Principles of Cosmic Particle Scattering Tomography-Green Radiography
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Muon Tomography↗
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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
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Ultra-High-Speed X-ray Tomography: Bridging the Gaps to See the Unknown
Rapid, time-varying, three-dimensional physics underpin numerous engineering challenges. Often, these physics occur within opaque environments, internal to a component, severely limiting applicable diagnostics. Development of novel diagnostics is necessary to understand and predict transient three-dimensional (3D) phenomena within opaque environments. This report highlights progress in four key areas leading to advancements in high-speed X-ray radiography and tomography. The first area is enabling MHz-rate imaging of energetics at the Advanced Photon Source at Argonne National Laboratory. The second is modeling a high-flux, rotating-anode X-ray source to understand the heat loads on the anode. The third effort was to develop a novel reconstruction algorithm that is validated by ground experimental tomography data and synthetic tomography data. The fourth is the development of a novel approach to two-color X-ray imaging.
42 ENGINEERING↗
Laboratory-Based Micro-X-ray Computed Tomography of Energy Materials at Idaho National Laboratory
Abstract The Idaho National Laboratory (INL) has implemented laboratory-based micro-X-ray computed tomography in a laboratory equipped for the examination of highly radioactive samples. This capability provides nondestructive three-dimensional volumetric information on samples to inform subsequent traditional destructive examinations as well as real-world inputs for high-fidelity scientific modeling. Samples can be imaged with spatial resolutions ranging from several hundred nm/voxel up to ~ 100 µm/voxel. The best usable spatial resolution achieved to date is 384 nm/voxel with this instrument, while the highest radiological dose rate of a sample imaged is ~ 60 R/h β/γ on contact. Advanced data analysis, including custom tomographic reconstruction and segmentation methods, have also been developed to support this capability. In addition to traditional digital X-ray radiography and tomography, this instrument is also able to visualize in situ tensile and compression testing as well as perform diffraction contrast tomography. This work describes the X-ray computed tomography post-irradiation examination capabilities at INL, as well as detailing a variety of applications this instrument has examined.
36 MATERIALS SCIENCE↗
Systematic Source Determination and X-Ray Radiography Detection of Nonuniformities on High-Density Carbon Ablators
Recent deuterium-tritium (D-T)–layered implosion experiments at the National Ignition Facility have achieved a burning plasma and >1-MJ neutron yield. A series of repeat experiments have shown that the degree of performance is very likely dependent on capsule quality, including the quantity of what are collectively termed “high- Z particles.” These particles are detected on a custom-built radiography system, known as the Sagometer, during the final target qualification process. The term particles is misleading, as the source of these nonuniformities in the capsule images is uncertain; the term detection will be used instead. An increased number of D-T targets have been rejected at the final stages of production due to Sagometer detections. Late detections are deleterious in terms of loss of production parts, effort, and overall operating efficiency. In response, we undertook an effort to determine the origin of these detections and to ultimately mitigate target losses caused by them. Through careful testing and analysis, we have determined neither insufficient production cleanliness nor hohlraum shedding is responsible for the detections on the capsule. Here, we determined that the detections are inherent to the capsule and have made efforts to use the Zeiss Xradia to identify them earlier in the production process. While testing revealed the Xradia is not currently sufficient for identifying such particles using radiography images, we continue to look to other forms of metrology to down select the capsules early in the process.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
Time-Resolved Neutron Imaging for Hydrogen Uptake in Subsurface Lithologies
Contains the neutron radiography and tomography images of hydrogen uptake in different geological lithologies.
