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VERAView Software Requirements, Test Plan, and Test Report

This document details the software requirements, test plan, and test results for VERAView. In this document, the test platform hardware and software are described. Section 2 provides a list of the tests run and their acceptability as a test report. Section 3 provides the step-by-step execution of these tests and their results.

97 MATHEMATICS AND COMPUTING↗

VERAIn Software Requirements, Test Plan, and Test Report

This document describes the software test plan for VERAIn and provides appendices for the software requirements and software test report. In this document, the test platform hardware and software are described. Appendix A provides a list of the tests run and their acceptability as a test report, and Appendix B provides the list of low-level software requirements as a requirements traceability matrix.

97 MATHEMATICS AND COMPUTING↗

MPACT Software Test Plan, Requirements, and Test Report (V.4.3)

This document presents the software test plan for MPACT. The software requirements and software test report are provided in the appendices. The test platform hardware and software are described herein. Appendix A provides a list of the tests that were run and their acceptability as a test report. Appendix B provides the list of low-level software requirements as a requirements traceability matrix.

97 MATHEMATICS AND COMPUTING↗

Optimal Nested Test Plan for Combinatorial Quantitative Group Testing

We consider the quantitative group testing problem where the objective is to identify defective items in a given population based on results of tests performed on subsets of the population. Under the quantitative group testing model, the result of each test reveals the number of defective items in the tested group. The minimum number of tests achievable by nested test plans was established by Aigner and Schughart in 1985 within a minimax framework. Furthermore, the optimal nested test plan offering this performance, however, was not obtained. In this paper, we establish the optimal nested test plan in a closed form. This optimal nested test plan is also order optimal among all test plans as the population size approaches infinity. Using heavy-hitter detection as a case study, we show via simulation examples orders of magnitude improvement of the group testing approach over two prevailing sampling-based approaches in detection accuracy and counter consumption. Other applications include anomaly detection and wideband spectrum sensing in cognitive radio systems.

97 MATHEMATICS AND COMPUTING↗

Hanford Waste End Effector Prototype Test Plan

This test plan describes the Phase 1 testing program of the Hanford Waste End Effector (HWEE) at the Washington River Protection Solutions (WRPS) Cold Test Facility (CTF) using a Pacific Northwest National Laboratory (PNNL)-designed testing setup. This task supports Phase 1 development testing of the HWEE to support the informational needs for initial assessment of the HWEE to support Hanford single shell tank A-105 retrieval. This task will install the HWEE on a PNNL-designed robotic gantry system at CTF, install instrumentation to measure reaction forces and process parameters, prepare and characterize simulant materials, and implement the test program. The tests will involve retrieval of water, sludge, and hardpan simulants to determine pumping rate, dilution factors, and screen fouling rate.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Test Plan for the Reirradiation Heating Test of Fuel Particles from AGR 2 Compact 5-4-2

Post irradiation examination (PIE) and high-temperature heating tests of tristructural isotropic (TRISO)-coated fuel particles and compacts from the second Advanced Gas Reactor (AGR) irradiation experiment, AGR 2, are in progress. This test plan describes the reirradiation and subsequent high-temperature testing of loose fuel particles obtained from AGR 2 Compact 5-4-2. To simulate exposed kernels, four of these particles have been cracked at Oak Ridge National Laboratory (ORNL) to produce localized defects that extend through the TRISO layers (outer-pyrolytic carbon [OPyC], silicon carbide [SiC], and inner-pyrolytic carbon [IPyC]) while keeping these layers in-place and maintaining the shape and integrity of the kernel. To generate short-lived fission products, these particles will be reirradiated in the Neutron Radiography (NRAD) reactor prior to heating testing in the Fuel Accident Condition Simulator (FACS) furnace. FACS testing will be at 1600°C, and fission products released from the reirradiated particles will be measured. The intention of the test is to assess the retention of short-lived fission products I-131 (t1/2 = 8.02 days) and Xe-133 (t1/2 = 5.2 days) in the fuel kernels at accident temperatures.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Hanford Waste End Effector Prototype Test Plan (Rev.1)

