Determination of the pitch of a cholesteric liquid crystal by infrared transmission measurements
Infrared transmission measurement of pitch of cholesteric liquid crystal
Baessler, H.↗
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Application of SAMMY for Non-Destructive Characterization of Irradiated Samples Using Neutron Transmission Measurements at VENUS
This report presents the application of SAMMY (Larson 2008), an R-matrix Bayesian fitting system, for analyzing neutron transmission data to enable non-destructive isotopic identification. Transmission measurements were conducted at the VENUS (Bilheux et al. 2023) beamline of the Spallation Neutron Source (SNS) using samples with unknown or partially characterized compositions. Through the application of SAMMY’s R-matrix Bayesian fitting capabilities to the measured transmission spectra and comparison against evaluated nuclear data libraries, isotopic constituents can be quantitatively determined based on their characteristic neutron resonance signatures. This methodology demonstrates significant potential for applications in nuclear safeguards, forensics, and post-irradiation examination.
73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
Determination of surface resistance and magnetic penetration depth of superconducting YBa2Cu3O(7-delta) thin films by microwave power transmission measurements
A novel waveguide power transmission measurement technique was developed to extract the complex conductivity of superconducting thin films at microwave frequencies. The microwave conductivity was taken of two laser ablated YBa2Cu3O(7-delta) thin films on LaAlO3 with transition temperatures of approx. 86.3 and 82 K, respectively, in the temperature range 25 to 300 K. From the conductivity values, the penetration depth was found to be approx. 0.54 and 0.43 micron, and the surface resistance (R sub s) to be approx. 24 and 36 micro-Ohms at 36 GHz and 76 K for the two films under consideration. The R sub s values were compared with those obtained from the change in the Q-factor of a 36 GHz Te sub 011-mode (OFHC) copper cavity by replacing one of its end walls with the superconducting sample. This technique allows noninvasive characterization of high transition temperature superconducting thin films at microwave frequencies.
Bhasin, K. B.↗
Determination of surface resistance and magnetic penetration depth of superconducting YBa2Cu3O(7-delta) thin films by microwave power transmission measurements
A novel waveguide power transmission measurement technique was developed to extract the complex conductivity of superconducting thin films at microwave frequencies. The microwave conductivity was taken of two laser ablated YBa2Cu3O(7-delta) thin films on LaAlO3 with transition temperatures of approximately 86.3 and 82 K, respectively, in the temperature range 25 to 300 K. From the conductivity values, the penetration depth was found to be approximately 0.54 and 0.43 micron, and the surface resistance (R sub s) to be approximately 24 and 36 micro-Ohms at 36 GHz and 76 K for the two films under consideration. The R sub s values were compared with those obtained from the change in the Q-factor of a 36 GHz Te sub 011-mode (OFHC) copper cavity by replacing one of its end walls with the superconducting sample. This technique allows noninvasive characterization of high transition superconducting thin films at microwave frequencies.
Bhasin, K. B.↗
Development of Transmission Measurements Capability at VISION Spectrometer [Slides]
This presentation covers the development of transmission measurements capability at VISION Spectrometer. Main takeaways include that INS and transmission measurements are and should be the most significant part of TSL validation, as they are the fundamental quantities used by Monte Carlo neutronics codes. Additionally, the development of transmission capability at VISION instrument has commenced. Promising first results have been obtained with a big impact by the use of the collimators. Finally, Areas of improvement have been identified and new measurements are planned for June.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
Determination of the pitch of a cholesteric liquid crystal by infrared transmission measurements
Cholesteric liquid crystal pitch from IR transmission measurements
Baessler, H.↗
Advancements in Validation of TSLs through Inelastic Neutron Scattering and Transmission Measurements [Slides]
This presentation finds that INS measurements are not as variable based on sample composition, because phonon spectra is a properly of the bulk material. Additionally, INS and transmission measurements are and should be the most significant part of TSL validation, as they are the fundamental quantities used by Monte Carlo neutronics codes. Relaying solely on theoretical atomistic calculations for TSL evaluation is not enough, they are highly dependent on inter-atomic potentials (which are not the most accurate depending on the quantity trying to be reproduced) and evaluators knowledge and understanding of the material being studied. When dealing with Crit. benchmarks - While extremely useful for validation of nuclear data at all energies, critical benchmarks are not the best tool to provide a definitive answer on conflicting TSLs. Finally, INS and transmission measurements need to be the basis of validation of TSLs.
