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DOE OSTI2019

Data Release Report Source Physics Experiments 5 and 6 (SPE-5 and SPE-6), Nevada National Security Site

The fifth Source Physics Experiment test (SPE-5) was conducted in Nevada on April 26, 2016, at 20:49:00 Coordinated Universal Time (UTC). The explosive source was 4,288.7 kilograms (kg) of polymer-bonded explosive (PBXN) –110, equivalent to 5,035 kg of trinitrotoluene (TNT) detonated at a depth of 76.5 meters (m). The sixth Source Physics Experiment test (SPE-6) was conducted in Nevada on October 12, 2016 at 18:36:00 UTC. The explosive source was 1,982.2 kg of PBXC-141, equivalent to 2,240.2 kg of TNT detonated at the depth of 31.4 m. Both tests were recorded by an extensive set of instrumentation that includes sensors both at near-field (less than 100 m) and far-field (100 m or greater) distances. The near-field instruments consisted of three-component accelerometers installed at various depths ranging from 4 to 99 m below ground surface in boreholes positioned around the shot, and a set of single-component vertical accelerometers on the surface. The far-field network was composed of a variety of seismic and acoustic sensors, including short-period geophones, broadband seismometers, and three-component accelerometers at distances of 100 m to 400 kilometers. In addition, both explosions were recorded in a temporary array of 996 geophones arranged in a densely spaced grid pattern (“large N”). This report coincides with the release of these data for analysts and organizations that are not participants in this program. This report describes the fifth and sixth Source Physics Experiment tests and the various types of near-field and far-field data that are available.

58 GEOSCIENCES↗

DOE OSTI2018

Direct Shear and Triaxial Shear test Results on Core from Borehole U-15n and U-15n#10, NNSS in support of SPE

Direct Shear (DS) and Triaxial Shear (FCT) tests from Core holes U-15n and U-15n#10 are part of a larger material characterization effort for the Source Physics Experiment (SPE) project. This larger effort encompasses characterizing a granite body from Nevada both before and after each SPE shot. Core hole U-15n is the vertically oriented source hole for all SPE shots; pre shot core was taken from this hole for DS and FCT testing. After two SPE shots were executed, an inclined core hole (U-15n#10) was drilled; both DS and FCT tests were conducted from this core hole. The first shot (SPE-1) conducted on May 3, 2011 was a calibration shot. SPE-1 was an order of magnitude smaller than the second shot (SPE-2). After SPE-2 was conducted on October 25, 2011 the aforementioned inclined core hole (U-15n#10) was drilled. At its bottom, the inclined core hole intersects the source hole. The third shot (SPE-3) occurred on July 24, 2012. Vertical and inclined core holes were drilled post SPE-3 and specimens will soon be selected for geomechanical characterization. At the time of this writing, work is ongoing at Nevada in preparation for the fourth SPE shot (SPE-4).

36 MATERIALS SCIENCE↗

DOE OSTI2018

Unconfined Compression Results on Core from Borehole U-15n#10, NNSS, in support of SPE

The Nevada National Security Site (NNSS) serves as the geologic setting for a Source Physics Experiment (SPE) program. The SPE provides ground truth data to create and improve strong ground motion and seismic S-wave generation and propagation models. The NNSS was chosen as the test bed because it provides a variety of geologic settings ranging from relatively simple to very complex. Each series of SPE testing will comprise the setting and firing of explosive charges (source) placed in a central borehole at varying depths and recording ground motions in instrumented boreholes located in two rings around the source, positioned at different radii. Modeling using advanced simulation codes will be performed both before and after each test to predict ground response and to improve models based on acquired field data, respectively. A key component in the predictive capability and ultimate validation of the models is the full understanding of the intervening geology between the source and the instrumented boreholes including the geomechanical behavior of the site's rock/structural features. This memorandum reports on an initial phase of unconfined compression testing from corehole U-15n#10. Specimens tested came from the U-15n#10 core hole, which was drilled at -60° to the horizontal in granitic rock (quartz monzonite) after the second SPE shot (SPE-2). Figure 1 illustrates at the surface, the core hole was approximately 90 feet from the central SPE borehole. Corehole U 15n#10 intersects the central SPE borehole (U-15n) at a core depth of 170 feet (approximately 150 feet vertical depth) which is within the highly damaged zone of SPE-2. The U-15n#10 location is the site of the first, second and third SPE's, in Area 15 of the NNSS.