This test plan describes the Phase 1 testing program of the Hanford Waste End Effector (HWEE) at the Washington River Protection Solutions (WRPS) Cold Test Facility (CTF) using a Pacific Northwest National Laboratory (PNNL)-designed testing setup. This task supports Phase 1 development testing of the HWEE to support the informational needs for initial assessment of the HWEE to support Hanford single shell tank A-105 retrieval. This task will install the HWEE on a PNNL-designed robotic gantry system at CTF, install instrumentation to measure reaction forces and process parameters, prepare and characterize simulant materials, and implement the test program. The tests will involve retrieval of water, sludge, and hardpan simulants to determine pumping rate, dilution factors, and screen fouling rate.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Test Plan for the 1600°C Heating Test of AGR-3/4 Compact 3-2

Post irradiation examination (PIE) and heating tests of tristructural isotropic (TRISO)-coated fuel particles, fuel compacts, and graphite from the Advanced Gas Reactor (AGR) irradiation experiment AGR 3/4 is in progress. The AGR-3/4 test train consisted of twelve separate capsules irradiated in the northeast flux trap of the Advanced Test Reactor (ATR) at Idaho National Laboratory (INL) from December 14, 2011, to April 12, 2014 (Collin 2015). This test plan describes the heating test of AGR-3/4 Compact 3-2. The heating test will involve heating the compact in the Fuel Accident Condition Simulator (FACS) furnace to a peak temperature of 1600°C while collecting fission products released from the compact for subsequent analysis. One of several features of AGR-3/4 that set it apart from AGR-1 and AGR-2 is the incorporation of 20 designed-to-fail (DTF) particles in each compact. The fuel kernels in the DTF particles were coated only with a thin (20 µm thick) pyrocarbon layer having high anisotropy such that the coating should most-likely fail during the irradiation, resulting in up to 20 exposed kernels per compact. One of the main goals of this test is to assess the retention of fission products in the exposed kernels and the surrounding graphitic matrix material comprising the compact. Future heating tests will expose AGR-3/4 compacts at different temperatures in the FACS furnace (Demkowicz 2017). Additionally, the ability may be developed to heat re-irradiated AGR-3/4 compacts to allow a determination of the retention of short-lived fission products I-131 and Xe-133.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Test Plan for the 1400°C Heating Test of AGR-3/4 Compact 10-4

Post irradiation examination (PIE) and heating tests of tristructural isotropic (TRISO)-coated fuel particles, fuel compacts, and graphite from Advanced Gas Reactor (AGR) irradiation experiment AGR 3/4 is in progress. The AGR-3/4 test train consisted of twelve separate capsules irradiated in the northeast flux trap of the Advanced Test Reactor (ATR) at Idaho National Laboratory (INL) from December 14, 2011, to April 12, 2014 (Collin 2015). This test plan describes the heating test of AGR-3/4 Compact 10-4. The test will involve heating the compact in the Fuel Accident Condition Simulator (FACS) furnace to a peak temperature of 1400°C while collecting fission products released from the compact for subsequent analysis. One of several features of AGR-3/4 that set it apart from AGR-1 and AGR-2 is the incorporation of 20 designed-to-fail (DTF) particles in each compact. The fuel kernels in the DTF particles were coated only with a thin (20 µm thick) pyrocarbon layer having high anisotropy such that the coating would most-likely fail during the irradiation, resulting in up to 20 exposed kernels per compact. One of the main goals of this test is to assess the retention of fission products in the exposed kernels and the surrounding graphitic matrix material comprising the compact. Future heating tests will expose a number of AGR-3/4 compacts at different temperatures in the FACS furnace (Demkowicz 2017). Additionally, the ability may be developed to heat re-irradiated AGR-3/4 compacts to allow a determination of the retention of short-lived fission products I-131 and Xe-133.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Test Plan for the 1400°C Heating Test of AGR-3/4 Compact 8-2

Post irradiation examination (PIE) and heating tests of tristructural isotropic (TRISO)-coated fuel particles, fuel compacts, and graphite from Advanced Gas Reactor (AGR) irradiation experiment AGR 3/4 is in progress. The AGR-3/4 test train consisted of twelve separate capsules irradiated in the northeast flux trap of the Advanced Test Reactor (ATR) at Idaho National Laboratory (INL) from December 14, 2011, to April 12, 2014 (Collin 2015). This test plan describes the heating test of AGR-3/4 Compact 8-2. The test will involve heating the compact in the Fuel Accident Condition Simulator (FACS) furnace to a peak temperature of 1400°C while collecting fission products released from the compact for subsequent analysis. One of several features of AGR-3/4 that set it apart from AGR-1 and AGR-2 is the incorporation of 20 designed-to-fail (DTF) particles in each compact. The fuel kernels in the DTF particles were coated only with a thin (20 µm thick) pyrocarbon layer having high anisotropy such that the coating would most-likely fail during the irradiation, resulting in up to 20 exposed kernels per compact. One of the main goals of this test is to assess the retention of fission products in the exposed kernels and the surrounding graphitic matrix material comprising the compact. Future heating tests will expose a number of AGR-3/4 compacts at different temperatures in the FACS furnace (Demkowicz 2017). Additionally, the ability may be developed to heat re-irradiated AGR-3/4 compacts to allow a determination of the retention of short-lived fission products I-131 and Xe-133.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Test Plan for the 1200°C Heating Test of AGR-3/4 Compact 10-2

