal phase-space area. By surpassing the requirements of PIP-II operation, the harmonic RF cavity will support extending slip-stacking operation for subsequent beam power upgrades of Main Injector, including a proposed cycle rate improvement. Our ongoing research will verify the simulation of harmonic slip-stacking (HSS) operation under RF phase-errors, such as those causes by beam-loading effects.
Habibeh, Mohammad↗
Interactions in misaligned layered materials
The deliberate introduction of stacking faults has been found to induce properties markedly distinct from those of perfectly stacked particles or sheets, with even minute deviations leading to significant alterations in material characteristics. In this review article, we discuss the effects of stacking faults – both linear and rotational – on surface structures influencing ion adsorption, particle–particle affinity governing crystal growth, friction, and electronic properties. In conclusion, our comprehensive overview sheds light on the multifaceted impact of stacking faults on these phenomena, offering insights that bridge multiple disciplines, and provides numerous interdisciplinary research questions, paving the way for future innovations.
36 MATERIALS SCIENCE↗
Cosmic-Ray Detectors With Interdigitated Electrodes
Detectors measure both positions of incidence and energies of incident charged particles. Stack of detector wafers intercept cosmic ray. Measure positions of incidence to determine cosmic-ray trajectory and charge generated within them (proportional to cosmic-ray energy dissipated within them). Interdigital electrode pattern repeated over many rows and columns on tops of detector wafers in stack. Electrode pattern defines pixels within which points of incidence of incident cosmic rays located.
Cunningham, Thomas J.↗
3D Tomography insights on particle-particle bonding in cold spray
The conditions of the target surface during cold spray affect deformation and bonding. While surface preparation can influence the adhesion of the first particles, such modification is not relevant to the particle-particle interfaces that dominate the growth of a coating. Here we study two-particle Cu stacks produced with a single-particle launch apparatus and compare them to single-particle experiments on a clean polished substrate. Serial cross-sectioning using microtomography permits a systematic evaluation and quantification of bonding at the particle-particle interfaces. We observe that the top particle in the two-particle stacks is much more flattened compared to single impacts on the polished substrate. Although the resulting interfacial area expansion is comparable to that of single impacts at the same velocities, bonding at the particle-particle interfaces is significantly less (never exceeding 18% even around the “optimal” velocity for bonding). Lastly, we find that hydrodynamic jetting, a form of localization known to promote adhesion in cold spray, is hindered for impacts on top of a prior particle deposition. Here, the results point to a need for future studies that separately consider topography and mechanical properties of substrates in the pursuit of optimal bonding.
Bonding↗
Tomographic assessment of peening for metallurgical bonding in cold spray
It is widely asserted that peening densifies cold spray coatings and improves particle–particle and particle–substrate bonding, yet systematic studies analyzing the evolution of bonding due to peening particle strikes are scarce. We explore peening at the level of individual particle impacts, by creating two-particle Cu-on-Cu stacks using laser-induced particle impact testing. Exploring impact velocities that range from the onset of bonding at the “critical velocity”, V cr , to its peak near 1.4⋅V cr , we perform full 3D tomography of the particle stacks to characterize the bonding state at the particle-substrate interface. Direct labeling of non-bonded patches and the total particle-substrate interface permits quantification and comparison of bonding in single impacts with bonding after subsequent impacts to reveal the origins of the peening effect. The data reveal a surprising finding: although a second impact directly atop the first particle increases the area of the particle-substrate interface (~40% area increase), there is no improvement in metallurgical bonding. Analysis of these data suggest that not only area expansion (and associated oxide rarefication), but also stress-induced extrusion of metal at that interface needs to occur to achieve metal-on-metal contact to see an enhancement in bonding. Furthermore, our analysis suggests that the subsequent impacting particle needs to have ~70% more kinetic energy to produce additional bonding; this implies that particle and velocity distributions within a spray may be helpful, and that peening may rely on unaligned impacts.
