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This presentation is to update DOE at the Molten Salt Program review in May on the work at INL and Argonne National Laboratory on surveillance specimen development. This includes thermal-mechanical testing and test article designs.
Two thermography techniques, passive and active, are used to detect damage initiation and progression in a cyclically loaded composite cylinder. The passive thermography tracks damage progression in real time during cyclic loading. Active flash thermography, using a flash tube enclosed within the cylinder, images delaminations in a cylinder under different loads. A differential thermography processing technique eliminates normal material variations and improves sensitivity to and sizing of delaminations. The thermography results were compared to nonimmersion ultrasonic results.
The fatigue life of composite stiffened panels with indentation damage was investigated experimentally using single stringer compression specimens. Indentation damage was induced on one of the two flanges of the stringer. The experiments were conducted using advanced instrumentation, including digital image correlation, passive thermography, and in-situ ultrasonic scanning. Specimens with initial indentation damage lengths of 37 millimeters to 56 millimeters were tested in fatigue and the effects of cyclic load amplitude and damage size were studied. A means of comparison of the damage propagation rates and collapse loads based on a stress intensity measure and the Paris law is proposed.
The fatigue life of composite stiffened panels with indentation damage was investigated experimentally using single stringer compression specimens. Indentation damage was induced on one of the two flanges of each stringer. The experiments were conducted using advanced instrumentation, including digital image correlation, passive thermography, and in-situ ultrasonic scanning. Specimens with initial indentation damage lengths of 32 millimeters to 56 millimeters were tested quasi-statically and in fatigue, and the effects of cyclic load amplitude and damage size were studied. A means of comparison of the damage propagation rates and collapse loads based on a stress intensity measure and the Paris law is proposed.
The fatigue life and damage tolerance of composite stiffened panels with indentation damage are investigated experimentally using single-stringer compression specimens. The indentation damage was induced to one of the two flanges of the stringer of every panel. The advantages of indentation compared to impact are the simplicity of application, less dependence on boundary conditions, better controllability, and repeatability of the imparted damage. The tests were conducted using advanced instrumentation, including digital image correlation, passive thermography, and in situ ultrasonic scanning. Specimens with initial indentation damage ranging between 32 and 56 mm in length were tested quasi-statically and in fatigue, and the effects of cyclic load amplitude and damage size were studied. A means of comparison of the damage propagation rates and collapse loads based on a stress intensity measure and the Paris law is proposed. The stress intensity measure provides the means to compare the collapse loads of specimens with different damage types and damage sizes, while the Paris law is used to compare the damage propagation rates in specimens subjected to different cyclic loads. This approach enables a comparison of different tests and the potential identification of the effects that influence the fatigue lives and damage tolerance of postbuckled structures with defects.
Lateral shaft vibrations produced by a rotating unbalance weight were damped by means of eddy currents generated in copper conductors that were precessing cyclicly in the gap formed by the pole faces of C-shaped, permanent magnets. The damper assembly, which was located at the lower bearing support of a vertically oriented rotor was completely immersed in liquid nitrogen during the test run. The test rotor was operated over a speed range from 800 to 10,000 rpm. Three magnet/conductor designs were evaluated. Experimental damping coefficients varied from 180 to 530 N sec/m. Reasonable agreement was noted for theoretical values of damping for these same assemblies. Values of damping coefficients varied from 150 to 780 N sec/m. The results demonstrate that passive eddy-current damping is a viable candidate for vibration control in cryogenic turbomachinery.
The potential of the alkaline electrolyte fuel cell as the power source in a multi hundred kilowatt orbital energy storage system was studied. The total system weight of an electrolysis cell energy storage system was determined. The tests demonstrated: (1) the performance stability of a platinum on carbon anode catalyst configuration after 5000 hours of testing has no loss in performance; (2) capability of the alkaline fuel cell to operate to a cyclical load profile; (3) suitability of a lightweight graphite electrolyte reservoir plate for use in the alkaline fuel cell; (4) long life potential of a hybrid polysulfone cell edge frame construction; and (5) long term stability of a fiber reinforced potassium titanate matrix structure. The power section tested operates with passive water removal eliminating the requirement for a dynamic hydrogen pump water separator thereby allowing a powerplant design with reduced weight, lower parasite power, and a potential for high reliability and extended endurance. It is concluded that two perovskites are unsuitable for use as a catalyst or as a catalyst support at the cathode of an alkaline fuel cell.
