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DOE OSTI2021

Summary of MCU Flush Sample Results

Starting in May 2021, samples from the Modular Caustic-Side Solvent Extraction Unit (MCU) were sent to the Savannah River National Laboratory (SRNL) for analysis. Samples resulting from flushes of the Strip Effluent Hold Tank (SEHT) and the Decontaminated Salt Solution Hold Tank (DSSHT) were sent on multiple dates. Over the range of samples, all had less than detectable concentrations of Isopar-L™, and there was an overall decline in 137 Cs activity.

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DOE OSTI2020

2019 Annual Sampling - Results Summary Table [Requested documents for Department of Toxic Substance Control]

A table showing sampling results from 2019 is provided.

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DOE OSTI2021

Soil Sampling Results for Closure of a Portion of Solid Waste Management Unit #16

The U.S. Department of Energy/National Nuclear Security Administration (DOE/ NNSA) and National Technology & Engineering Solutions of Sandia, LLC (NTESS), the management and operating contractor for Sandia National Laboratories/California (SNL/CA), has prepared this soil sampling results report for closure of a portion of Solid Waste Management Unit (SWMU) #16. The entire network of SNL/CA sanitary sewer lines, including building laterals, was identified as SWMU #16 under a Resource Conservation and Recovery Act (RCRA) Facility Assessment conducted for SNL/CA in April 1991 (DOE 1992). Along with the previous SWMU #16 investigation results (SNL/CA 2019), the results of this investigation are intended to support closure decisions by the San Francisco Bay Regional Water Quality Control Board (RWQCB), as discussed below. SNL/CA personnel completed upgrading its sanitary sewer discharge network in 2019. These upgrades included installing new sections of underground lines and decommissioning certain sections of the old piping system by capping in place. To date, several sections of the sewer line have been abandoned-in-place by capping as new sewer lines were installed or flow was rerouted to other existing lines. To formally close these abandoned sections of the sewer line, the RWQCB required that SNL/CA personnel collect soil samples to be analyzed for contaminants potentially released from the sewer lines. SNL/CA personnel hired Weiss Associates (Weiss) of Emeryville, California to prepare a sampling and analysis plan, implement the sampling plan and report the results of the investigation under Purchase Order #2166257. The Sampling and Analysis Plan for Partial Closure of Solid Waste Management Unit #16 (SAP) was submitted to the RWQCB on August 14, 2020 by Weiss on behalf of SNL/CA. The RWQCB approved the SAP on September 30, 2020 after Weiss updated the method detection limit and reporting limits for total polychlorinated biphenyls (PCBs) and individual aroclors. Soil sampling was conducted in accordance with the SAP except that fewer locations were sampled due to site constraints, as discussed below. This report presents the results of the sampling effort and documents all associated field activities including borehole clearing, soil sample collection, storage and transportation to the analytical laboratories, borehole backfilling and surface restoration, and storage of investigation-derived waste (IDW) for future profiling and disposal by SNL/CA waste management personnel.

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DOE OSTI2023

Soil Sampling Results for Delineating BH-056 for Partial Closure of Solid Waste Management Unit #16

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DOE OSTI2021

Soil Sampling Results for Closure of a Portion of Solid Waste Management Unit #16

This report presents the results of the sampling effort and documents all associated field activities including borehole clearing, soil sample collection, storage and transportation to the analytical laboratories, borehole backfilling and surface restoration, and storage of investigation-derived waste (IDW) for future profiling and disposal by SNL/CA waste management personnel.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2022

Response Letter to RWQCB's Comments on Soil Sampling Results for SWMU #16

The Department of Energy, National Nuclear Security Administration, Sandia Field Office, and National Technology & Engineering Solutions of Sandia, LLC (NTESS), the management and operating contractor for Sandia National Laboratories, California (SNL/CA), are responding to the Regional Water Quality Control Board (Water Board) comments dated February 16, 2022 (Enclosure 1) on the report titled Soil Sampling Results for Closure of a Portion of Solid Waste Management Unit (SWMU) #16 dated January 6, 2022 (Report).

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2023

IAEA PT sample results and analysis [Slides]

Data shows that we need to keep the requirement for matching samples and standards as the set of data from matching standards and samples is qualitatively better with fewer questionable or actionable measurements. Both before and after estimated buoyance corrections.

