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At least 19 records

Dating fractures using luminescence

Rock fracturing (cracking) is a universal process that drives and limits chemical degradation, sediment production and erosion, and deterioration of infrastructure. Despite extensive research gains in rock mechanics on one hand and geochronology on the other, there remains a glaring gap in our ability to understand the long term evolution of natural, in situ fractures. Here we develop a novel fracture exposure dating technique, grounded in modern advances in luminescence geochronology. We apply our new dating method to a granitic boulder from a glacial outwash terrace in California, US. We conclude that the longest, clast-splitting E-W fracture appeared shortly after the boulder's deposit, whereas the secondary N-S fracture appeared 5 ka after the deposition, approximately correlating with the Last Glacial Maximum and Younger Dryas periods of the region, respectively. However, dating of the third fracture (<< 50 µm width) which does not fully split the rock, is ambiguous due to negligible daylight penetration and poor determination of fracture width. The fracture dating method presented herein brings with it the potential to decipher relationships that are crucial for the interpretation and modeling of, for example, long-term landscape and atmospheric evolution relating rock weathering to climate change and erosion.

58 GEOSCIENCES↗

Continued Development of in Situ Geochronology for Planetary Missions

The instrument 'Potassium (K) Argon Laser Experiment' (KArLE) is developed and designed for in situ absolute dating of rocks on planetary surfaces. It is based on the K-Ar dating method and uses the Laser Induced Breakdown Spectroscopy - Laser Ablation - Quadrupole Mass Spectrometry (LIBSLA- QMS) technique. We use a dedicated interface to combine two instruments similar to SAM of Mars Science Laboratory (for the QMS) and ChemCam (for the LA and LIBS). The prototype has demonstrated that KArLE is a suitable and promising instrument for in situ absolute dating.

geochronology↗

In situ Be-10-Al-26 exposure ages at Meteor Crater, Arizona

A new method of dating the surface exposure of rocks from in situ production of Be-10 and Al-26 has been applied to determine the age of Meteor Crater, Arizona. A lower bound on the crater age of 49,200 + or - 1,700 years has been obtained by this method.

Nishiizumi, K.↗

Lunar regolith dynamics based on analysis of the cosmogenic radionuclides Na-22, Al-26, and Mn-53

Depth profiles of Na-22 and Al-26 in the upper portions of five lunar cores are analyzed. From the analyses, it is concluded that the natural gardening processes on the lunar surface result in mixing of the regolith to a depth of 2-3 cm over a time period which is short compared with the half-life of Al-26 (0.73 m.y.). It is also concluded that the rotary drill processes which were used to obtain the deep drill samples generally resulted in loss and/or mixing of the upper portions of the cores. In contrast, the near-surface regions of the drive tube cores appear to have a well-preserved stratigraphy. Analysis of Mn-53 in samples of six lunar rocks helps substantiate the accuracy of age date estimates by other means, and provides definite information that the total lunar surface exposure of two of these rocks has occurred during a single surface event which continued to their collection.

Fruchter, J. S.↗

Lunar surface dynamics: Some general conclusions and new results from Apollo 16 and 17

Exposure ages of Apollo 17 rocks as measured by tracks and the Kr-Kr rare gas method are reported. Concordant ages of 22 - or + 1 million year (my) are obtained for the station 6 boulder sample 76315. This value is interpreted as the time when the station 6 boulder was emplaced in its present position. Reasonable agreement is also obtained by the two methods for another station 6 boulder, sample 76015. Discordant ages (respectively 5 and 28 my by the track and rare gas methods) are obtained for the station 7 boulder sample, 77135, indicating that the boulder was emplaced at least 5 my ago. The 72 my exposure age of 75035, in general agreement with previous measurements of approximately 85 my for another Camelot boulder, may well date the formation of Camelot. Rock 76015 was split and one surface exposed to the sky through a very small solid angle.