The Air Force Research Laboratory (AFRL) has developed a passive broadband radio frequency (RF) receiver, called a Sounder Receiver (SoRcer), as an ionospheric diagnostic instrument. These systems can produce ionospheric specifications to characterize the local ionosphere. The specifications from the SoRcers can then be used to inform data-assimilation models; monitor diurnal, seasonal, or other cyclical changes; and detect irregularities or abnormalities in the ionosphere, such as traveling ionospheric disturbances (TIDs), sporadic E, and spread F.
The U.S. Air Force Research Laboratory (AFRL) has developed a passive broadband radio frequency (RF) receiver, called a Sounder Receiver (SoRcer), as an ionospheric diagnostic instrument. These systems can produce ionospheric specifications to characterize the local ionosphere. The specifications from the SoRcers can then be used to inform data assimilation models; monitor diurnal, seasonal, or other cyclical changes; and detect irregularities or abnormalities in the ionosphere, such as traveling ionospheric disturbances (TIDs), sporadic E, and spread F.
The turbine under study incorporates the combination of two features: the application of blade cyclic pitch variation; and the use of yaw angle control for rotor speed and torque regulation. Due to its emasculation by passive cyclic pitch variation the rotor can be rapidly yawed without encountering gyroscopic and aerodynamic hub moments and without noticeable out of plane excursions. The two bladed upwind rotor is vane stabilized and of very simple and rugged design. The principle was first checked out with a small scale wind tunnel model and then tested in the atmosphere with a 7.6 meter diameter experimental fully instrumented wind turbine driving a 3 phase alternator. The test results are summarized with respect to structural dynamics and yaw dynamics.
The electrochemical stability of LiSbF6 and LiPF6 in aprotic organic solvents has been investigated. Electrochemical studies, conductivity measurements, and open-circuit stability tests were conducted on LiSbF6 in tetrahydrofuran and sulfolane. Cyclic voltammetric studies of SbF6(-) were compared with those of AsF6(-) and PF6(-) anions. Sb(V) was reduced to Sb(III), and then to Sb(0). AsF6(-) was reduced to AsF3, while no reduction of PF6(-) was observed. The reduction products of AsF6(-) and SbF6(-) passivated the glassy carbon electrode, presumably due to LiF precipitation. Peak potentials were observed to shift in the positive direction as a function of concentration. This was accounted for on the basis of a follow-up chemical reaction.
A novel additive manufacturing (AM) methodology combined with a compression molding (CM) process has been developed to optimize the microstructure of short fiber thermoplastic composites (SFTs)with higher fiber alignment and lower porosity, yielding superior stiffness, strength, and structural integrity. Here, the current work examines the efficacy of the ‘passive’ infrared thermography (IRT) techniques for rapid fatigue characterization of SFTs that use the surface temperature evolution during cyclic loading due to self-heating as a fatigue indicator. A comparison of fatigue limits obtained from traditional stress-life (SN) (≈53.1%σ uts ) and IRT (≈54.1%σ uts ) shows a close match. However, the SN curve required 18 specimens and two weeks of continuous cyclic testing, while IRT used three specimens with 5 hours of testing. Thus, the IRT approach provides an accelerated testing framework for rapidly estimating the fatigue limit. Additionally, existing phenomenological approaches to IRT fatigue characterization have been examined.
Abstract We produced a 10 Myr synthetic stratigraphic section using a forward stratigraphic model that generates marine deltaic stratigraphy over geological timescales. We recursively fit the model using a Bayesian inversion algorithm to test: (1) if it could be accurately reconstructed; (2) if the parameters used to create it could be recovered; and (3) the sensitivity of the model output to given model parameters and the attendant physical processes. The original synthetic stratigraphic section was produced with cyclical sea‐level variations of 40 and 30 m with 2.4 and 10 Myr periods respectively. Sediment was also supplied cyclically, in 2.4 and 10 Myr cycles with amplitudes of 30 and 80 tons/100 kyr, respectively, varying from a mean of 232 tons/100 kyr. Parameter values were sampled to fit the model using a Markov chain Monte Carlo algorithm, resulting in a ±5 m (1σ) variation between the experimental output and the original. Sea level varied by ±7 m (1σ) within the posterior distribution of parameters. As a result, both the 10 Myr and 2.4 Myr sea‐level cycles could be extracted from the original output. The variation in sediment supply was approximately ±38 tons/100 kyr (1σ) and, as a result, only the larger long‐term supply variations could be accurately recovered in refitting the model. The variation in thermal, flexural and total subsidence across those parameter sets is less than ±10 m (1σ). The original section experienced 150 m of total subsidence at the depocentre. Our results demonstrate the distinct and interpretable imprint of sea level and subsidence on continental margin stratigraphy can be quantified. Moreover, we conclude that sea‐level change produces a defined effect on the geometries of stratigraphic architecture, and that techniques applied for the purpose of delineating sea‐level variation from continental margin strata have a well‐founded conceptual basis.
