The measurement of rock deformability in bore holes on earth. Adaptability to a lunar exploration program
Dilatometers, bore hole jacks, and penetrometers, for measurement of rock deformability in bore holes on earth
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Dilatometers, bore hole jacks, and penetrometers, for measurement of rock deformability in bore holes on earth
The implementation of distributed strain measurement methods in triaxial and uniaxial tests have demonstrated the development of strain localization, even at early stages. This implies that single point measurement methods are location dependent. The use of distributed methods is required not only to improve the interpreted constitutive parameters obtained from triaxial tests, but also to understand the implications of strain localization in the failure process. Here, this work uses optical fibers in triaxial tests. The developed distributed measurement method was implemented on granite, gabbro, and sandstone samples and tested under different confining pressures, reaching 200 MPa on the granite sample. Using a temporal resolution of 0.25 Hz and 5 mm of spatial resolution, the strain evolution at over 300 locations at the sample surface was measured during testing. When compared to point sensing methods, the use of optical fiber greatly increases the number of measurements at the surface of the sample, and their interpolation provides the entire deformation of the sample surface. In all the tests performed, strain localizations were revealed before failure. A three-dimensional interpretation of a test, combining an optical scan of the sample and the distributed measurements, show good correlation between the fractures and the strain localization.
Carbonate samples from the 8.9-Mt nuclear (near-surface explosion) crater, OAK, and a terrestrial impact crater, Meteor Crater, were analyzed for shock damage using electron paramagnetic resonance (EPR). Samples from below the OAK apparent crater floor were obtained from six boreholes, as well as ejecta recovered from the crater floor. The degree of shock damage in the carbonate material was assessed by comparing the sample spectra to the spectra of Solenhofen and Kaibab limestone, which had been skocked to known pressures. Analysis of the OAK Crater borehole samples has identified a thin zone of allocthonous highly shocked (10-13 GPa) carbonate material underneath the apparent crater floor. This approx. 5- to 15-m-thick zone occurs at a maximum depth of approx. 125 m below current seafloor at the borehole, sited at the initial position of the OAK explosive, and decreases in depth towards the apparent crater edge. Because this zone of allocthonous shocked rock delineates deformed rock below, and a breccia of mobilized sand and collapse debris above, it appears to outline the transient crater. The transient crater volume inferred in this way is found to by 3.2 +/- 0.2 times 10(exp 6)cu m, which is in good agreement with a volume of 5.3 times 10(exp 6)cu m inferred from gravity scaling of laboratory experiments. A layer of highly shocked material is also found near the surface outside the crater. The latter material could represent a fallout ejecta layer. The ejecta boulders recovered from the present crater floor experienced a range of shock pressures from approx. 0 to 15 GPa with the more heavily shocked samples all occurring between radii of 360 and approx. 600 m. Moreover, the fossil content, lithology and Sr isotopic composition all demonstrate that the initial position of the bulk of the heavily shocked rock ejecta sampled was originally near surface rock at initial depths in the 32 to 45-m depth (below sea level) range. The EPR technique is also sensitive to prehistoric shock damage. This is demonstrated by our study of shocked Kaibab limestone from the 49,000-year-old Meteor (Barringer) Crater Arizona.
Deformation localization is a widely observed, but rarely quantified process in the crust. Recent observations suggest that the localization of seismicity and fracture networks can help identify the approach to catastrophic failure. Here, we quantify the localization processes of the volumetric and deviatoric strain components in twelve triaxial compression experiments imaged with X-ray tomography. We capture three-dimensional images of the rock cores during triaxial compressing toward failure, and then calculate the local strain components using digital volume correlation. The divergence and curl of the incremental displacement vector field provide the volumetric and deviatoric components of the strain field. We quantify localization using the proportion of the rock occupied by high magnitudes of the volumetric and deviatoric strains, and the Gini coefficient of these high magnitude strains, which measures the deviation from a uniform process. We find that the vast majority, but not all, of the experiments experience strain localization toward failure. The rocks typically experience their maximum degree of strain localization not immediately preceding failure, but on average at 90% of the failure stress. The volumetric strain tends to localize more than the deviatoric strain. Finally, these observations support using the localization of the volumetric strain, along with the deviatoric strain, to identify the evolution of the precursory phase preceding earthquakes.