Post irradiation examination (PIE) and heating tests of tristructural isotropic (TRISO)-coated fuel particles, fuel compacts, and graphite from Advanced Gas Reactor (AGR) irradiation experiment AGR 3/4 is in progress. The AGR-3/4 test train consisted of twelve separate capsules irradiated in the northeast flux trap of the Advanced Test Reactor (ATR) at Idaho National Laboratory (INL) from December 14, 2011, to April 12, 2014 (Collin 2015). This test plan describes the heating test of AGR-3/4 Compact 10-2. The test will involve heating the compact in the Fuel Accident Condition Simulator (FACS) furnace to a peak temperature of 1200°C while collecting fission products released from the compact for subsequent analysis. One of several features of AGR-3/4 that set it apart from AGR-1 and AGR-2 is the incorporation of 20 designed-to-fail (DTF) particles in each compact. The fuel kernels in the DTF particles were coated only with a thin (20 µm thick) pyrocarbon layer having high anisotropy such that the coating would most-likely fail during the irradiation, resulting in up to 20 exposed kernels per compact. One of the main goals of this test is to assess the retention of fission products in the exposed kernels and the surrounding graphitic matrix material comprising the compact. Future heating tests will expose a number of AGR-3/4 compacts at different temperatures in the FACS furnace (Demkowicz 2017). Additionally, the ability may be developed to heat re-irradiated AGR-3/4 compacts to allow a determination of the retention of short-lived fission products I-131 and Xe-133.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Aluminum Clad Spent Nuclear Fuel Task 1: Oxyhydroxide Layer Behavior and Chemistry Experimental Test Plan

This document presents the test plan for Task 1 of the Aluminum Clad Spent Nuclear Fuel Long Term Dry Storage Technical Issues Action Plan, which covers aluminum clad spent nuclear fuel (ASNF) fuel that is currently or may in the future be held in dry storage for an extended period. The objectives of the Task 1 test plan are to: 1. Understand how ASNF performs over extended dry storage periods. 2. Understand mechanisms that could alter aluminum hydroxide/oxyhydroxide layers during extended storage. 3. Characterize thickness and growth rates of oxyhydroxide layers based on fuel history and provide anticipated H2 gas generation rates based on chemical corrosion. 4. Characterize materials properties for oxides present on ASNF. 5. Interface with canister modeling activity to deliver degradation rates for package performance for both sealed and vented configurations. 6. Understand implications of higher temperature drying (250°C) on stability in dry storage. This test plan lays out the technical activities that will be performed to achieve the test objectives described above. Experiments will be performed at Idaho National Laboratory in-town facilities. Specimens for testing will include those supplied by Savannah River National Laboratory. Activities will include both experiments and modeling and will coordinate with other tasks within the project.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Test Plan for the Third Reirradiation Heating Test of Fuel Particles from AGR 2 Compact 5-4-2

Post irradiation examination (PIE) and high-temperature heating tests of tristructural isotropic (TRISO)-coated fuel particles and compacts from the second Advanced Gas Reactor (AGR) irradiation experiment, AGR 2, are in progress. This test plan describes the reirradiation and subsequent high-temperature testing of loose fuel particles obtained from AGR 2 Compact 5-4-2. To simulate exposed kernels, four of these particles have been cracked at Oak Ridge National Laboratory (ORNL) to produce localized defects that extend through the TRISO layers (outer pyrolytic carbon, silicon carbide [SiC], and inner pyrolytic carbon) while keeping these layers in place and maintaining the shape and integrity of the kernel. To generate short-lived fission products, these particles will be reirradiated in the Neutron Radiography Reactor (NRAD) at the Hot Fuel Examination Facility (HFEF) at the Idaho National Laboratory (INL) Materials and Fuels Complex prior to heating testing in the Fuel Accident Condition Simulator (FACS) furnace at HFEF. FACS testing will be at 1200°C, and fission products released from the reirradiated particles will be measured. The intention of the test is to assess the retention of short-lived fission products I-131 (t1/2 = 8.02 days) and Xe-133 (t1/2 = 5.2 days) in the fuel kernels at high temperatures.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Test Plan for the Second Reirradiation Heating Test of Fuel Particles from AGR 2 Compact 6-4-1