The overarching purpose of this semester-long internship at the National Aeronautics and Space Administration's (NASA) John F. Kennedy Space Center (KSC) was to study the impacts of corrosion regarding the development of ground support equipment (GSE), launch support structures, and flight hardware in aid of the Space Launch System (SLS) and Orion program. Environmental corrosion is known as one of the largest material degradation issues for any structure comprised of metal on the Space Coast and requires the initiation of special protective measures for proper corrosion mitigation. The four (4) projects to be described were conducted with NASA Civil Servants and NASA Contractors who provided necessary resources to ensure the highest quality of data acquisition and knowledge transfer. The main objective shared between all four (4) of the following projects was to assess the modes by which corrosion takes place in multiple environments as well as the methods by which these modes of corrosion can be reduced for the enhancement of the mechanical, structural, and chemical compatibility of those respective environments with different candidate metals. A multitude of test methods were performed over the duration of this internship to assess the corrosive properties of these different candidate metals.
The influence of the native oxide film on passive film properties and localized corrosion of additively manufactured SS 316L was studied in 1 wt% HCl by XPS characterization, electrochemical polarization curves, and post-test morphology analysis by SEM. Increased Cr oxidation kinetics was observed in the as-polished sample with the native oxide film resulting in formation of an overall more protective and compact film compared to the cathodically-activated sample. Electrochemical analysis showed that corrosive attack varied between dislocation cell boundaries to cell interiors depending on the initial surface state and polarization conditions. In conclusion, a corrosion mechanism is proposed to explain this variation.
Abstract Cellulosic materials offer sustainable advantages for building energy conservation. However, their development has been hindered by reduced thermal performance, often caused by structural collapse during the transition from solution to solid. Inspired by natural goose down, a bio‐based, lightweight insulation foam derived from agricultural waste straw is presented. Through in situ synthesis, bio‐silica fibers with branched structures capable of supporting hollow silica microspheres are fabricated. After steam‐mediated processing, the resulting foam exhibit low density (95 mg cm − 3 ), high porosity (95.5%), low thermal conductivity (0.03 ± 0.003 W mK −1 ), and a cyclic compressive strength of 90 kPa at 50% strain. Owing to the synergistic microstructure formed by branched bio‐fibers and hollow silica spheres, the bio‐silica foam exhibit outstanding thermal insulation performance relative to other bio‐based foams prepared by ambient drying. A passivated insulation panel is further developed by incorporating this material as the core component, achieving a thermal conductivity of 0.0275 W mk −1 and flexural strength of 6.85 MPa. The panel demonstrated durability with stable thermal performance throughout a 60‐day outdoor test. Moreover, the bio‐silica foam shows a carbon footprint of 7.50 kgCO₂ kg −1 at 70.2 wt.% silica, highlighting its promise as a sustainable insulation solution for green buildings.
Real time nondestructive evaluation is required for composites load testing. The early detection and measurement of damage progression is important to understand failure modes. A single stringer panel was subjected to quasi-static loading to induce deformation which can result in the formation of delamination damage between the stiffener flange and skin. Passive thermography was used to detect damage in real time as a function of the applied load. The loading was stopped when damage growth was detected. Of particular interest was the early detection of damage formation which can be challenging, as compared to cyclic fatigue loading. Passive thermography data were acquired and processed in real time and revealed damaged areas due to heating from fiber breakage and delamination formation. The processed thermal imagery was also compared to acoustic emission and ultrasound data.
We report on the degradation and recovery of surface passivation of fired poly-Si/SiOx passivating contacts with hydrogen containing Al2O3 during annealing in the dark and under illumination. Upon firing to a peak temperature of 670 degrees C, the iVoc for symmetric test structures with n+, p+, and intrinsic poly-Si/SiOx contacts decreases due to a loss of surface passivation. Upon further annealing over the temperature range of 200-350 degrees C in the dark, depending on the type of doping, the surface passivation either shows further degradation followed by recovery, or direct recovery to the initial iVoc. Annealing at higher temperatures and/or higher illumination intensities accelerates the kinetics for both degradation and recovery processes. We show that the degradation and recovery processes are thermally activated and proceed identically in subsequent firing and annealing steps showing their cyclic nature. We present a series reaction model to explain the kinetics of degradation and recovery processes for n+ and intrinsic poly-Si/SiOx contacts. By fitting the model's rate expressions to the data, the determined effective activation energy barriers for degradation and recovery for n+ poly-Si/SiOx contacts in the dark are 1.24 and 1.51 eV, which are lowered under 7.5 Suns illumination to 0.76 and 1.15 eV, respectively.