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DOE OSTI2021

Solvent Hold Tank Sample Results for MCU-20-32-33-34 (Quarterly Report, September 2020)

In late FY13, MCU implemented the Next Generation Solvent (NGS) flow sheet. Facility personnel added a non-radioactive, NGS “cocktail” containing the new Extractant (MaxCalix) and a new Suppressor (TiDG) to the SHT heel to implement the NGS flow sheet. The resulting “blend” solvent (“NGS blend solvent”) is essentially NGS with residual amounts of calix[4]arene-bis(tert-octylbenzo-crown-6) (BOBCalixC6) and trioctylamine (TOA). For process monitoring, SHT samples are sent to Savannah River National Laboratory (SRNL) to examine solvent composition changes over time. With the exception of Isopar™ L which is regularly added to the SHT due to its high vapor pressure, this report shows the cumulative chemical composition data, including impurities like mercury, of the September 2020 (MCU-20-32-33-34) solvent SHT sample. A summary report of the September SHT solvent sample was issued earlier. This report examines the cumulative results from these and several past monthly reports. These samples are intended to verify that the solvent is within the specified composition range. A baseline “scratch” solvent - a scratch solvent is a preparation of all 6 solvent components (this includes the old extractant BoBCalix and the old suppressor TrioctylAmine that remained when solvent was converted to Next Generation Solvent [NGS]) of the composition that approximates the blend of cocktail and heel solvent - was prepared in the lab (September 2018) and used for comparison and evaluation. The results from the analyses are presented in this document. This report is the last characterization analysis of the SHT solvent. MCU entered a lay-up state and about 128 gallons of the SHT solvent were pumped into 55 gallons drums for future disposal.

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DOE OSTI2020

Solvent Hold Tank Sample Results for MCU-19-557- 558-559 (July 2019), MCU-19-560-561-562 (August 2019), MCU-19-566-567-568 (September 2019) (Quarterly Report)

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DOE OSTI2020

Solvent Hold Tank Sample Results for MCU-19-569-571 (December 2019), MCU-20-1-28 (January 2020), and MCU-20-29-30-31 (June 2020) (Quarterly Report)

A trend summary of three Solvent Hold Tank (SHT) monthly samples MCU-19-569-570-571 (December 2019), MCU-20-1-28 (January 2020), and MCU-20-29-30-31 (June 2020) are reported. Most of the conclusions are based on the June 2020 SHT sample (MCU-20-29-30-31). Analyses of the June 2020 SHT sample indicated that the Modifier (Cs-7SB) and the Extractant (MaxCalix) concentrations were above their nominal recommended concentrations (169,000 mg/L and 46,900 mg/L respectively) by 6% and 7% respectively. The Suppressor (N,N’,N”–tris(3,7-dimethyloctyl)guanidine or TiDG) concentration has remained at 833 ± 16 mg/L, but it is above the minimum recommended concentration (479 mg/L). The Semi-Volatile Organic Analysis (SVOA) and FT-HNMR did not detect any organic impurities. Another impurity observed in the samples was mercury. Based on the June 2020 SHT sample, up to 23 ± 5 micrograms of mercury per gram of solvent (or 19 ± 4 mg/L) was detected. The mercury concentration steadily decreased from 34.8 ug/g solvent (or 21.9 mg/L) in the December 2019 SHT sample to 34.8 ug/g solvent (or 19 mg/L) in the June 2020 SHT sample. The gamma concentration (~3.33E4 dpm/mL) measured in the June 2020 SHT samples was consistent with previous values observed when MCU was idle (for example, between February 2017 and August 2017). If additional SHT samples become available, the laboratory will continue to monitor the quality of the solvent for any new impurities or degradation of the solvent components.