Post irradiation examination (PIE) and high-temperature heating tests of tristructural isotropic (TRISO)-coated fuel particles and compacts from the second Advanced Gas Reactor (AGR) irradiation experiment, AGR 2, are in progress. This test plan describes the reirradiation and subsequent high-temperature testing of loose fuel particles obtained from AGR 2 compact 6-4-1. Four of these particles will have been cracked, gamma counted, and re-irradiated in the Neutron Radiography (NRAD) reactor prior to the heating test. The heating test will involve heating the particles in the Fuel Accident Condition Simulator (FACS) furnace to a peak temperature of approximately 1600°C while collecting fission products released from the particles for post-heating test analysis. The intention of the test is to assess the retention of fission products in the fuel kernel. Reirradiation of the particles will allow a determination of the retention of short-lived fission products I-131 (t1/2 = 8.02 days) and Xe-133 (t1/2 = 5.2 days) in the kernel.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Robustness of Asymptotic Optimal Accelerated Test Plans to Small-Sample Settings

Accelerated testing is a form of testing commonly employed in industry, especially at Sandia National Laboratories, in order to extract information about product lifetime behavior that cannot be acquired under normal operating conditions due to the extensive durations of the intended life- times. As of the writing of this report, there is no known guideline for the design of accelerated tests at the laboratories and yet there is an entire field in the statistical literature on the optimal design of accelerated tests covering a wide range of limitations and constraints available for reference. A potential roadblock to incorporating this knowledge is the common difficulty at Sandia of having severely limited data available for such testing. Nearly all of the methodology presented in the statistical literature is based on asymptotic or large-sample theory and so may not be appropriate for the testing conditions present at Sandia. This report investigates optimal accelerated test plans derived based on small-sample or exact methodology for both a basic test setting as well as a more realistic setting and compares the resulting test plans to those derived based on the large- sample methodology from the literature. It is shown that the large-sample test plans are actually quite robust to the presence of limited data and are generally more flexible than the small-sample test plans.

36 MATERIALS SCIENCE↗

Radiation Hardened Foam Cold Test Plan - Phase II: Foam Characterization Testing and Environmental Chamber Testing of FoamBag Fixative Foam

This document outlines the Phase II test objectives and implementation plan for a down-select foam fixative technology intended to facilitate activities in support of the Savannah River Site (SRS) F/H labs deactivation and decommissioning (D&D) efforts. It is a collaborative effort between Savannah River National Laboratory (SRNL), Florida International University (FIU), and the SRS F/H labs team intended to test and evaluate the potential of a polyurethane resin foam in mitigating the release of contamination during dismantling operations on radioactively contaminated piping in legacy facilities. The cold test plan addresses specific requirements highlighted by site and safety personnel and will be executed at FIU and SRNL test and lab facilities. Results from the cold tests will inform the hot test at F/H labs, which will use the foam fixative to confine and/or isolate residual contamination within a 3-dimensional void space of Hastelloy C-22 piping designated for removal from the area and transported to a designated disposal facility. Phase I testing was previously conducted using Hilti CP620 fixative foam. Results from Phase I testing indicate Hilti CP-620 fixative foam is incompatible with SRS site hot taps as an effective foam delivery method into Hastelloy C-22 piping. Phase II testing will be conducted using FoamBag TM fixative foam as an alternative fixative foam option. Phase II testing will address eight test objectives: (1) evaluation of the adhesion and bonding properties of FoamBag TM in Hastelloy C-22 piping, (2) evaluation of the adhesion of FoamBag TM in piping under various moisture conditions, (3) determination of the heat profile of FoamBag TM during curing, (4) determination of the internal pipe pressure after FoamBag TM deployment and curing, (5) conduct a leak test to determine if FoamBag TM is effective at creating a full seal within piping, (6) headspace testing of FoamBag TM to determine if there are any associated off-gas hazards during FoamBag TM curing, (7) conduct environmental chamber testing of FoamBag TM to understand how environmental parameters impacts FoamBag TM curing, and (8) conduct fire testing to evaluate FoamBag TM fire retardant characteristics.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