Crozaz, G.↗

Absolute ages from crater statistics: Using radiometric ages of Martian samples for determining the Martian cratering chronology

In the absence of dates derived from rock samples, impact crater frequencies are commonly used to date Martian surface units. All models for absolute dating rely on the lunar cratering chronology and on the validity of its extrapolation to Martian conditions. Starting from somewhat different lunar chronologies, rather different Martian cratering chronologies are found in the literature. Currently favored models are compared. The differences at old ages are significant, the differences at younger ages are considerable and give absolute ages for the same crater frequencies as different as a factor of 3. The total uncertainty could be much higher, though, since the ratio of lunar to Martian cratering rate which is of basic importance in the models is believed to be known no better than within a factor of 2. Thus, it is of crucial importance for understanding the the evolution of Mars and determining the sequence of events to establish an unambiguous Martian cratering chronology from crater statistics in combination with clean radiometric ages of returned Martian samples. For the dating goal, rocks should be as pristine as possible from a geologically simple area with a one-stage emplacement history of the local formation. A minimum of at least one highland site for old ages, two intermediate-aged sites, and one very young site is needed.

Neukum, G.↗

Investigations of lunar materials

In the particle track work, a series of dating techniques for learning about the surface history of soil and rock samples was developed. The surface behavior and history of diverse lunar rocks and soils, erosion rates, and deposition rates were studied, along with incident heavy cosmic ray spectrum.

Fleischer, R. L.↗

Lunar surface processes and cosmic ray histories over the past several million years

Measurements of the Al-26 and Mn-53 in interior portions of lunar rocks have shown that lunar surface processes which move a significant fraction of kilogram size rocks on the lunar surface occur on time scales of a few million years. These measurements, together with noble gas age dating have made it possible to define the history for nine rock samples selected from whole rock counting data because of anomalously low Al-26 relative to Na-22. Six of the rocks from the Apollo 15 and 16 missions showed evidence of movement during the past five million years. Of these six, only two are of an age consistent with their origin from the South Ray Crater Event. In addition, our measurements of Na-22 and Al-26 in Apollo 17 double drive tube 74001-74002 suggest that one to two cm of soil is missing from the top of this core tube. Even with this loss, at least two cm of gardening is indicated in the top portion of 74002.

Fruchter, J. S.↗

WEATHERING ON VENUS: CONSTRAINTS FROM MODEL AND EXPERIMENTAL RESULTS

The surface of Venus is in contact with a hot (~470° C), high pressure (92 bars), and caustic (CO2 with S) atmosphere, which should cause progressive alteration of the crust [1, 2]. Alteration should form rock coatings of iron-oxides and sulfates, since water is not stable on the surface to make clay minerals [1, 3]. These coatings could, in theory, be used as a way to age date different lava flows, since the amount of alteration should correlate with the age of the rock exposed to the atmosphere [4, 5]. However, the exact alteration mineralogy and rate are still not well constrained [5]. Further, how the alteration mineralogy affects orbital emissivity measurements of the Venus surface is similarly not well understood [6]. Here we review the recent geochemical modeling [1, 7] and experimental [8-15] studies to constrain the main alteration minerals, potential alteration rates, and open questions about the surface mineralogy of Venus.

J. Filiberto↗

Argon-isotopic Age Dating Analyses for Eastern Snake River Plain Volcanic Rock Samples

Argon-isotopic age dating analyses were conducted on 25 volcanic rock samples obtained from 22 boreholes and collected at three surface locations in the Eastern Snake River Plain (ESRP). The analyses were conducted to reduce uncertainties for characterizing volcanic hazards at Idaho National Laboratory (INL) as part of the Senior Seismic Hazard Analysis Committee (SSHAC) Level 3 Probabilistic Volcanic Hazards Assessment (PVHA). Results of the argon-isotopic age dating analyses will be used to estimate the recurrence of basaltic and silicic volcanism and for assessing the spatial and temporal distributions of volcanic events in the ESRP.

58 - GEOSCIENCES↗

Technical note: Optimizing the in situ cosmogenic 36 Cl extraction and measurement workflow for geologic applications