36 MATERIALS SCIENCE↗

DOE OSTI2018

Unconfined Compression Results on Core from Boreholes U-15n#12 and U-15n#13, NNSS in support of SPE

The Nevada National Security Site (NNSS) serves as the geologic setting for a Source Physics Experiment (SPE) program. The SPE provides ground truth data to create and improve strong ground motion and seismic S-wave generation and propagation models. The NNSS was chosen as the test bed because it provides a variety of geologic settings ranging from relatively simple to very complex. Each series of SPE testing will comprise the setting and firing of explosive charges (source) placed in a central borehole at varying depths and recording ground motions in instrumented boreholes located in two rings around the source, positioned at different radii. Modeling using advanced simulation codes will be performed both before and after each test to predict ground response and to improve models based on acquired field data, respectively. A key component in the predictive capability and ultimate validation of the models is the full understanding of the intervening geology between the source and the instrumented boreholes including the geomechanical behavior of the site's rock/structural features. This report summarizes unconfined compression testing (UCS) from coreholes U-15n#12 and U-15n#13 and compares those datasets to UCS results from coreholes U-15n and U-15n#10. U-15n#12 corehole was drilled at -60° to the horizontal and U-15n#13 was drilled vertically in granitic rock (quartz monzonite) after the third SPE shot. Figure 1 illustrates at the surface, U 15n#12 and U-15n#13 coreholes were approximately 30 meters and 10 meters from the central SPE borehole (U-15n) respectively. Corehole U-15n#12 intersects the central SPE borehole (U 15n) at a core depth of 174 feet (approximately 150 feet vertical depth). The location of U 15n#12 and U-15n#13 is the site of the first, second and third SPE's, in Area 15 of the NNSS.

58 GEOSCIENCES↗

DOE OSTI2018

Mechanical Testing Results on Core from Borehole U-15n, NNSS, in support of SPE

The Nevada National Security Site (NNSS) will serve as the geologic setting for a Source Physics Experiment (SPE) program. The SPE will provide ground truth data to create and improve strong ground motion and seismic S-wave generation and propagation models. The NNSS was chosen as the test bed because it provides a variety of geologic settings ranging from relatively simple to very complex. Each series of SPE testing will comprise the setting and firing of explosive charges (source) placed in a central bore hole at varying depths and recording ground motions in instrumented bore holes located in two rings around the source positioned at different radii. Modeling using advanced simulation codes will be performed both a priori and after each test to predict ground response and to improve models based on acquired field data, respectively. A key component in the predictive capability and ultimate validation of the models is the full understanding of the intervening geology between the source and the instrumented bore holes including the geomechanical behavior of the site rock/structural features. This report presents a limited scope of work for an initial phase of primarily unconfined compression testing. Samples tested came from the U-15n core hole, which was drilled in granitic rock (quartz monzonite). The core hole was drilled at the location of the central SPE borehole, and thus represents material in which the explosive charges will be detonated. The U-15n location is the site of the first SPE, in Area 15 of the NNSS.

58 GEOSCIENCES↗

DOE OSTI2018

Study of Rg wave amplitude for SPE series using zero-mean stacking method

A modified version of the zero-mean stacking method is proposed to study Rgwave propagation effects recorded on the five lines of geophones during the first Phase of SPE. The relatively shallow depth of this series favors the generation of SPE series. We expect significant propagation effects due the strong azimuthal variation of the local geology and topography within the 2km extent of the geophone lines. We add bootstrapping to the method allowing to obtain a profile for each line and for five frequency-bands optimized in regards to consistency between explosions. Our results show that there is indeed consistency so we can conclude there were no significant changes in the subsurface of SPE in the 5 years of the first phase of SPE. We estimate attenuation coefficients for each lines and found consistent results between lines for the frequencies between 3 and 10Hz despite the difference of geology setting. This result is consistent with previous studies. We also deduce amplitude at Rg waves at ground-zero. We conclude that we need a better understanding of the uncertainty on these results to bring insight into the seismic sources of Rg waves.