36 MATERIALS SCIENCE↗
Generalizable Convex Mono-Density Object Reconstruction
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97 MATHEMATICS AND COMPUTING↗
TRTR NRAD NRS Beamline Abstract
The Neutron Radiography (NRAD) Reactor is a 250kW TRIGA housed under the largest hot cell in the United States, making it the foremost location to perform neutron imaging of irradiated nuclear fuels and materials, including those intended for use with advanced reactors. Currently, NRAD has two radial beamlines that are used for neutron radiography and tomography. Upgrades to the North neutron beamline include the replacement of the in-tank beam chamber, through-the-wall collimator, and neutron shutter. These beamline upgrades will not only improve image quality for current capabilities but will also condition the beam to be more suitable for advanced methods such as neutron powder diffraction. These upgrades will increase the excess reactivity of the core, reduce unnecessary activation and exposure to workers, and significantly reduce the amount of shielding required around the beam. This presentation will describe how these upgrades improve beam quality, increase utilization of the reactor, and reduce radiation exposure to personnel.
21 - SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLAN↗
Cosmic ray radiography of a human phantom
Cosmic ray muons that reach the earth's surface provide a natural source of radiation that is used for radiography. In this paper, we show that radiography using the cosmic radiation background provides a method that can be used to monitor bulk aspects of human anatomy. We describe a method that can be used to measure changes in patients as a function of time by cosmic ray muon radiography. Modeling shows muon tomography could provide hourly readouts of parameters such as lung density with sufficient sensitivity to detect the time changes in the inflammation of the lungs in, e.g., COVID patients.
60 APPLIED LIFE SCIENCES↗
Imaging Bragg Edge Analysis TooLs for Engineering Structures (iBeatles)
The Spallation Neutron Source (SNS) at Oak Ridge National Laboratory (ORNL) provides pulsed neutrons with energies varying from epithermal to cold. In preparation for VENUS, the neutron imaging beamline to be located at beam port 10, we have performed a series of experiments focused on wavelength-dependent radiography and computed tomography for a broad range of applications, from materials science to biological tissues.One of the time-of-flight (TOF) techniques that is of interest to the scientific community is the 2-dimensional mapping of phases and average crystalline plane orientation in samples both ex-situ and during applied stresses such as tensile loading and heating. This technique is known as Bragg edgeimaging and relies on the identification of changes of transmission values, fitting of the edge to measure its displacement, and thus identify the shift in lattice parameter due to stresses. One of the challenges of TOF imaging measurements is the amount of data and the inability to observe Bragg edge shifts in real time during an experiment. Thus, we have been focusing on creating a Python-based interface that allows fast data processing and instantaneous mapping and fitting of the Bragg edges, and their evolution through time. Python libraries and Jupyter notebooks have been implemented to facilitate decision making during an experiment. The advantage of the notebooks is the possibility to guide an experiment as they can quickly process and display Bragg edge data. These notebooks can be used independently, or can be combined in a Python Graphical User Interface (GUI) tool called iBeatles. This interface permits visualization and fitting of the Bragg edges, and ultimately back-projects the fitting results onto the radiographs to display a strain map. Assuming data collection has sufficient statistics, the strain mapping analysis can be performed on a pixel-by-pixel basis. This development is a step forward toward a better user experience at the future VENUS beamline in terms of live feedback and productivity. Analysis that used to take days of switching between different applications can now be done in minutes within the
Bilheux, JeanChristophe [Oak Ridge National Labora↗
Integral Experiment Request 554 CED-1 Summary Report
This Critical Engineering Decision 1 report for the Integral Experiment Request 554 describes the effects of adding a commercially available neutron absorber material to a known light-water low-enriched uranium assembly. The assembly in question is the Seven Percent Critical Experiments at Sandia National Laboratories. The neutron absorber plates considered for the experiment are called Boralcan, which are made of boron carbide (B 4 C) particles embedded in 1100 aluminum alloy. The concentrations of B 4 C and 1100 aluminum, as well as the thickness and size of the plates, were changed, and the fuel rod configuration was adapted to ensure that the assembly would be critical in each case studied. A total of 10 critical configurations with a neutron absorber plate inserted are described in this report. No results of high-quality integral experiments involving neutron absorbers made with B 4 C and 1100 aluminum plates are currently publicly available. Sensitivity to the neutron absorber plate material definition, isotopes, and cross sections of specific regions and configurations are also analyzed. The study results indicate that these experiments are achievable with sufficiently low uncertainties and minimal modification to the assembly. The experimental uncertainty can be further decreased with an additional characterization of the plates by x-ray computerized tomography or neutron radiography methods.