Abstract. In situ cosmogenic 36Cl analysis by accelerator mass spectrometry (AMS) is routinely employed to date Quaternary surfaces and assess rates of landscape evolution. However, standard laboratory preparation procedures for 36Cl dating require the addition of large amounts of isotopically enriched chlorine spike solution; these solutions are expensive and increasingly difficult to acquire from commercial sources. In addition, the typical workflow for 36Cl dating involves measuring both 35Cl/37Cl and 36Cl/Cl concurrently on the high-energy (post-accelerator) end of the AMS system, but 35Cl/37Cl determinations using this technique can be complicated by isotope fractionation and system memory during measurement. The traditional workflow also does not provide 36Cl extraction laboratories with the data needed to calculate native Cl concentrations in advance of 36Cl/Cl measurements. In light of these concerns, we present an improved workflow for extracting and measuring chlorine in geologic materials. Our initial step is to characterize 35Cl/37Cl on sample aliquots of up to ∼1 g prepared in Ag(Cl, Br) matrices, which greatly reduces the amount of isotopically enriched spike solution required to measure native Cl content in each sample. To avoid potential issues with isotope fractionation through the accelerator, 35Cl/37Cl is measured on the low-energy, pre-accelerator end of the AMS line. Then, for 36Cl/Cl measurements, we extract Cl as AgCl or Ag(Cl, Br) in analytical batches with a consistent total Cl load across all samples; this step is intended to minimize source memory effects during 36Cl/Cl measurements and allows the preparation of AMS standards that are customized to match known Cl contents in the samples. To assess the efficacy of this extraction and measurement workflow, we compare chlorine isotope ratio measurements on seven geologic samples prepared using standard procedures and the updated workflow. Measurements of 35Cl/37Cl and 36Cl/Cl are consistent between the two workflows, and 35Cl/37Cl values measured using our methods have considerably higher precision than those measured following standard protocols. The chemical preparation and measurement workflow presented here (1) reduces the amount of isotopically enriched chlorine spike used per rock sample by up to 95 %; (2) identifies rocks with high native Cl concentrations, which may be lower priority for 36Cl surface exposure dating, at an early stage of analysis; and (3) allows laboratory users to maintain control over the total chlorine content within and across analytical batches. These methods can be incorporated into existing laboratory and AMS protocols for 36Cl analyses and will increase the accessibility of 36Cl dating for geologic applications.

58 GEOSCIENCES↗

NASA Tech Briefs, March 2012

The topics include: 1) Spectral Profiler Probe for In Situ Snow Grain Size and Composition Stratigraphy; 2) Portable Fourier Transform Spectroscopy for Analysis of Surface Contamination and Quality Control; 3) In Situ Geochemical Analysis and Age Dating of Rocks Using Laser Ablation-Miniature Mass Spectrometer; 4) Physics Mining of Multi-Source Data Sets; 5) Photogrammetry Tool for Forensic Analysis; 6) Connect Global Positioning System RF Module; 7) Simple Cell Balance Circuit; 8) Miniature EVA Software Defined Radio; 9) Remotely Accessible Testbed for Software Defined Radio Development; 10) System-of-Systems Technology-Portfolio-Analysis Tool; 11) VESGEN Software for Mapping and Quantification of Vascular Regulators; 12) Constructing a Database From Multiple 2D Images for Camera Pose Estimation and Robot Localization; 13) Adaption of G-TAG Software for Validating Touch and Go Asteroid Sample Return Design Methodology; 14) 3D Visualization for Phoenix Mars Lander Science Operations; 15) RxGen General Optical Model Prescription Generator; 16) Carbon Nanotube Bonding Strength Enhancement Using Metal Wicking Process; 17) Multi-Layer Far-Infrared Component Technology; 18) Germanium Lift-Off Masks for Thin Metal Film Patterning; 19) Sealing Materials for Use in Vacuum at High Temperatures; 20) Radiation Shielding System Using a Composite of Carbon Nanotubes Loaded With Electropolymers; 21) Nano Sponges for Drug Delivery and Medicinal Applications; 22) Molecular Technique to Understand Deep Microbial Diversity; 23) Methods and Compositions Based on Culturing Microorganisms in Low Sedimental Fluid Shear Conditions; 24) Secure Peer-to-Peer Networks for Scientific Information Sharing; 25) Multiplexer/Demultiplexer Loading Tool (MDMLT); 26) High-Rate Data-Capture for an Airborne Lidar System; 27) Wavefront Sensing Analysis of Grazing Incidence Optical Systems; 28) Foam-on-Tile Damage Model; 29) Instrument Package Manipulation Through the Generation and Use of an Attenuated-Fluent Gas Fold; 30) Multicolor Detectors for Ultrasensitive Long-Wave Imaging Cameras; 31) Lunar Reconnaissance Orbiter (LRO) Command and Data Handling Flight Electronics Subsystem; and 32) Electro-Optic Segment-Segment Sensors for Radio and Optical Telescopes.