58 GEOSCIENCES↗

DOE OSTI2018

Explosion Source Models and the Scattering Origin of Regional Phases from SPE Phase 1 Coda Spectral Ratios

The Source Physics Experiment(SPE)explosions provide comprehensive ground truth information,and nearby recordings that are rarely available in typical monitoring scenarios. Here, we look for relationships with local and regional distance data to understand source and propagation effects in an effort to improve monitoring at a distance. We examine source spectral ratios, which can be measured to high precision by taking advantage of many SPE and independently operated stations, as well as the redundancy available from coda waves. Classical source models (Mueller and Murphy, 1971, MM71; Denny and Johnson, 1991, DJ91)predict the source ratios poorly; however, a hybrid model(MM71 with DJ91 cavity radii)performs better, and by varying cavity and elastic radii we obtain models that fit to within measurement precision. Based on this, the best prediction model for the SPE suite is the hybrid model with cavity radius decreased by 95%, and elastic radius decreased by 75%. This works best for mid-range scaled depths of burial (SPE-1, 2, 3, and 5). We do not guarantee transportability to other geologies,depth and scaled depth ranges. Finally, we observe a distinct spectral modulation at 6-9Hzthat is not predicted by classical models, and is most likely the result of interference of short period surface waves(Rg)with those produced by spallation of near surface layers.The same modulationis observed for compressional (P) and shear(S) waves at distance, indicating the origin of these waves as scattered Rg.The scattering process must be accounted for quantitatively when using distant signals to monitor treaty compliance over broad regions.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2019

The Source Physics Experiment (SPE) Science Plan (Version 2.4c)

The Source Physics Experiment (SPE) series is a long-term NNSA research and development effort designed to improve U.S. arms control and nuclear nonproliferation verification and monitoring capabilities. The findings from the SPE will advance the United States’ nuclear explosion monitoring capabilities, particularly with respect to detection, discrimination and determination of yields associated with small nuclear explosions that can be lost amid the noisy seismo-acoustic background from other sources. The data generated from the SPE, a series of well-designed and recorded chemical explosions, will contribute to the development and validation of first-principles explosive source generated seismo-acoustic modeling codes. These codes will then facilitate the update of semi-empirical methods, currently based on historic test site data, such that key explosion observables can be reproduced, thus improving confidence in nuclear test monitoring in new areas and/or under novel emplacement conditions. The overall SPE project is comprised of both the development of the new explosion simulation codes and the chemical explosion test series. The chemical explosion test series will generate the empirical data required to both develop and validate the new simulation codes.

58 GEOSCIENCES↗

DOE OSTI2022

The Source Physics Experiment (SPE) Science Plan

58 GEOSCIENCES↗

DOE OSTI2025

SPE-CZE-MS Quantifies Zeptomole Amounts of Phosphorylated Peptides

Capillary zone electrophoresis (CZE) is gaining attention in the field of single-cell proteomics for its ultralow-flow and high-resolution separation abilities. Even more sample-limited yet rich in biological information are phosphoproteomics experiments, as the phosphoproteome composes only a fraction of the whole cellular proteome. Rapid analysis, high sensitivity, and maximization of sample utilization are paramount for single-cell analysis. Some challenges of coupling CZE analysis with mass spectrometry analysis (MS) of complex mixtures include 1. sensitivity due to volume loading limitations of CZE and 2. incompatibility of MS duty cycles with electropherographic time scales. Here, we address these two challenges as applied to singlecell- equivalent phosphoproteomics experiments by interfacing a microchip-based CZE device integrated with a solid-phaseextraction (SPE) bed with the Orbitrap Astral mass spectrometer. Using 225 phosphorylated peptide standards and phosphorylated peptide-enriched mouse brain tissue, we investigate microchip-based SPE-CZE functionality, quantitative performance, and complementarity to nano-LC-MS (nLC-MS) analysis. We highlight unique SPE-CZE separation mechanisms that can empower fitfor- purpose applications in single-cell-equivalent phosphoproteomics.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2018