Forecasting the timing of catastrophic failure, such as crustal earthquakes, has been a central concern for centuries. Such forecasting requires identifying signals that evolve or accelerate in the precursory phase leading to failure, and the subset of signals that may be detected in the crust. We develop machine learning models to predict the proximity of catastrophic failure in synchrotron X-ray tomography triaxial compression experiments on rocks using characteristics of evolving fracture networks. We then examine the characteristics that most strongly influence the model results, and thus may be considered the best predictors of the proximity of macroscopic failure. Finally, the resulting suite of predictive parameters underscores the importance of dilation in the precursory phase leading to catastrophic failure. The results indicate that the evolution of the strain energy density field may provide more robust predictions of the proximity of failure than other existing metrics of rock deformation.
Core formation is an important event in the evolution of a planetary body, affecting both the geochemical and geophysical properties of the body. Metal-silicate segregation could have proceeded either by settling of liquid metal through a magma ocean or by percolation of liquid metal through a solid silicate mantle. Percolation of metallic melt had previously been excluded as a viable segregation mechanism because metallic melts do not form an interconnected network under hydrostatic conditions, except at high melt fraction (>5 vol%), due to the high dihedral angle between metals and silicates (>60 ). Without an interconnected network, porous flow of metallic melt is impossible, leaving the magma ocean scenario as the only mechanism to form the core. Moment-of-inertia measurements of Europa and Ganymede from the Galileo probe indicate that they are differentiated. This evidence suggests that a method for segregating metals and silicates at temperatures low enough to retain volatile compounds must exist. We have investigated the effect of deformation on the distribution of metallic melts in silicates. We have deformed samples of olivine + 5-9 vol% Fe-S to strains of 2.5 in simple shear and find that the metallic melt segregates into melt-rich planes oriented at 20 to the shear plane. These metallic melt-rich bands are similar in structure to the silicate melt-rich bands reported by Holtzman, indicating that deformation can interconnect isolated metallic melt pockets and allow porous flow of non-wetting melts. Such a core formation process could have occurred in the jovian satellites.
Reexamination of Upheaval Dome in the Canyonlands National Park, Utah, shows that the structure of this remarkable feature conforms with that expected for a deeply eroded astrobleme. The structure is definitely not compatible with an origin due simply to plastic flowage of salt and other rocks in the underlying Paradox Formation. The most strongly deformed rocks are bounded by a series of circumferential listric faults. The convergent displacement of the rocks corresponds to the deformation that results from collapse of a transient cavity produced by high speed impact. From considerations of the probable depth of exposure of the impact structure and upward extrapolation of the listric faults, the final collapsed crater is estimated to be about 8 to 10 km in diameter; the impacting body was on the order of 0.5 km in diameter.
This grant supported travel and conference fees for participants in the 2022 Gordon Research Conference (GRC) and Gordon Research Seminar (GRS) on Rock Deformation. The theme of the conference was “Combining Laboratory Measurements with Observational Constraints to Understand Tectonic Processes”, which focused on how to scale up observations from laboratory experiments to tectonic processes. Dan Faulkner (Univ. of Liverpool) was the GRC chair and Heather Savage (UC Santa Cruz) was the vice chair. The GRS was run by Carolyn Tewksbury-Christle and Taka Kanaya. The majority of the funds from this grant supported early career researchers.