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DOE OSTI2020

Solvent Hold Tank Sample Results for MCU-19-366- 367-368 (April 2019), MCU-19-469-470-471 (May 2019), MCU-19-524-525-526 (June 2019): Quarterly Report

A trend summary of three sets of Solvent Hold Tank (SHT) monthly samples MCU-19-366-367-368 (April), MCU-19-469-470-471 (May), and MCU-19-524-525-526 (June) are reported. Most of the conclusions are based on the June SHT sample (MCU-19-524-525-526). Analyses of the June SHT sample (MCU-19-524- 525-526) indicated that the Modifier (Cs-7SB) and the Extractant (MaxCalix) concentrations were below their nominal recommended concentrations (169,000 mg/L and 46,900 mg/L respectively) by 4% and 2% respectively but consistent with previously observed levels during normal runs. The Suppressor (N,N’,N”– tris(3,7-dimethyloctyl)guanidine or TiDG) concentration has decreased since the March 2019 measurement to 793 mg/L, which is above the minimum recommended concentration (479 mg/L). The Semi-Volatile Organic Analysis (SVOA) did not detect any impurities. However, the Fourier Transform Hydrogen Nuclear Magnetic Resonance (FT-HNMR) analysis detected presence of phthalates at a few ppm. The impurity concentration was highest in the April sample and consistently detected in the May and June samples (but always registered as a few ppm or less). Another impurity observed in the samples was mercury. Based on the June SHT sample, up to 25 ± 5 micrograms of mercury per mL of solvent was detected (as the average of the Direct Mercury Analysis (DMA) and X-Ray Fluorescence (XRF) methods). The higher mercury concentration in the solvent (as determined in the last three-monthly samples) is possibly due to the higher mercury concentration in Salt Batches 9 and 10. The gamma concentration (~2.90E4 dpm/mL) measured in the June 2019 SHT samples was consistent with previous values observed when the Modular Caustic-Side Solvent Extraction Unit (MCU) was operating continuously (for example, between December 2016 and January 2017). Statistical analysis of the different analytical methods detected a bias between the FT-HNMR and the High Performance Liquid Chromatography (HPLC) methods when measuring the MaxCalix and Modifier concentrations; the FT-HNMR gave a higher concentration possibly due to peak overlapping in the measured data. A bias was detected when measuring total mercury by the DMA method versus the XRF method with the XRF method reported higher mercury concentrations. The laboratory will continue to monitor the quality of the solvent for any new impurities or degradation of the solvent components.

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NASA NTRS2009

Blended-Wing-Body Low-Speed Flight Dynamics: Summary of Ground Tests and Sample Results

A series of low-speed wind tunnel tests of a Blended-Wing-Body tri-jet configuration to evaluate the low-speed static and dynamic stability and control characteristics over the full envelope of angle of attack and sideslip are summarized. These data were collected for use in simulation studies of the edge-of-the-envelope and potential out-of-control flight characteristics. Some selected results with lessons learned are presented.

Vicroy, Dan D.↗

NASA NTRS2009

Blended-Wing-Body Transonic Aerodynamics: Summary of Ground Tests and Sample Results

The Blended-Wing-Body (BWB) concept has shown substantial performance benefits over conventional aircraft configuration with part of the benefit being derived from the absence of a conventional empennage arrangement. The configuration instead relies upon a bank of trailing edge devices to provide control authority and augment stability. To determine the aerodynamic characteristics of the aircraft, several wind tunnel tests were conducted with a 2% model of Boeing's BWB-450-1L configuration. The tests were conducted in the NASA Langley Research Center's National Transonic Facility and the Arnold Engineering Development Center s 16-Foot Transonic Tunnel. Characteristics of the configuration and the effectiveness of the elevons, drag rudders and winglet rudders were measured at various angles of attack, yaw angles, and Mach numbers (subsonic to transonic speeds). The data from these tests will be used to develop a high fidelity simulation model for flight dynamics analysis and also serve as a reference for CFD comparisons. This paper provides an overview of the wind tunnel tests and examines the effects of Reynolds number, Mach number, pitch-pause versus continuous sweep data acquisition and compares the data from the two wind tunnels.

Carter, Melissa B.↗

NASA NTRS1985

Statistical mechanics of light elements at high pressure. VII - A perturbative free energy for arbitrary mixtures of H and He

A model free energy is presented which accurately represents results from 45 high-precision Monte Carlo calculations of the thermodynamics of hydrogen-helium mixtures at pressures of astrophysical and planetophysical interest. The free energy is calculated using free-electron perturbation theory (dielectric function theory), and is an extension of the expression given in an earlier paper in this series. However, it fits the Monte Carlo results more accurately, and is valid for the full range of compositions from pure hydrogen to pure helium. Using the new free energy, the phase diagram of mixtures of liquid metallic hydrogen and helium is calculated and compared with earlier results. Sample results for mixing volumes are also presented, and the new free energy expression is used to compute a theoretical Jovian adiabat and compare the adiabat with results from three-dimensional Thomas-Fermi-Dirac theory. The present theory gives slightly higher densities at pressures of about 10 megabars.