73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
Nondestructively Visualizing and Understanding the Mechano-Electro-chemical Origins of “Soft Short” and “Creeping” in All-Solid-State Batteries
All-solid-state Li-metal batteries (ASLMBs) represent a significant breakthrough in the quest to overcome limitations associated with traditional Li-ion batteries, particularly in energy density and safety aspects. However, widespread implementation is stymied due to a lack of profound understanding of the complex mechano-electro-chemical behavior of Li metal in the ASLMBs. Herein, operando neutron imaging and X-ray computed tomography (XCT) are leveraged to nondestructively visualize Li behaviors within ASLMBs. This approach offers real-time observations of Li evolutions, both pre- and post- occurrence of a “soft short”. The coordination of 2D neutron radiography and 3D neutron tomography enables charting of the terrain of Li metal deformation operando. Concurrently, XCT offers a 3D insight into the internal structure of the battery following a “soft short”. Despite the manifestation of a “soft short”, the persistence of Faradaic processes is observed. To study the elusive “soft short”, phase field modeling is coupled with electrochemistry and solid mechanics theory. The research unravels how external pressure curbs dendrite growth, potentially leading to dendrite fractures and thus uncovering the origins of both “soft” and “hard” shorts in ASLMBs. Furthermore, by harnessing finite element modeling, it dive deeper into the mechanical deformation and the fluidity of Li metal.
25 ENERGY STORAGE↗
High spatial resolution neutron imaging of lithium-ion batteries: Correlating microstructure and lithium transport
Thick electrodes for lithium-ion batteries can increase the overall energy density, but increasing the electrode thickness introduces charge transport limitations. These limitations may be mitigated through proper electrode structuring. Here, high spatial resolution neutron imaging was used to understand the correlation between microstructure and lithium transport in lithium-ion anodes. Batteries with distinct graphite anode microstructures were produced and studied with high spatial resolution in operando neutron radiography to observe the effects of structure on transport. High spatial resolution neutron computed tomography was performed following in operando neutron radiography. X-ray computed tomography and scanning electron microscopy were used to observe the finer scale anode structure to complement neutron imaging. Solvent-free anodes containing a tightly-packed layered structure confined lithium movement close to the separator. This structure limited capacity, but supported better rate capability. Conversely, a more open pore structure in the wet cast anodes yielded higher capacity with reduced rate capability. Together, these results show that lithium distributions can be controlled by the macroscopic structure of the electrodes, the microstructural pore network, and the microscale active areas that support electrochemical reactions. Furthermore, multimodal imaging applying the complementary strengths of neutron and X-ray methods is shown as a tool for advancing battery design.
25 ENERGY STORAGE↗
Needs, Trends, and Advances in Scintillators for Radiographic Imaging and Tomography
Not Available
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
Characterization of Porous Transport Layers Towards the Development of Efficient Proton Exchange Membrane Water Electrolysis
The current goals for implementing the hydrogen economy have highlighted a need to further optimize water-splitting technologies for clean hydrogen production. Proton exchange membrane water electrolysis (PEMWE) is a leading technology, but further optimizations of anode materials including the porous transport layer (PTL) and the adjacent catalyst layer (CL) are required to increase overall cell performance and reduce cost. This literature review describes advances in PTL development and characterization, highlighting early PTL characterization work and most common methods including capillary flow porometry and mercury intrusion porometry, optical imaging, neutron and x-ray radiography, and x-ray computed tomography. The article also discusses PTL protective coatings and their characterizations, focusing on platinum group metal (PGM)-based coatings, alternative non-PGM-based coatings, post-treated PTLs, and investigations into thin PGM-based coatings. Furthermore, it highlights the integration of the PTL and the adjacent CL along with associated characterization challenges. Lastly, this review discusses future developments in the characterization needed to improve PEMWE's performance and long-term durability are discussed.