Resistivity changes, ground potentials, electromagnetic (EM) and luminous signals prior to or during earthquakes have been reported, in addition to ground uplift and tilt, and to changes in the seismic wave propagation parameters. However, no physical model exists that ties these diverse phenomena together. Through time-resolved impacts experiments it has been observed that, when igneous rocks (gabbro, diorite, granite) are impacted at low velocities (approx. 100 m/sec), highly mobile electronic charge carriers are generated, spreading from a small volume near the impact point, causing electric potentials, EM and light emission. The rock becomes momentarily conductive. When impacted at higher velocities (approx. 1.5 km/sec), the propagation of the P and S waves is registered through the transient piezoelectric response of quartz. At the same time, the rock volume is filled with mobile charge carriers, and a positive surface potential is registered. During the next 1-2 msec the surface potential oscillates, due to electron injection from ground. These observations are consistent with positive holes, e.g. defect electrons in the O(2-) sublattice, that can travel via the O 2p-dominated valence band of the silicate minerals at the speed of a phonon-mediated charge transfer. Before activation, the positive hole charge carriers lay dormant in form of positive hole pairs, PHP, electrically inactive, chemically equivalent to peroxy links in the structures of constituent minerals. PHPs are introduced by way of hydroxyl (O3Si-OH) incorporated into nominally anhydrous minerals when they crystallize in water-laden environments. Given that sound waves of even relatively low intensity appear to cause PHPs dissociation, thus generating mobile positive holes, it is proposed that microfracturing during rock deformation cause PHP dissociation. Depending on where and how much the rock volume is stressed, the positive holes are expected to form fluctuating charge clouds in the earthquake source region that may account for earthquake-related electrical phenomena and the reported low frequency EM signals.
Structural petrology of fluid inclusions in deformed rocks can be used to identify inclusions entrapped during various stages of deformation. Standard thermobarometry on these inclusions can then provide estimates of the P-T (pressure-temperature) conditions of deformation. The application of this technique is illustrated using fluid inclusions in mylonites from the Quetico Fault Zone, Canada. The inferred P-T conditions fall with the P-T field of mylonitisation derived from isotopic, microstructural and phase equilibrium studies.
The existence of a deep borehole in the Earth’s crust disturbs the local stresses and creates a stress concentration that may result in breakout and damage to the borehole. Maintaining wellbore integrity mitigates environmental impacts such as groundwater contamination, gas leakage to the atmosphere, and fluid spills and seepage at the surface. In this paper, the stability of deep boreholes (5 km) is examined by laboratory experiments and numerical models in the context of nuclear waste disposal in Israel. Two rock types in southern Israel are considered: the crystalline basement (granite) and the Zenifim Formation (arkose). A series of room-temperature triaxial rock deformation experiments were conducted at different confining pressures. This mechanical characterization was then used to parameterize the elastic properties and damage behavior of the rocks. This facilitated modeling the stability of the deep boreholes by two different formulations of damage rheology: a dynamic-oriented formulation used to model deformation immediately after the creation of the open hole and a quasi-static formulation used to model longer stress corrosion regime. The calibrated modeling results indicate greater stability with Zenifim arkose than the crystalline granite for deep borehole conditions despite the granite having a greater triaxial compressive strength. Dissipation associated with dilation and porous compaction in the arkose during deformation plays a significant stabilizing role in the borehole compared to crystalline rocks. These results suggest that common strength-based borehole stability assessment may lead to inaccurate predictions. Three-dimensional modeling of bottom-hole stress conditions and the effects of transient borehole geometry show conventional two-dimensional analysis may not be conservative when predicting borehole damage.
Time-dependent rock deformation caused by the initiation and growth of fractures leads to the weakening of the rock mass. Understanding the fracturing mechanisms involved in the time-dependent behavior in brittle rocks is very important and to achieve this goal, a systematic series of three types of experiments was performed on double-flawed prismatic Barre granite specimens under unconfined compression. The first series aimed to identify the failure mechanism in the short-term failure mode under monotonic loading, the, second series involved multistage relaxation (constant strain) experiments to analyze the damage at different strain levels, and the third series explored the fracture propagation under multistage creep (constant load) experiments. The spatial and temporal evolution of cracking mechanisms were evaluated using the acoustic emission (AE) and two-dimensional digital image correlation (2D-DIC) techniques to observe the whole crack growth process as well as the accumulated inelastic strain at the specified region of interest. Results suggest that in the case of multistage creep experiments, the time to failure was less compared to the multistage relaxation, when loaded above the crack damage threshold (CD) estimated from the monotonic testing. Furthermore, the frequency magnitude distribution of the AE events generated in the three loading conditions followed the Gutenberg Richter model. A relatively lower b-value was obtained for the creep experiments, indicative of high energy AE events and faster crack growth. In addition, the AE and DIC results also revealed high evolution of tensile cracks at-different stages of creep and relaxation compared to shear and mixed-mode cracks.