73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
Advancements in Validation of TSLs through Inelastic Neutron Scattering and Transmission Measurements [Abstract]
Historically, the free gas approximation has been used to treat the thermal scattering of neutrons with energies below a few electron-volts (eV) in unevaluated materials. However, this method inadequately reproduces neutron scattering at these energies. Until recently, only a limited number of materials had available thermal scattering law (TSL) files/libraries in the ENDF nuclear data libraries in this energy range. With advancements in atomistic modeling techniques, such as molecular dynamics, ab-initio molecular dynamics, and density functional theory, TSL libraries have become available for many more materials. This is particularly relevant due to the rising interest in several advanced reactor systems that require novel moderator and reflector materials. While quasi-integral and integral benchmarks have been designed to validate historically important moderator materials (such as light water and polyethylene), there is currently a lack of standard validation methods for TSLs, especially when multiple conflicting TSLs exist. To address this issue, the Oak Ridge National Lab Nuclear Data group has been working on utilizing inelastic neutron scattering (INS) measurements combined with transmission (i.e., total cross section) measurements to evaluate and validate TSLs for different materials. We plan to demonstrate how this method has worked on materials such as polyethylene, lucite, and polystyrene. In addition, we will compare the newly created libraries to ENDF libraries for these materials and explain why integral benchmarks should not be used for validation when multiple TSLs exist.
73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
Spectral transmission measurements in the nu sub 6 fundamental of /C-12/H3D at 8.65 microns
Spectral transmission measurements were performed at 300 K in the 8.65-micron fundamental band of monodeuterated methane, a trace constituent in the atmosphere of Jupiter. A theoretical curve is obtained from line-by-line computation of the spectral transmission utilizing a triangular slit function with full width at half-maximum. The agreement between theoretical and experimental spectral transmission curves suggests that deuteration does not affect the collision-broadened half-widths significantly in the two extreme cases of broadening being considered.
Varanasi, P.↗
Neutron Capture and Transmission Measurements of 54 Fe at the RPI LINAC
54 Fe radiative capture cross section and transmission measurements were conducted at the Rensselaer Polytechnic Institute (RPI) Gaerttner Linear Accelerator (LINAC) Center using an enriched 54 Fe sample in the keV energy region. 54 Fe is a constituent of natural iron, which is present in a large variety of nuclear grade materials. Therefore, it is important to have an accurate understanding of the cross sections of 54 Fe, which can be measured experimentally. In the time-of-flight measurements conducted at the LINAC, an array of four C 6 D 6 detectors surrounded the sample and radiative capture data were collected using a digital data acquisition system. Additionally, a Li-glass detector was used to collect transmission data using an analog data acquisition system. The radiative capture yield of the 54 Fe measurements were normalized to saturated resonances observed in Au and Ta to obtain an absolute capture yield. The preliminary capture yield and preliminary transmission obtained can be compared to evaluations and existing experimental data. Some disagreements were observed in prominent d-wave capture resonances observed in 54 Fe in the low-keV neutron energy region. Both sets of experimental data along with pre-existing datasets will greatly enhance RPI’s ability to perform resonance evaluation for 54 Fe up to roughly 1 MeV.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
A Large Area Picosecond Photodetector for Neutron Transmission Measurements at DICER at LANSCE
The Device for Indirect Capture Experiments on Radionuclides (DICER) is a new instrument that is being developed at the Los Alamos Neutron Science Center (LANSCE) to study neutron capture reactions on short-lived radionuclides. To achieve that, DICER is using an indirect technique based on measuring the neutron transmission through very small samples (0.12–1.2 mm in diameter, $\mu \text{g}$ -mg in mass). The main detection system of DICER consists of two dual photomultiplier (PMT)-based detectors which are sensitive to the scintillation light produced when neutrons interact with 6 Li glass disks. DICER is developing a new collimation system that includes a 0.1-mm collimator. In such small sizes, the need for neutron beam imaging is crucial and necessary to confirm the appropriate alignment between the irradiated sample and the neutron detectors. The large area picosecond photodetector (LAPPD) is a multichannel plate (MCP)-based photodetector, with picosecond-level timing, single-photon detection capabilities, and spatial resolution of the order of 1 mm. Coupling the LAPPD with a 6 Li glass scintillator results in a neutron imaging detector. The first irradiation of the LAPPD at DICER indicated that apart from imaging the beam, the LAPPD can be used as the main neutron detection system. Furthermore, these results were proof of principle measurements demonstrating the capabilities of the beamline, and the challenge with small samples will be addressed in the future. The first efforts and developments, including irradiations of the LAPPD and the first beam images, will be presented.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
Offset Waveguide Transmission Measurements
This report describes measurements to determine transmission losses in S-band (2.60-3.95 GHz) waveguide sections due to misalignment of the sections relative to each other. The experiments were performed in support of the Hydrostar program to determine the feasibility of using deployable waveguide sections in a large space radiometer. The waveguide sections would possibly be hinged and folded for launch, then deployed in space to form long sections of waveguide. Since very low losses are required for radiometer applications, the effects of potential misalignment after deployment of the waveguide sections may be significant. These measurements were performed in the Electromagnetic Properties Measurement Laboratory in the Electromagnetics Research Branch.
