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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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NASA NTRSDate not supplied

The Marshall 100-Meter X-ray Beamline

The Marshall 100-Meter X-ray Beamline is a user facility for x-ray and EUV optics and instrumentation calibration, located at NASA’s Marshall Space Flight Center in Huntsville, Alabama. Also known as the Stray Light Test Facility, the Marshall-100 provides a range of focal plane detectors, x-ray sources, translation stages, cleanrooms, and high-vacuum level capability to the high-energy astrophysics community. Facility time is made available to Astronomy and Physics Research and Analysis (APRA) funded projects and is also available to the broader community upon request made to beamline management. The beamline has successfully been employed in the calibration of larger scope projects such as the Spectrum-Roentgen-Gamma Astronomical Roentgen Telescope X-ray Concentrator (ART-XC) telescope and the Small Explorer (SMEX) class Imaging X-ray Polarimetry Explorer (IXPE) Space Telescope. Additionally, the Marshall-100 is instrumental in supporting testing related to MSFC’s high-angular resolution optics development program.

X-ray Beamline, Test Facility, X-ray Calibration↗
NASA NTRS2016

Ground Calibration of the Astro-H (Hitomi) Soft X-Ray Spectrometer

The Astro-H (Hitomi) Soft X-ray Spectrometer (SXS) was a pioneering imaging x-ray spectrometer with 5 eV energy resolution at 6 keV. The instrument used a microcalorimeter array at the focus of a high-throughput soft x-ray telescope to enable high-resolution non-dispersive spectroscopy in the soft x-ray waveband (0.3-12 keV). We present the suite of ground calibration measurements acquired from 2012-2015, including characterization of the detector system, anti-coincidence detector, optical blocking filters, and filter-wheel filters. The calibration of the 36-pixel silicon thermistor microcalorimeter array includes parameterizations of the energy gain scale and line spread function for each event grade over a range of instrument operating conditions, as well as quantum efficiency measurements. The x-ray transmission of the set of five Al/polyimide thin-film optical blocking filters mounted inside the SXS dewar has been modeled based on measurements at synchrotron beamlines, including with high spectral resolution at the C, N, O, and Al K-edges. In addition, we present the x-ray transmission of the dewar gate valve and of the filters mounted on the SXS filter wheel (external to the dewar), including beryllium, polyimide, and neutral density filters.

detectors↗
NASA NTRS2012

The Astro-H Soft X-Ray Mirror

The Astro-H is led by the Japanese Space Agency (JAXA) in collaboration with many other institutions including the NASA Goddard Space Flight Center. Goddard's contributions include two soft X-ray telescopes (SXTs). The telescopes have an effective area of 562 square cm at 1 keV and 425 square cm at 6 keV with an image quality requirement of 1.7 arc-minutes half power diameter (HPD). The engineering model has demonstrated 1.1 arc-minutes HPD error. The design of the SXT is based on the successful Suzaku mission mirrors with some enhancements to improve the image quality. Two major enhancements are bonding the X-ray mirror foils to alignment bars instead of allowing the mirrors to float, and fabricating alignment bars with grooves within 5 microns of accuracy. An engineering model SXT was recently built and subjected to several tests including vibration, thermal, and X-ray performance in a beamline. Several lessons were learned during this testing that will be incorporated in the flight design. Test results and optical performance are discussed, along with a description of the design of the SXT.

Robinson, David↗
NASA NTRS2018

Analysis of the NGXO Telescope X-Ray Hartmann Data

Next Generation X-Ray Optics (NGXO) team at the Goddard Space Flight Center (GSFC) has been developing a new silicon-based grazing incidence mirror technology for future high resolution x-ray astronomical missions. Recently, the GSFC team completed the construction of first few mirror modules that contain one pair of mirrors. One of the mirror pairs was tested in GSFC 600-m long beamline facility and Panter (Neuried, Germay) 120-m long x-ray beamline facility. Both full aperture x-ray tests, Hartmann tests, and focal plane sweeps were completed. In this paper we present the data analysis process and compare the results from our models to measured x-ray centroid data, x-ray performance data, and out of focus images of the mirror pair.

Spaceborne telescopes↗
NASA NTRS2016

Performance of NICER Flight X-Ray Concentrator

Neutron star Interior Composition ExploreR (NICER) is a NASA instrument to be onboard International Space Station, which is equipped with 56 pairs of an X-ray concentrator (XRC) and a silicon drift detector for high timing observations. The XRC is based on an epoxy replicated thin aluminum foil X-ray mirror, similar to those of Suzaku and ASTRO-H (Hitomi), but only a single stage parabolic grazing incidence optic. Each has a focal length of 1.085 m and a diameter of 105 mm, with 24 confocally aligned parabolic shells. Grazing incident angles to individual shells range from 0.4 to 1.4 deg. The flight 56 XRCs have been completed and successfully delivered to the payload integration. All the XRC was characterized at the NASA/GSFC 100-m X-ray beamline using 1.5 keV X-rays (some of them are also at 4.5 keV). The XRC performance, effective area and point spread function, was measured by a CCD camera and a proportional counter. The average effective area is about 44 sq cm at 1.5 keV and about 18 sq cm at 4.5 keV, which is consistent with a micro-roughness of 0.5 nm from individual shell reflectivity measurements. The XRC focuses about 91% of X-rays into a 2mm aperture at the focal plane, which is the NICER detector window size. Each XRC weighs only 325 g. These performance met the project requirement. In this paper, we will present summary of the flight XRC performance as well as co-alignment results of the 56 XRCs on the flight payload as it is important to estimate the total effective for astronomical observations.