Bonding↗
Reverse segregation and self-organization in inclined chute flows of bidisperse granular mixtures
In the usual segregation scenario for stable inclined chute flows of bidisperse mixtures of fine and coarse spherical particles, coarse particles rise toward the free surface, forming a coarse-rich region atop the flowing pile. Beyond a threshold coarse-to-fine diameter ratio of approximately 4, conversely, the weight of the coarse particles exceeds the segregation driving forces, causing individual coarse particles to sink within the pile and producing a reversed segregation state. However, an understanding of the collective evolution of the pile structure is still lacking when the particle diameter ratio exceeds 4 and the coarse-particle mass fraction is appreciable. To explore this broadly bidisperse limit, we perform discrete element method simulations considering mean particle diameter ratios of up to 8 and coarse-particle mass fractions spanning 0.1 to 0.9. The steady-state flow profiles reveal several intriguing behaviors that depend on the diameter ratio and mass fraction. These include a previously identified transition from usual to reverse segregation and a newfound tendency to self-organize into alternating coarse- and fine-rich particle layers stacked along the shear gradient direction, with layer thickness dictated by the coarse-particle diameter. A fuller understanding of segregation at this scale could pave the way for enhanced mixing or demixing techniques at the commercial scale.
granular flow↗
Towards an understanding of particle-scale flaws and microstructure evolution in cold spray via accumulation of single particle impacts
Cold spray coatings are the sum of countless individual bonding events between single particles impacting on top of one another at high velocities. Thus, the collective behavior of microparticles must be considered to elucidate the origins of coating flaws at the scale of the particles and larger, or the dynamic evolution of the overall coating microstructure. Laser-induced particle impact testing (LIPIT) has been extensively used to study single-particle impacts, and in this work is adapted to study the accumulation of numerous particles with knowledge of each individual particle's impact parameters (particle size, velocity). The method reproducibly deposits stacks of gold particles (>20 particles) with different characteristic spectra of impact velocity. The observation of impact-induced erosion lets us define a critical velocity for material-build-up that is higher than that for single-particle bonding. The quantitative single-particle data are analyzed in a correlative manner to the structure and flaws in the resulting stacks, providing some first statistical connections between, e.g., strain and recrystallization, or aberrant particle characteristics and defects. The results highlight opportunities for the study of many-particle phenomena in microparticle impact—from interaction of particles in cold spray to multi-step erosion processes—with a quantitative view of the behavior of single particles.
Erosion↗
Further measurements and reassessment of the magnetic-monopole candidate
The data on the 1975 Lexan event are reexamined in a framework that does not depend on the details of a particular track model. Instead, visual measurements of two quantities, photographic evidence, and silver-grain densities measured with an automated microscopic-image dissector are cited. It is shown that throughout the detector stack the particle had a roughly constant value of absolute Z/beta of about 109-114 based on energy deposition at radial distance less than about 0.01 micron. Its energy deposition at radial distance greater than about 20 microns was incompatible with that expected from any known cosmic ray nucleus with Z/beta in this range. A monopole is ruled out, and the three candidates compatible with the data are: (1) a slow, supermassive particle with beta about 0.4, charge about 45e, and mass above 1000-10,000 amu; (2) a fast antinucleus with Z/beta about -109 to -114 and absolute Z between 76 and 96; and (3) a very fast nucleus with Z about 110-114 and beta above about 0.99.
Price, P. B.↗
Wide Band Gap Radiation Detectors for Deep Space Science
Understanding how the Sun, Earth, and other objects in the solar system interact with the space radiation environment is crucial for improving activities of humans on Earth and in space. Low-power, low-noise, multidirectional robust detectors for detecting ions with a wide range of mass and energies will provide a more complete understanding of space environment physics. To meet these challenges, new ion detectors based on wide band gap (WBG) semiconductors are being developed for integration on a variety of deep space platforms. NASA Glenn Research Center (GRC) is applying its expertise and facilities in harsh environment instrumentation to develop supporting technologies to enable improved instruments for space science missions. New detector technologies being developed at GRC include SiC solid-state devices as practical robust, thermally stable large area detectors for LET measurements in compact, stacked charged particle telescope. The low-noise, thermally stable nature of the WBG detectors allows a small multidirectional array of charged particle telescopes to be packed in a 6U CubeSat without active cooling for operation in lunar orbit or deep space. Using a full variety of different WBG detectors, an extremely compact instrument to provide multi-directional, comprehensive (composition, velocity, and direction) in-situ measurements of heavy ions in space plasma environments can be realized.
ion detectors↗
Array of micro-machined mass energy micro-filters for charged particles
An energy filter for charged particles includes a stack of micro-machined wafers including plural apertures passing through the stack of wafers, focusing electrodes bounding charged particle paths through the apertures, an entrance orifice to each of the plural apertures and an exit orifice from each of the plural apertures and apparatus for biasing the focusing electrodes with an electrostatic potential corresponding to an energy pass band of the filter.