Dynamic Brazilian Tension Results on Core from Borehole U-15n, NNSS, in support of SPE

Dynamic Brazilian tension (DBR) tests from core hole U-15n are part of a larger material characterization effort for the Source Physics Experiment (SPE) project. This larger effort encompasses characterizing Climax Stock granite rock from the Nevada National Security Site (NNSS) both before and after each SPE shot. The current test series includes DBR tests on dry intact granite and fault material at depths of -85 and -150 ft.

36 MATERIALS SCIENCE↗

DOE OSTI2018

Triaxial Compression Results on Core from Borehole U-15n, NNSS, in support of SPE

Triaxial compression tests from core hole U-15n are part of a larger material characterization effort for the Source Physics Experiment (SPE) project. This larger effort encompasses characterizing Climax Stock granite rock from the Nevada National Security Site (NNSS) both before and after each SPE shot. The current test series includes triaxial compression tests on dry and saturated intact granite and fault material at 100, 200, 300, and 400 MPa confining pressure.

58 GEOSCIENCES↗

DOE OSTI2019

A Traditional Look at SPE Phase 1 Surface Seismic Data: Far-Field Instruments, Measurements, and Analysis

We visually examined surface seismic data from the Source Physics Experiment (SPE) Phase-1 chemical explosions in preparation for waveform analysis and interpretation. Recording stations included far-field (near source) geophone lines, and both permanent network, reoccupied USArray, and temporary stations at local and regional distances. We found that near-source waveforms are dominated by broad band compressional (P), and band limited surface wave (Rg) (< 10 Hz) phases. Distinct, consistent shear (S) phases are difficult to observe visually even with a comprehensive bank of frequency bands. Secondary phases are indistinct at near-local distances, unlike for earthquake sources, especially at the high frequencies of interest for discrimination (e.g. 4-8 Hz), likely due to intense near surface scattering. S phases begin to emerge from the scattered background at and beyond 100 km. We identified regional Pn, Pg and Lg phases to 446 km for SPE-5. The data set is, unfortunately, plagued by poorly recorded instrument responses, or, possibly, time varying site amplification due to human interaction with sensors. Instrument response issues should be fixable, and this should be attempted to make this a truly, high-quality data set for use by the monitoring community.

58 GEOSCIENCES↗

DOE OSTI2019

Explosion Source Models and the Scattering Origin of Regional Phases from SPE Phase 1 Coda Spectral Ratios: Monitoring Implications –Discrimination and Yield Estimation

The Source Physics Experiment (SPE) explosions provide comprehensive ground truth information, and near-source recordings that are rarely available in typical monitoring scenarios. Here, we analyze these data together with local and regional distance recordings to isolate source and propagation effects, and to potentially improve monitoring at distance. We examine source spectral ratios, which can be measured to high precision by taking advantage of many SPE and independently operated stations, as well as the redundancy available from coda waves. Classical source models (Mueller and Murphy, 1971, MM71; Denny and Johnson, 1991, DJ91) predict the source ratios poorly; however, a hybrid model (MM71 with DJ91 cavity radii) performs better. We observe a distinct spectral modulation at 6-9 Hz that is not predicted by classical models, most likely caused by short period surface waves (Rg) interfering with those produced by spallation of near surface layers. The same modulation is observed for compressional (P) and shear (S) waves at distance, indicating that local and regional phases originate as near-source Rg that is scattered into body waves. The scattering process must be accounted for quantitatively to best use remotely recorded signals to monitor treaty compliance, discriminate event types, and estimate explosion yields over broad regions.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2021