X-ray concentrator↗
NASA NTRS2014

Search for Fluid Inclusions in a Carbonaceous Chondrite Using a New X-Ray Micro-Tomography Technique Combined with FIB Sampling

Early solar system aqueous fluids are preserved in some H chondrites as aqueous fluid inclusions in halite (e.g., [1]). Although potential fluid inclusions are also expected in carbonaceous chondrites [2], they have not been surely confirmed. In order to search for these fluid inclusions, we have developped a new X-ray micro-tomography technique combined with FIB sampling and applied this techniqu to a carbanaceous chondrite. Experimental: A polished thin section of Sutter's Mill meteorite (CM) was observed with an optical microscope and FE-SEM (JEOL 7001F) for chosing mineral grains of carbonates (mainly calcite) and sulfides (FeS and ZnS) 20-50 microns in typical size, which may have aqueous fluid inclusions. Then, a "house" similar to a cube with a roof (20-30 microns in size) is sampled from the mineral grain by using FIB (FEI Quanta 200 3DS). Then, the house was atached to a thin W-needle by FIB and imaged by a SR-based imaging microtomography system with a Fresnel zone plate at beamline BL47XU, SPring-8, Japan. One sample was imaged at two X-ray energies, 7 and 8 keV, to identify mineral phases (dual-enegy microtomography: [3]). The size of voxel (pixel in 3D) was 50-80 nm, which gave the effective spatial resolution of approx. 200 nm. A terrestrial quartz sample with an aqueous fluid inclusion with a bubble was also examined as a test sample by the same method. Results and discussion: A fluid inclusion of 5-8 microns in quartz was clearly identified in a CT image. A bubble of approx. 4 microns was also identified as refraction contrast although the X-ray absorption difference between fluid and bubble is small. Volumes of the fluid and bubble were obtained from the 3D CT images. Fourteen grains of calcite, two grains of iron sulfide and one grain of (Zn,Fe)S were examined. Ten calcite, one iron sulfide and one (Zn,Fe)S grains have inclusions >1 micron in size (the maximum: approx. 5 microns). The shapes are spherical or irregular. Tiny inclusions (<1 micron) are also present in all the grains examined. These results show that mineral grains have more inclusions than expected from 2D observations. The X-ray absorption of the inclusions shows that they are not solid inclusions. No bubbles were observed inside, indicating that we cannot determine whether they are really aqueous fluids or merely voids. One calcite grain has an inclusion approx. 2 microns in size, which seems to have a bubble and a tiny solid daughter crystal inside (three-phase inclusion). As we know the exact 3D position of the inclusion, we will anlyze the inclusion by SIMS after freezing the sample as has been done for a halite sample [3]. The present technique is useful for finding small inclusions not only in carbonaceous chondrites but also for terrestrial materials.

Tsuchiyama, A.↗
NASA NTRS2011

Development of the ASTRO-H Soft X-ray Telescope (SXT): Engineering Model Performance

The X-ray astronomy satellite ASTRO-H, being developed under the collaboration among JAXA, NASA's GSFC and ESA, will have two Soft X-ray Telescopes (SXTs), among other instuments onboard, with a sensitive energy band below 12 keV. One is for an X-ray micorocalorimeter detector and the other for a X-ray CCD detector. The SXT uses a conically approximated Wolter I grazing incidence optic implemented by thin aluminum foil substrates with thickness of 0.152, 0.229, and 0.305 mm. It is similar to the Suzaku XRT, but with larger diameter (45 cm) and longer focal length (5.6 m). Goal of the angular resolution and effective area are 1 arcmin and 390 cm$A2$ at 6 keV, respectively. We made serveral improvements from Suzaku to ASTRO-H, such as thicker substrates, more forming mandrels, thinner epoxy layer for replication, stiffer housings, precise alignment bars, etc. With all these changes, we have fabricated the engineering test unit of the SXT. In this paper, we will discuss all the changes made, their effects, and report X-ray performance of the SXT test unit. An angular resolution of the test unit was measured at new Goddard X-ray calibration facility (100 m X-ray beamline) and was found to be 1.1 arcmin. We will also discuss further improvements toward the flight unit to be delivered to JAXA in 2012.

Okajima, Takashi↗
NASA NTRS2016

Reflectivity Around the Gold L-Edges of X-Ray Reflector of the Soft X-Ray Telescope Onboard ASTRO-H

We report the atomic scattering factor in the 11.215.4 keV for the ASTRO-H Soft X-ray Telescope (SXT) obtained in the ground based measurements. The large effective area of the SXT covers above 10 keV. In fact, the flight data show the spectra of the celestical objects in the hard X-ray band. In order to model the area, the reflectivity measurements in the 11.2-15.4 keV band with the energy pitch of 0.4-0.7 eV were made in the synchrotron beamline Spring-8 BL01B1. We obtained atomic scattering factors f1 and f2 by the curve fitting to the reflectivities of our witness sample. The edges associated with the golds L-I, II, and III transitions are identified, of which the depths are found to be roughly 60 percent shallower than those expected from the Henke's atomic scattering factor.

X-rays↗