Stalder, Roland E.↗
Analytical Tools for Cloudscope Ice Measurement
The cloudscope is a ground or aircraft instrument for viewing ice crystals impacted on a sapphire window. It is essentially a simple optical microscope with an attached compact CCD video camera whose output is recorded on a Hi-8 mm video cassette recorder equipped with digital time and date recording capability. In aircraft operation the window is at a stagnation point of the flow so adiabatic compression heats the window to sublimate the ice crystals so that later impacting crystals can be imaged as well. A film heater is used for ground based operation to provide sublimation, and it can also be used to provide extra heat for aircraft operation. The compact video camera can be focused manually by the operator, and a beam splitter - miniature bulb combination provide illumination for night operation. Several shutter speeds are available to accommodate daytime illumination conditions by direct sunlight. The video images can be directly used to qualitatively assess the crystal content of cirrus clouds and contrails. Quantitative size spectra are obtained with the tools described in this report. Selected portions of the video images are digitized using a PCI bus frame grabber to form a short movie segment or stack using NIH (National Institute of Health) Image software with custom macros developed at DRI. The stack can be Fourier transform filtered with custom, easy to design filters to reduce most objectionable video artifacts. Particle quantification of each slice of the stack is performed using digital image analysis. Data recorded for each particle include particle number and centroid, frame number in the stack, particle area, perimeter, equivalent ellipse maximum and minimum radii, ellipse angle, and pixel number. Each valid particle in the stack is stamped with a unique number. This output can be used to obtain a semiquantitative appreciation of the crystal content. The particle information becomes the raw input for a subsequent program (FORTRAN) that synthesizes each slice and separates the new from the sublimating particles. The new particle information is used to generate quantitative particle concentration, area, and mass size spectra along with total concentration, solar extinction coefficient, and ice water content. This program directly creates output in html format for viewing with a web browser.
Arnott, W. Patrick↗
Deciphering volume changes in Li-S solid-state battery components during cycling: Implication for advanced battery design
Here, in this work, we developed custom fixtures to investigate the mechanical and electrochemical behavior of all-solid-state lithium batteries during cycling under constant pressure and constant volume conditions. We successfully monitored vertical displacements during constant pressure cycling and pressure variations during constant volume cycling, allowing us decouple volume changes in the sulfur, Li 2 S cathodes, LixIn anode, and solid-state electrolyte. Scanning electron microscopy and electrochemical impedance spectroscopy confirmed that two structural changes occur during ASSLB cycling: (1) irreversible fractures in the active material particles, and (2) void formation within the electrode matrix. While the fractures in primary particles are permanent, void formation can be mitigated through stack pressure, which promotes particle rearrangement in the electrode matrix. Our findings emphasize the importance of stack pressure in maintaining the microscale integrity of all-solid-state lithium batteries, preventing void formation and enhance battery performance and durability.
Cell Design↗
Nuclear particle detection using a track-recording solid
The design of the nuclear particle detector located in Purdue University's Get Away Special package which was flown aboard STS-7 is detailed. The experiment consisted of a stack of particle-detecting polymer sheets. The sheets show positive results of tracks throughout the block. A slide of each sheet was made for further analysis. Recommendations for similar experiments performed in the future are discussed.
Weber, M.↗
Complex motion of steerable vesicular robots filled with active colloidal rods
Abstract While the collective motion of active particles has been studied extensively, effective strategies to navigate particle swarms without external guidance remain elusive. We introduce a method to control the trajectories of two-dimensional swarms of active rod-like particles by confining the particles to rigid bounding membranes (vesicles) with non-uniform curvature. We show that the propelling agents spontaneously form clusters at the membrane wall and collectively propel the vesicle, turning it into an active superstructure. To further guide the motion of the superstructure, we add discontinuous features to the rigid membrane boundary in the form of a kinked tip, which acts as a steering component to direct the motion of the vesicle. We report that the system’s geometrical and material properties, such as the aspect ratio and Péclet number of the active rods as well as the kink angle and flexibility of the membrane, determine the stacking of active particles close to the kinked confinement and induce a diverse set of dynamical behaviors of the superstructure, including linear and circular motion both in the direction of, and opposite to, the kink. From a systematic study of these various behaviors, we design vesicles with switchable and reversible locomotions by tuning the confinement parameters. The observed phenomena suggest a promising mechanism for particle transportation and could be used as a basic element to navigate active matter through complex and tortuous environments.