Source record↗

Martian Chronology and Atmospheric Composition: In Situ Measurements versus Sample Return

I examine two significant issues of martian science from the point of view of in situ measurements by robotic spacecraft versus sample return and analysis in terrestrial labs. (1) To define martian history, ages of geological processes and surface features are required. Estimated ages from surface crater densities have limitations, and the ages measured for martian meteorites cannot be associated with specific martian locales. Whereas returned martian rocks could be accurately dated, some have suggested sending a robotic spacecraft to Mars to measure rock ages using the classical K- Ar-40 technique, considered the easiest to implement. (2) To understand the evolution of the martian atmosphere and its interactions with the surface, requires precise measurements of atmospheric composition. A significant amount of information has derived from measurements by Viking and of martian meteorites. Instrumentation on the Mars Science Lander (MSL) spacecraft to be launched in the near future promises to determine atmospheric composition even more precisely. If MSL is successful, which questions about atmospheric composition will remain and thus will require atmospheric sample return to answer?

Bogard, Donald D.↗

Crater Retention Observations of the Crater Floor–Fractured Rough Unit in Jezero Crater

A main goal of the Mars2020 Perseverance Rover mission is to provide a compelling suite of samples for eventual return to Earth [1]. A high priority goal for Mars Sample Return is calibrating Mars’ crater retention isochrons that are used to date geologic surfaces and events across the planet [2]. Several factors are necessary to consider what type of rock would be most useful for this purpose: ability to retain craters across a large exposure, access to drillable outcrop, identifiable stratigraphic context, and understanding why this specific rock type preferentially retains crater morphology. Now that we’ve seen the surface and sampled some of the main constituent outcrops on the Crater Floor – Fractured Rough unit [3, Simon et al, this conference] (Figure 1), we can begin assessing which rocks can help us achieve this important goal to not only understand the age relationships between stratigraphic units in Jezero crater, but also improve age estimates across Mars.

Mars 2020↗

Testing Mars 2020 Flight Software and Hardware in the Surface System Development Environment

The Mars 2020 (M2020) Perseverance Rover is NASA's most advanced planetary rover mission to date. It includes a novel Sample Caching Subsystem (SCS) which will collect rock cores for possible future return to Earth, as well as an improved mobility system with enhanced autonomous navigation which will enable it to traverse faster and farther than prior rovers. The development of both systems required extensive flight software and flight hardware testing. To support this testing, we developed the Surface System Development Environment (SSDEV) and used it for a wide variety of testing. SSDEV is a bundled subset of M2020 Flight Software which runs on commercially available Linux computers and can be combined with multiple backend options for simulation and hardware control. The SSDEV architecture enabled our teams to perform much more testing of flight software and flight hardware than would have otherwise been possible. As a secondary benefit, the SSDEV-based test campaigns also helped our teams enter the operations phase of the mission with greater readiness of operations products and tools. In this paper, we summarize the motivation for SSDEV, provide an overview of the SSDEV architecture, list several examples of how SSDEV was used, and summarize lessons learned. SSDEV is not a substitute for integrated testing with flight-like avionics, but it enabled substantially more testing than would have otherwise been possible and also provided some unique benefits. We recommend architectures like SSDEV to future projects that need to perform extensive hardware and software testing using a limited set of flight-like avionics.

Wai, Dennis↗

Apollo Sample 64455: Petrologic and Geochemical Characterization of a Glass-Coated Impact Melt Rock