Cravey, Robin↗
Neutron Capture and Transmission Measurements and Evaluation of 54 Fe at the RPI LINAC [Slides]
This presentation covers neutron capture and transmission measurements and evaluation of 54 Fe (Iron) at the Rensselaer Polytechnic Insitute (RPI) Linear Accelerator (LINAC). Presentation conclusions find that 54 Fe is near its conclusion, covariance matrix generation is needed for both experiments before data is made available and released (Completion by April 2023). RPI will be conducting a full Resolved Resonance Region (RRR) evaluation following release of data (Completion by September 2023). Additionally, the neutron beam imager shows promise in providing an easy way to align samples in the most intense part of the neutron beam and there will be a new evaluation that will offer improvements in crit safety, shielding, and stellar applications.
07 ISOTOPE AND RADIATION SOURCES↗
Land mobile satellite transmission measurements at 869 MHz: Selected results from the dedicated stratospheric balloon experiment of November 12 and 13, 1984
Satellite transmissions were simulated by placing an 869 MHz and a 1501 MHz transmitter aboard a stratospheric balloon. The balloon was followed on the ground by a van equipped with receivers and data acquisition equipment capable of creating a permanent record of the variations of the received signal amplitude and phase at the two signal frequencies. Results from simulated satellite transmission measurements at 869 MHz are presented. The data show that attenuation by roadside trees can be a limiting factor in systems with a 5 dB fade margin, if 84% availability is not acceptable. In less extreme environments, fading is much less severe. Without fading present, the signal power density function often could be described as Ricean with direct to scattered ratio power ratios of about 100. Phase fluctuations were apparent whenever the signal amplitude fluctuated. The duration of the fades and nonfades tended to cluster close to one wavelength. The power spectrum of both the amplitude and the phase show that most of the fluctuations occur at frequencies below the Doppler shift.
Vogel, W. J.↗
Vertical profiles of aerosol volume from high-spectral-resolution infrared transmission measurements. I. methodology
The wavelength-dependent aerosol extinction in the 800-1250-cm(-1) region has been derived from ATMOS (atmospheric trace molecule spectroscopy) high-spectral-resolution IR transmission measurements.
Dependant optical conatants sulfuric acid radiativ↗
Transmission measurement based on STM observation to detect the penetration depth of low-energy heavy ions in botanic samples
The penetration depth of low-energy heavy ions in botanic samples was detected with a new transmission measurement. In the measurement, highly oriented pyrolytic graphite (HOPG) pieces were placed behind the botanic samples with certain thickness. During the irradiation of heavy ions with energy of tens of keV, the energetic particles transmitted from those samples were received by the HOPG pieces. After irradiation, scanning tunneling microscope (STM) was applied to observe protrusion-like damage induced by these transmitted ions on the surface of the HOPG. The statistical average number density of protrusions and the minimum transmission rate of the low-energy heavy ions can be obtained. The detection efficiency of the new method for low-energy heavy ions was about 0.1-1 and the background in the measurement can be reduced to as low as 1.0 x 10(8) protrusions/cm2. With this method, the penetration depth of the energetic particles was detected to be no less than 60 micrometers in kidney bean slices when the slices were irradiated by 100 keVAr+ ion at the fluence of 5 x 10(16) ions/cm2. c2002 Elsevier Science Ltd. All rights reserved.
DNA Damage↗
Laser Transmission Measurements of Soot Extinction Coefficients in the Exhaust Plume of the X-34 60K-lb Thrust Fastrac Rocket Engine
A four-channel laser transmissometer has been used to probe the soot content of the exhaust plume of the X-34 60k-lb thrust Fastrac rocket engine at NASA's Marshall Space Flight Center. The transmission measurements were made at an axial location approximately equal 1.65 nozzle diameters from the exit plane and are interpreted in terms of homogeneous radial zones to yield extinction coefficients from 0.5-8.4 per meter. The corresponding soot mass density, spatially averaged over the plume cross section, is, for Rayleigh particles, approximately equal 0.7 microgram/cc, and alternative particle distributions are briefly considered. Absolute plume radiance at the laser wavelength (515 nm) is estimated from the data at approximately equal 2,200 K equivalent blackbody temperature, and temporal correlations in emission from several spatial locations are noted.
Dobson, C. C.↗
Laser Transmission Measurements of Soot Extinction Coefficients in the Exhaust Plume of the X-34 60k-lb Thrust Fastrac Rocket Engine
A four-channel laser transmissometer has been used to probe the soot content of the exhaust plume of the X-34 60k-lb thrust Fastrac rocket engine at NASA's Marshall Space Flight Center. The transmission measurements were made at an axial location about equal 1.65 nozzle diameters from the exit plane and are interpreted in terms of homogeneous radial zones to yield extinction coefficients from 0.5-8.4 per meter. The corresponding soot mass density, spatially averaged over the plume cross section, is, for Rayleigh particles, approximately equal to 0.7 micrograms/cubic cm and alternative particle distributions are briefly considered. Absolute plume radiance at the laser wavelength (515 nm) is estimated from the data at approximately equal to 2.200 K equivalent blackbody temperature, and temporal correlations in emission from several spatial locations are noted.
Dobson, C. C.↗