42 ENGINEERING↗
Harmonic Slip-Stacking
Slip-stacking is a particle acceleration technique used at Fermilab to increase Main Injector intensity by combining two beams at the cost of longitudinal beam quality.In a conventional beam line, a single beam is typically accelerated and delivered to the experimental area without combining it with another beam
43 PARTICLE ACCELERATORS↗
Vertical Lunar Regolith Conveying as a Flight Experiment in Simulated Lunar-Gravity
Regolith conveying will be an essential task for supplying regolith feedstock to In-Situ Resource Utilization (ISRU) reactor systems for regolith processing on the Moon and Mars. The Vertical Lunar Regolith Conveyor (VLRC) is a technology being developed at NASA Kennedy Space Center (KSC) as a regolith transport task for the GCD ISRU FLEET project led by NASA Glenn Research Center (GRC). Single test loop versions of the VLRC are being developed at NASA KSC as a technology demonstration for a flight experiment. The NASA Flight Opportunities program selected the VLRC for a technology demonstration opportunity on a future Blue Origin New Shepard suborbital launch vehicle to study regolith transport physics in a relevant environment in a vacuum chamber under simulated lunar gravity conditions in order to advance its technology readiness level (TRL) for future space applications. The VLRC system includes four primary subsystems to achieve the objectives of the lunar gravity (Lunar-G) flight experiment. (1) An eccentric vibratory conveyor stack to convey regolith particles consisting of three single-loop helical surface conveyors with each actuated by two vibratory motors that vibrate in unison. One of the three single-loops contains a 0.8°-3.1° inclined helical path and the other two contain a 1.6°-6.2° incline. (2) A stick-slip conveyor stack to convey regolith particles consisting of three single-loop helical surface conveyors with each actuated by the same motor to move in unison in a stick-slip motion. One of the three single-loops contains a 0.8°-3.1° inclined helical path and the other two contain a 1.6°-6.2° incline. (3) A regolith containment system to contain the regolith in each single-loop track during launch before the start of the experiment using containment caps that will be lifted in unison at the start of Lunar-G. (4) COTS cameras will record the motion of regolith and tracer particles. Post-flight analysis of the videos will be used to determine convey speeds and flow rates. The VLRC experiment will use the well-known technique of Particle Image Velocimetry (PIV) image analysis to determine the velocity of tracer particles entrained in the regolith flow. This velocity will be used to calculate the mass flow rate of the regolith being conveyed.
ISRU↗
Levelized cost and carbon intensity of solar hydrogen production via water splitting using a scalable and intrinsically safe photocatalytic Z-scheme raceway system
Generating hydrogen from local energy resources such as solar or wind would unlock a low-carbon energy carrier that could be used to reduce greenhouse gas emissions in sectors such as industry and transportation. Yet, the allocation of new or existing power generation solely to hydrogen production remains contentious due to disputes regarding emissions accounting. Photocatalytic (PC) hydrogen production technologies offer a unique solution, as hydrogen is produced directly from solar energy and water, without the need for electricity generation. However, cost projections for all photocatalytic designs to date have suggested that they are not cost competitive compared to conventional electrolysis systems manufactured at scale. Herein, we offer the first illustrative benchmark of cost and carbon intensity of hydrogen produced in a type 2 “Z-scheme” photocatalytic reactor design, which employs suspended semiconducting nanoconductor particles organized into two stacked volumes in a raceway design. The “Z-scheme” system utilizes two separate photoabsorber particles, tuned to drive either the hydrogen evolution reaction or the oxygen evolution reaction individually, connected via a reversible, charge transfer redox couple in solution. Furthermore, the results suggest a highly competitive and scalable technology, that justifies further experimental validation and prototyping in the field.
Carbon↗