2021 Summer SPE Project

SPE is a project in order to develop new, more physics-based, seismic models of explosions (see Nelson et al. 2013). One key component of this effort is numerical modeling enabled by modern state-of-art code/software. Accurate modeling of the shape and amplitude of seismic waves from their generation to their propagation to remote monitoring seismic stations is important to our ability to determine the origin and strength of the source from remote recording. In this project, the modeling is performed by coupling two codes HOSS and SPECFEM3D. HOSS models the dynamic nonlinear processes happening near the explosion. SPECFEM3D computes the propagation of seismic waves as they travel through 3D complex Earth models. SPECFEM3D was modified in order to be driven by a set of time-series calculated by HOSS in lieu of a seismic source. The goal of this summer project is the investigation of several questions pertinent to the establishment of a full end-to-end modeling capability from the high-rate strain regime area to remote distances where seismic station record seismic waves generated by explosions. The investigated questions are: (1) How to perform proper filtering? Direct-solution modeling only sustains a limited range of frequency depending on the grid size. As we go from one modeling domain to the other via coupling, the mesh size is getting coarser to allow modeling at large scale but also to account for the fact that high-frequency waves do not physically travel to large distances. So filtering of the time-series generated by the near-field hydrodynamic modeling is a current practice often employed but its effects on the modeled waveforms has to be investigated. (2) Quantitative assessment of the efficiency of attenuation to remove high-frequency content of the wavefield. This assessment will allow to create meshes with a grid size appropriate to the actual physics of wave propagation for a given explosion. (3) Checking that the coupling process and the two codes respect the cylindrical symmetry that is expected in the case of a pure explosion in a half-space. (4) The effect of the state-of-stress in the near-source area on the modeled seismic waveforms. These questions will be investigated through the modeling of SPE-4P, the fourth explosion of this series because it was designed to have little interaction with the geologic surrounding and the free surface of the Earth so that it is the most explosion-like experiment, with the most symmetries to be verified.

58 GEOSCIENCES↗

DOE OSTI2017

Data Release Report for Source Physics Experiment 4Prime (SPE-4Prime) Nevada National Security Site (Revision 1)

The fourth test in the Source Physics Experiment series (SPE-4Prime) was conducted at a granite site in Nevada on May 21, 2015, at 18:35:44.000,003,989 ± 20 nanoseconds Coordinated Universal Time. The explosive source was 69.1 kilograms (kg) (including detonator assembly) of Composition C4 plastic explosive (89.14 kg TNT equivalent) detonated at a depth of 87.2 meters (m). The explosion was recorded by an extensive set of instrumentation that includes sensors both at near-field (less than 100 m) and far-field (100 m or greater) distances. The near-field instruments consisted of three-component accelerometers installed at various depths from 7 to 99 m in boreholes positioned around the source hole, and a set of single-component vertical accelerometers on the surface. The far-field network was composed of a variety of seismic and acoustic sensors, including short-period geophones, broadband seismometers, and three-component accelerometers at distances of 100 m to 25 kilometers. Infrasound data were collected from ground-based sensor arrays at distances out to 5 kilometers. This revised document includes a new Section 3.2.2, which is a discussion of clock timing issues discovered at four far-field stations.

58 GEOSCIENCES↗

DOE OSTI2017

Data Release Report for Source Physics Experiment 4Prime (SPE-4Prime) Nevada National Security Site

58 GEOSCIENCES↗

DOE OSTI2019

Testing the MDAC2 Far-field Approximation with Application to SPE-5 and DAG-2

Our test is to compare calculated far-field amplitudes with the MDAC2 predicted amplitudes for two source media; one where the source is in hard-rock (SPE-5) and one where the source is in soft-rock (DAG-2). The receiver medium will remain the same, and is similar to the hard-rock source medium. The far-field displacement amplitudes are calculated by the Serpentine Wave Propagation 4th-order (SW4) solver. More information on SW4 can be found in Petersson and Sjogreen (2017).

58 GEOSCIENCES↗