Hubbard, W. B.↗

NASA NTRS1985

Modeling the filament winding process

A model is presented which can be used to determine the appropriate values of the process variables for filament winding a cylinder. The model provides the cylinder temperature, viscosity, degree of cure, fiber position and fiber tension as functions of position and time during the filament winding and subsequent cure, and the residual stresses and strains within the cylinder during and after the cure. A computer code was developed to obtain quantitative results. Sample results are given which illustrate the information that can be generated with this code.

Calius, E. P.↗

NASA NTRS2002

Effect of Random Geometric Uncertainty on the Computational Design of a 3-D Flexible Wing

The effect of geometric uncertainty due to statistically independent, random, normally distributed shape parameters is demonstrated in the computational design of a 3-D flexible wing. A first-order second-moment statistical approximation method is used to propagate the assumed input uncertainty through coupled Euler CFD aerodynamic / finite element structural codes for both analysis and sensitivity analysis. First-order sensitivity derivatives obtained by automatic differentiation are used in the input uncertainty propagation. These propagated uncertainties are then used to perform a robust design of a simple 3-D flexible wing at supercritical flow conditions. The effect of the random input uncertainties is shown by comparison with conventional deterministic design results. Sample results are shown for wing planform, airfoil section, and structural sizing variables.

Gumbert, C. R.↗

DOE OSTI2023

Measurement Acceptance Region (MAR) Assessment Results Based on Confirmation Sample Sludge Batch 10 Projections

The Defense Waste Processing Facility (DWPF) is currently preparing to initiate processing of Sludge Batch 10 (SB10), which is comprised of material from Tanks 11H, 13H, 15H, 26F, 40H (heel only), and Alternate Feed Stock-2 and Sodium Reactor Experiment material from H-Canyon. Frit 473 was recommended for sludge-only (SO) and coupled processing with the Salt Waste Processing Facility (SWPF) based on previous assessments of SB10 projections with the DWPF Product Composition Control System (PCCS) glass property models and their associated Measurement Acceptance Region (MAR) constraints. Savannah River Mission Completion (SRMC) subsequently pursued Wash Cycle Y to further reduce the total sulfur in the sludge batch and increase processing flexibility at DWPF. In October 2022, SRMC System Planning provided an updated SB10 Tank 40H blend baseline projection based on the Tank 51 confirmation sample results. Due to the reduced Na concentration relative to previous SB10 projections, two additional projections based on the addition of 7,000 gallons of caustic were provided in November 2022.

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DOE OSTI2020

Summary of Analytical Results from Samples Supporting Tank Closure Cesium Removal (TCCR) Batch 3 and Modeling Results for Cs Loading on CST

Savannah River Remediation (SRR) is currently operating the Tank Closure Cesium Removal (TCCR) process to remove 137 Cs from tank waste supernate using an ion exchange process. As part of that process, Savannah River National Laboratory (SRNL) receives and analyzes samples in support of the qualification of each batch to be processed. SRNL recently received supernate samples retrieved from Tank 10H as well as in-tank batch contact samples for characterization in support of qualifying Batch 3 for processing through the TCCR unit. Some results from analysis of those samples have been previously reported. This report documents the remaining analyses of the in-tank batch contact samples as well as the results of ZAM (Zheng, Anthony, Miller) isotherm modeling performed for comparison to the measured results. Results of the additional analyses include analysis of the loading of other radionuclides besides 137 Cs on the crystalline silicotitanate (CST) contained within the in-tank batch contact test samples. Results from those analyses revealed the next highest contributor to the activity on the CST was 90 Sr with an average loading of 2.76E+08 dpm/g CST compared to 3.56E+10 dpm/g CST for the 137Cs. Isotopes of plutonium were also detected on the samples. ZAM modeling was performed using the measured composition of the Tank 10H Batch 3 qualification samples. The modeling predicted a maximum Cs loading approximately 2.2x higher than the measured result. This is a slightly lower ratio (expected/measured) compared to what was observed for the prior TCCR in-tank batch contact testing performed for Batches 1A and 2 where the ZAM results were 2.7-2.8x higher than the measured values.

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