The Tuscaloosa Marine Shale (TMS) in Louisiana and Mississippi is an Upper Cretaceous source rock formation sandwiched between the sands of the upper and lower Tuscaloosa sections. The TMS is believed to be the source rock for underlying prolific Tuscaloosa sand formation. The TMS has an unproven estimate of 7,000,000,000 bbls of recoverable oil while its current total average production is about 3,000 bbls of oil per day in 2017. In 2013 and 2014, more than 80 wells were drilled horizontally into the TMS that were fractured using multi-stage fracturing technology. The results from this have been mixed, but recent production for several wells show an appealing initial oil production rate of more than 1000 bbl/day. The preliminary core analysis by industry partners and a few literature studies shows that the TMS is one of the most clay-rich and sensitive shales to water. Due to these and other technical problems, there is high risk for the economic development of TMS compared to other shale plays. The experiences of major industrial players in the TMS show the necessity of open and collaborative efforts to better understand the critical gaps in the development of this challenging and potentially highly economic shale play to enable more cost-efficient and environmentally-sound recovery from this unconventional liquid-rich shale play. The overall objective of this project is to form a consortium of science and industry partners to address the following six major objectives using scientific and technical approaches: 1. To improve wellbore integrity by better understanding the sources of the wellbore instability issues, proposing innovative mud and cement design for the TMS. 2. To improve formation evaluation using laboratory techniques for the evaluation of mineralogical composition, organic content, and produced-water chemistry as well as well log and geophysical analysis. 3. To determine the role of geologic discontinuities on fracture growth and shale creep behavior using digital image correlation technique. 4. To investigate the application of stable CO 2 foam and super-hydrophobic proppants for improved reservoir stimulation. 5. To better understand the nature of water/hydrocarbon/CO 2 flow in clay and organic-rich formation and the role of water/fluid interaction on recovery. 6. To prepare better socio-economic environment for TMS development by community engagement. Subsequently, the TMS virtual laboratory conducted testing and analysis of various properties of rock and formation fluids from the TMS, including but not limited to the following: Analyzing reports and logs to better understand the source of wellbore instability in TMS wells; Experiments to design a customized cement based on TMS requirements; Experiments to obtain the mineralogical and geochemical composition of TMS samples; Seismic analysis of TMS geophysical data to better predict total organic carbon (TOC) content and brittleness in TMS; Well log analysis to better estimate the TOC and geo-mechanical properties of TMS; Experiments on formation water to understand the chemistry of produced water; Experiments to determine the role of lamination and natural fractures on fracture propagation or rock deformation using digital image correlation technique in in-direct tensile tests, semi-circular bend test and creep tests Experiments to determine the stability and rheological properties of nanoparticle-stabilized CO 2 foam in TMS rock samples; Experiments to determine fluid dynamics in un-propped TMS fractures and the role of nano-coating of proppants on fluid dynamics in fractures with proppants; Micro-fluidics experiments to enhance the understanding of fluid dynamics in tight liquidrich pores with high clay content; Socio-economic studies to better engage communities in TMS development.
It is challenging to quantitatively predict shearing of intersecting fractures/faults because of dynamic frictional contacts accompanied by possible nonlinear rock deformation. To address such challenges, a new conceptual model—the simplified DFN model—was proposed and validated by Hu et al. 46 to use major paths (MPs) to represent complicated DFNs for calculation of shearing. In this work, we conducted a benchmark study for three examples that involve different levels of complexity of intersecting fractures, and correspondingly different numbers of MPs. The codes and software that were used in the benchmark cover a range of continuum, discontinuum and hybrid numerical methods: NMM (LBNL), FLAC3D (LBNL), GBDEM (KIGAM), FRACOD (DynaFrax), and CASRock (CAS). The general consistency between DFN and MP cases as predicted by all the codes/software demonstrates that major paths can be used to simplify the geometry of DFNs in a wide range of software. Disagreement in results made by some software and potential future improvements are discussed. We show that (1) shearing of one or multiple major fractures can be reduced if there are multiple smaller intersecting fractures in that area, which is a useful basis for understanding and controlling induced seismicity and merits further analysis, and (2) the agreement achieved in the benchmark examples provide confidence that the simplified DFN model is a promising conceptual model that can be used for different types of numerical approaches and software for simplifying the analysis of the shearing of intersecting fractures and faults.