Introduction and Background: Impact melts are a key product of the impact cratering process. Impact melts can turbulently entrain pre-existing rock fragments, and melt part of those entrained materials until thermal equilibrium is achieved [1–3]. Lunar impact melt rocks are valuable for determining the precise ages of basin-forming and cratering events, which anchor the cratering chronology and dynamics of the entire solar system [4, and references therein]. Additionally, entrained clasts can inform on the petrology and age of crustal materials that predate the melt-forming impact. In lithologies where no pristine samples are available, entrained materials may hold the record of endogenous lunar volatiles, provided we can untangle their impact histories as high temperature impact melt can heat the clasts and may alter their native volatiles or isotopic signatures [5–6]. Here, we characterize an Apollo 16 sample, 64455,70B, in an effort to understand the physical, microstructural, and geochemical consequences of impact melt contact metamorphism. We acquired optical light and x-ray maps of the sample, as well as quantitative analyses via electron probe microanalysis (EPMA). These tasks allow us to better understand the interaction between impact melts and entrained clasts, ultimately closing knowledge gaps in high-temperature impact processing on planetary surfaces. Sample Description: Sample 64455 is an oblong crystalline rock encased in glass to form an egg-like shape [7–8]. The impact melt coating has altered the outer (1 to 2 mm) rind of the crystalline rock and has preserved schlieren. The interior crystalline rock is likely a crystalline impact melt rock based on its bulk Ir content of 2.25 parts per billion [9]. The composition of the impact melt glass rind cannot be solely derived from the crystalline interior, the glassy rind is more aluminous and less magnesian [10]. Neither the crystalline interior nor the glassy rind were radiometrically age dated, although several studies investigated its cosmogenic isotopes and exposure ages, which reveal the sample was exposed on the lunar surface for ~1–2 Ma [11–13]. Preliminary Results: The interior crystalline rock consists primarily of plagioclase with interstitial pyroxene and olivine. Plagioclase grains are zoned and compositions range from An97–89, while pyroxene compositions generally range from En68Fs19Wo13 to En82Fs15Wo3 and olivine are Fo77 to Fo85. Minor phases include Fe-Ni metal, Ca-phosphates, a K- and Si-rich phase, sulfides, and Fe-phosphides. The glass rind contains approximately 44 wt.% SiO2, 25 wt.% Al2O3, 6 wt.% FeO, 8 wt.% MgO, and 14 wt.% CaO, with other oxides at <1 wt.% each, although the composition of the glass becomes more variable closest to the crystalline rock. The rind consists of rounded plagioclase, pyroxene, and olivine crystals with interstitial melt. In some locations, the rounded crystals are surrounded by closely-packed, blade-like crystals, <5 µm in width. These results indicate that the crystalline interior has partially melted where in contact with the high-temperature impact melt and while further investigation is needed, pyroxene may have preferentially melted relative to olivine and plagioclase. Future Work: We plan to conduct electron backscatter diffraction (EBSD) mapping in order to determine crystallinity and crystal orientation. Next using transmission electron microscopy (TEM) data in conjunction with EBSD and EPMA information, we will model the diffusion of moderately volatile elements between the melt and remnant crystals.

A C Stadermann↗

Overview of the Search for Space Weathering Signals on Bennu: One Rock Type, or Two?

We report on progress in the search for signs of space weathering on Bennu. We provide an overview of the space weathering evidence to date, and summarize relevant findings from several ongoing parallel studies of surface processes and surface properties. We examine trends from these studies in the context of space weathering, and what is known about near-Earth asteroid surface maturation. Because Bennu is covered with blocks, boulders, and rocks of various sizes, our search for space weathering signals has inevitably led to a study of the properties of Bennu’s rocks. Our research question is – do Bennu’s bright and dark rock populations form a maturity continuum due to space weathering, or alternatively, do the bright and dark rocks provide compelling evidence for two distinct rock populations on Bennu? In particular, we present our best estimate of the sub-field-of-view OVIRS (OSIRIS-REx Visible and Infrared Spectrometer) spectral properties of the largest bright boulders and compare them with the darker materials on Bennu’s surface to see if the observed spectral and albedo differences are consistent with space weathering effects, or not.

Clark, B. E.↗

McLaughlin Crater as a Candidate Landing Site for Humans on Mars

McLaughlin Crater is an ancient (Noachian) Martian impact crater located at 337.6 East, 21.9 North, just south of the dichotomy boundary. This site should be considered for future landed exploration because: a) it is located at the boundary of three types of scientifically important terrain that will yield key results about the geological evolution and habitability of Mars; b) it contains surfaces where radiometric dating can be related to age dates estimated from crater counting, c) it contains volatile-rich rocks that will not only yield interesting results regarding ancient atmospheric chemistry, but will also be high quality, accessible targets for in-situ resource utilization (ISRU), and d) the site within the crater provides a flat, low-risk and low-elevation landing zone, which will facilitate landing large payloads on Mars.

Michalski, J. R.↗