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SR19016 - Characterization of AM Materials for SRTE Service

This project addresses several issues and challenges for the use of AM produced components in the tritium facility. It will evaluate the effect of low level hydrogen and tritium exposure on the mechanical and chemical characteristics of Arcam A2X Electron Beam Powder Bed Fusion Produced (EPBF) Ti-6AI-4V by printing tensile samples and testing them in the as printed, machined, and hydrogen exposed conditions. Hydrogen uptake will be measured using an Eltra Hydrogen-Oxygen- Nitrogen analyzer. Hydride response will be measured using a Seiffert's apparatus and determining the effects of various surface treatments on the hydriding susceptibility. Tools, fixtures, and other objects will be deigned and printed for use in the AM lab and tritum facility and for other groups that support the tiritum mission.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Solidification texture, variant selection, and phase fraction in a spot-melt electron-beam powder bed fusion processed Ti-6Al-4V

The effect of a spot melt strategy on the solidification texture, variant selection, phase fraction, and their variations along the build height was investigated in comparison to a conventional linear melt strategy. Ti-6Al-4V alloy samples were manufactured by an electron-beam powder bed fusion process using two different melt strategies and characterized using high-energy synchrotron x-ray diffraction. The linear and spot melt cases resulted in β<100> cube and fiber textures, respectively, with the cube/fiber axis nearly parallel to the build direction. The α phase exhibited Burgers orientation relationship (BOR) with the parent β phase for both melt strategies. Although all of the key texture components and the BOR between the α and β phases were consistently observed in both cases along the build height, there were several measurable differences between the two. At the top of the build height, the β<100> build texture intensity was stronger in the linear case. However, the texture intensity in the linear case decreased gradually from the top to near the substrate, whereas the spot melt case did not show this trend. Moreover, the BOR was examined along the build height and the results showed that there is a distinct variant selection in the spot melt case, unlike the linear case. Specifically, the planar variants sharing ($\bar101$) β || (0002) α with [$\bar2\bar2\bar2$]β and [$2\bar22$]β were the most prominent in the spot melt, but no preference was identified in the directional variants. The β phase fraction was slightly lower in the spot melt case compared to the linear case. In both the cases, the β phase fraction decreased moving towards the substrate but remained significantly higher than that of the powder feedstock. Overall, the novel spot melt strategy produced a more homogeneous microstructure in terms of both the phase fraction and texture across the build height.

36 MATERIALS SCIENCE↗

Critical differences between electron beam melted and selective laser melted Ti-6Al-4 V

Effective optimization of the production of Ti-6Al-4 V using AM requires a fundamental understanding of the relative importance of different microstructural features to the deformation and failure mechanisms, particularly features that vary between production methods. In this study, the tensile response and deformation mechanisms of electron beam melted (EBM) AM Ti-6Al-4 V material loaded in different orientations and produced using various powder sizes were compared to those of selective laser melted (SLM) AM Ti-6Al-4 V material. The density and morphology of pores, phase fractions, prior-β grains, and defect microstructures were evaluated using scanning electron microscopy, X-ray computed tomography, electron backscatter diffraction, and transmission electron microscopy before and after deformation. The results were used to evaluate the relative importance of each feature on strengthening, deformation, and failure initiation mechanisms. Results focused primarily on coarse-powder EBM materials indicated that phase distribution and defect density were most influential for determining material yield strength as well as maximum possible strain to failure. Porosity was lower overall in EBM Ti-6Al-4 V than in SLM, allowing for occasional increases in part strain to failure, but remained a limiting factor determining overall part ductility.

36 MATERIALS SCIENCE↗