SUMMARY As the high-frequency analogue to field-scale earthquakes, acoustic emissions (AEs) provide a valuable complement to study rock deformation mechanisms. During the load-stepping creep experiments with CO2-saturated water injection into a basaltic sample from Carbfix site in Iceland, 8791 AE events are detected by at least one of the seven piezoelectric sensors. Here, we apply a cross-correlation-based source imaging method, called geometric-mean reverse-time migration (GmRTM) to locate those AE events. Besides the attractive picking-free feature shared with other waveform-based methods (e.g. time-reversal imaging), GmRTM is advantageous in generating high-resolution source images with reduced imaging artefacts, especially for experiments with relatively sparse receivers. In general, the imaged AE locations are found to be scattered across the sample, suggesting a complicated fracture network rather than a well-defined major shear fracture plane, in agreement with X-ray computed tomography imaging results after retrieval of samples from the deformation apparatus. Clustering the events in space and time using the nearest-neighbour approach revealed a group of ‘repeaters’, which are spatially co-located over an elongated period of time and likely indicate crack, or shear band growth. Furthermore, we select 2196 AE events with high signal-to-noise-ratio (SNR) and conduct moment tensor estimation using the adjoint (backpropagated) strain tensor fields at the locations of AE sources. The resulting AE locations and focal mechanisms support our previously assertion that creep of basalt at the experimental conditions is accommodated dominantly by distributed microcracking.
This dataset contains results from nine triaxial direct shear tests conducted by Los Alamos National Laboratory on samples from FORGE Well 16A(78)-32. The primary objectives of this work were to determine the shear strength in both intact and residual states, evaluate dilation against displacement, assess permeability in relation to displacement, time, and normal stress, understand the relationship between aperture and normal stress, and monitor the effluent chemistry as a function of time. The data includes time-series measurements of stress, displacement, permeability, and effluent chemistry, with and without experimental dilution corrections. Additional materials include profilometry data, photographic documentation of the experimental setups and apparatus, and test notes. The dataset is organized into folders corresponding to each test, containing hydromechanical data, effluent chemistry measurements, and images. The hydromechanical data consists of detailed time-series records capturing parameters such as shear force, confining pressure, permeability, and temperature. Effluent chemistry data tracks fluid composition changes over time. Also included are conference papers, presentation slides, and a summary document outlining the experiments.
Greater utilization of subsurface reservoirs perturbs in-situ chemical-mechanical conditions with wide ranging consequences from decreased performance to project failure. Understanding the chemical precursors to rock deformation is critical to reducing the risks of these activities. To address this need, we investigated the coupled flow-dissolution- precipitation-adsorption reactions involving calcite and environmentally-relevant solid phases. Experimentally, we quantified (1) stable isotope fractionation processes for strontium during calcite nucleation and growth, and during reactive fluid flow; (2) consolidation behavior of calcite assemblages in the common brines. Numerically, we quantified water weakening of calcite using molecular dynamics simulations; and quantified the impact of calcite dissolution rate on macroscopic fracturing using finite element models. With microfluidic experiments and modeling, we show the effect of local flow fields on the dissolution kinetics of calcite. Taken together across a wide range of scales and methods, our studies allow us to separate the effects of reaction, flow, and transport, on calcite fracturing and the evolution of strontium isotopic signatures in the reactive fluids.
Oil and gas recovery increasingly relies on stimulation and production strategies that involve complex interactions between rock deformation, fractures, and fluid flow underground. Conventional modeling approaches often simplify or separate these effects, which can limit their ability to accurately predict performance in fractured or geologically complex reservoirs.