08 HYDROGEN↗
Micro X-ray computed tomography examination of mini plate fuel with hot isostatic pressed aluminum cladding
In order to minimize proliferation risks and improve security of nuclear material, the United States high performance research and test reactors (USHPRR) program is tasked with converting nuclear reactors that are fueled with highly enriched uranium (HEU) fuels to operate with low-enriched uranium (LEU) nuclear fuels. One favorable LEU fuel configuration is plate fuel with a metallic uranium-molybdenum foil clad within an aluminum alloy (AA 6061). In this fuel, the aluminum cladding is bonded with a hot isostatic pressing (HIP) method to seal the cladding around the fuel meat. However, the HIP process parameters influence the cladding performance, as a defective or incomplete bond can cause a pathway for corrosion. Micro X-ray computed tomography (XCT), a nondestructive technique that provides volumetric imaging, can be applied to inspect fuel plate cladding at the engineering scale. In this work, XCT methodology was developed and successfully utilized to not only observe the bond line of unirradiated mini fuel plates, but to also identify subsurface abnormalities in the plates’ cladding. Importantly, in future work, this technique could be applied to fuel plates, pre- and post-irradiation, to quantify irradiation effects on cladding defects and bond line integrity.
36 MATERIALS SCIENCE↗
Livermore Computed Tomography Input/Output library
Read, write, and connect visualizers to data for LLNL radiography and CT tools (e.g. LTT: https://softwarelicensing.llnl.gov/product/livermore-tomography-tools-ltt).
Vardar-Irrgang, MichaelE [Lawrence Livermore Natio↗
Neutron-Friendly Li-Ion Battery Coin Cell for In Situ 3D Visualization of Li Plating
Advanced battery characterization using in situ/operando neutron imaging is critical for uncovering degradation modes such as lithium (Li) plating in Li-ion batteries (LIBs). However, conventional LIBs hinder operando neutron radiography (NR) and in situ neutron micro-computed tomography (N-μCT) for visualizing Li plating near the graphite-separator interface due to strong attenuation from hydrogen-rich components like PP–PE–PP separators, electrolyte, and Fe-based spacers. In this work, we designed and tested a neutron-friendly battery (NFB) optimized for in situ Li detection during extreme fast charging (XFC). Guided by neutron attenuation cross-sections and material transmission, the NFB enables clear visualization at the graphite–separator interface, which is typically opaque in standard LIBs. Electrochemical tests show the NFB exhibits voltage/current responses like standard cells for up to 50 XFC cycles. However, its lower reversibility and capacity are likely due to Cu-coated Al spacer degradation from delamination or corrosion. We propose titanium spacers as a more stable alternative, albeit requiring custom machining. Using this optimized cell, we achieved simultaneous neutron tomography of multiple cells, capturing in situ 3D images of dead Li accumulation, particularly near graphite edges. These heterogeneous deposits and disconnected Li clusters suggest localized current density hotspots during XFC.
25 ENERGY STORAGE↗
Detectors and diagnostics for multiprobe radiography using high-energy short-pulse lasers
Multiprobe radiography requires the following diagnostic capabilities at minimum: radiographic source diagnostics, spectroscopy, imaging, and tomography diagnostics. Depending on the repetition rate of the radiation sources, the diagnostics may be a single-shot diagnostic, such as photographic (radiochromic and X-ray films for high energy photons) films, or a multiple-shot diagnostic for repetitive source operations, such as a high-speed framing camera. Due to the drastically different detector physics of electrons, photons at different energies (keV to 10s of MeV in the radiography context), heavy ions such as protons, alphas, and neutrons, see, for example, Ref. [1, 2] for an overview, different types or configurations of detectors and constructions may be required for multiprobe radiography applications. Some of the common detector metricsinclude, independent of the particle/photon species, sensitivities or efficiency, energy resolution, spatial or temporal resolutions and others. Some unique detection scenarios arise in a multiprobe radiography setting, for example, crosstalk mitigation and particle identification (ID) when X-ray and higher energy photons, relativistic electrons, neutrons, other hadrons, and heavy particles coexist at the detector location.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