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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Stress Intensity Thresholds for Development of Reliable Brittle Materials

Brittle material failure in high consequence systems can appear random and unpredictable at subcritical stresses. Gaps in our understanding of how structural flaws and environmental factors (humidity, temperature) impact fracture propagation need to be addressed to circumvent this issue. A combined experimental and computational approach composed of molecular dynamics (MD) simulations, numerical modeling, and atomic force microscopy (AFM) has been undertaken to identify mechanisms of slow crack growth in silicate glasses. AFM characterization of crack growth as slow as 10 -13 m/s was observed, with some stepwise crack growth. MD simulations have identified the critical role of inelastic relaxation in crack propagation, including evolution of the structure during relaxation. A numerical model for the existence of a stress intensity threshold, a stress intensity below which a fracture will not propagate, was developed. This transferrable model for predicting slow crack growth is being incorporated into mission-based programs.

36 MATERIALS SCIENCE↗
NASA NTRS1992

Mechanical properties of brittle materials

Brittle materials are difficult to tensile test because of gripping problems. They either crack in conventional grips or they are crushed. Furthermore, they may be difficult to make into tensile specimens having, for example, threated ends or donut shapes. To overcome the problem, simple rectangular shapes can be used in bending (i.e., a simple beam) in order to obtain the modulus of rupture and the elastic modulus. The equipment necessary consists of a fixture for supporting the specimens horizontally at two points, these points contact points being rollers which are free to rotate. The force necessary to bend the specimen is produced by a tup attached to the crosshead of an Instron machine. Here, the experimental procedure is explained.

Cornwell, L. R.↗
NASA NTRS1985

Reliability of structural brittle materials

Traditionally, the use of brittle materials has been avoided in demanding structural applications because of their unreliability. They have been used however, due to other desirable properties, in nonstructural applications or where the mechanical load is minimal. The most common method utilized today for the design approach of brittle materials is the probabilistic, which takes into consideration the flaw and stress distribution within the brittle material. It does not take into consideration the fracture mechanics effect of strength degradation while aging under a mechanical load. This project will combine the two methods, probabilistic and fracture mechanics, into a more reliable design method for brittle materials.

Hall, W. B.↗
NASA NTRS1989

Reliability-based failure analysis of brittle materials

The reliability of brittle materials under a generalized state of stress is analyzed using the Batdorf model. The model is modified to include the reduction in shear due to the effect of the compressive stress on the microscopic crack faces. The combined effect of both surface and volume flaws is included. Due to the nature of fracture of brittle materials under compressive loading, the component is modeled as a series system in order to establish bounds on the probability of failure. A computer program was written to determine the probability of failure employing data from a finite element analysis. The analysis showed that for tensile loading a single crack will be the cause of total failure but under compressive loading a series of microscopic cracks must join together to form a dominant crack.

Powers, Lynn M.↗
NASA NTRS1988

Fracture technology for brittle materials

Ceramics materials have the potential for use in high-temperature, fuel-efficient engines. However, because these materials are brittle, their fracture characteristics must be well documented prior to their application. Thus Lewis is working to understand the fracture and strength properties of brittle ceramic and ceramic matrix materials. An understanding of fracture properties aids both designers who are attempting to design high-temperature structures and materials scientists who seek to design more temperature-resistant materials. Both analytical and experimental approaches to fracture analysis are being taken. Methods for testing fracture toughness, crack growth resistance, and strength are being developed. The failure mechanisms at both room and elevated temperatures are also being investigated. Such investigations aid materials scientists in developing better high-temperature materials. Of concern is the anisotropy of ceramic materials and the experimental verification of ceramic design codes that will allow brittle material behavior to be accurately predicted at high temperature.

Salem, Jonathan A.↗
DOE OSTI2026

C‐Cracking of Brittle‐Material Spheres From Eccentric Hertzian Contact

Contact of brittle-material spheres can occur while they are manufactured, handled, or used in operation as roller elements or in deformably processed composite material. Statistically, the directional contact between two spheres will nearly always be oblique or eccentric in an unconfined and mobile sphere population. Although analyses of oblique contact exist, the portrayal of its maximum (tensile) first principal stress ( S 1 ) field is lacking. This information is needed for improved judgment of the prospect of crack initiation. Given these, the S 1 due to eccentric contact and subsequent crack initiation was analyzed using finite element analysis (FEA) and corroborative demonstration of c-crack creation. The FEA shows that an asymmetric S 1 field is created about the contact patch and is caused by superimposed shear intrinsic to eccentric contact. A crack will initiate if the maximum S 1 exceeds the material's tensile strength, and its field will cause the crack to propagate and arrest to form a C-shaped crack, or c-crack. C-crack initiation trends with lower applied forces, with greater amount of contact eccentricity, higher coefficient of friction, and smaller spherical radius. Finally, these metrics deserve recognition, especially when c-cracked brittle-material spheres are used in a system whose functionality or reliability is potentially compromised by the c-cracks.

Hertzian contact↗
DOE OSTI2021

StressNet - Deep learning to predict stress with fracture propagation in brittle materials

Abstract Catastrophic failure in brittle materials is often due to the rapid growth and coalescence of cracks aided by high internal stresses. Hence, accurate prediction of maximum internal stress is critical to predicting time to failure and improving the fracture resistance and reliability of materials. Existing high-fidelity methods, such as the Finite-Discrete Element Model (FDEM), are limited by their high computational cost. Therefore, to reduce computational cost while preserving accuracy, a deep learning model, StressNet, is proposed to predict the entire sequence of maximum internal stress based on fracture propagation and the initial stress data. More specifically, the Temporal Independent Convolutional Neural Network (TI-CNN) is designed to capture the spatial features of fractures like fracture path and spall regions, and the Bidirectional Long Short-term Memory (Bi-LSTM) Network is adapted to capture the temporal features. By fusing these features, the evolution in time of the maximum internal stress can be accurately predicted. Moreover, an adaptive loss function is designed by dynamically integrating the Mean Squared Error (MSE) and the Mean Absolute Percentage Error (MAPE), to reflect the fluctuations in maximum internal stress. After training, the proposed model is able to compute accurate multi-step predictions of maximum internal stress in approximately 20 seconds, as compared to the FDEM run time of 4 h, with an average MAPE of 2% relative to test data.

36 MATERIALS SCIENCE↗
DOE OSTI2024

Spherical Indentation and Implementation of S 3 /P for yield stress determination of brittle materials

Here, a mathematically transparent and robust experimental method has been developed to estimate the yield stress of brittle materials through the analysis of depth-sensing spherical indentation. Employing Hertzian contact mechanics, an elastically invariant ratio based on the simple equation S 3 / P = 6RE r 2 , (where S and P are contact stiffness and indentation load, respectively) has been derived that enables more accurate and confident determination of the transition from elastic to inelastic deformation; a transition that the yield stress dictates and represents. Using two diamond spheres with radii of 3.2 and 8.6 μm, the indentation test method and analyses are applied to two vitreous silicates: Corning's HPFS 7980® fused silica and Vitro's Starphire® soda lime silicate. The estimated yield strengths are 8.15 GPa ± 2.5% for the fused silica and 6.1 GPa ± 3.3% for the soda-lime silicate, and both were independent of indenter radius. Verification of this new experimental method is demonstrated with an as-drawn titanium by showing equivalence of measured yield stress by its spherical indentation and that from uniaxial compression testing. This method will enable easier and more confident estimation of yield stress in brittle materials - a property that historically has been elusive to measure for these materials using common laboratory mechanical test methods.

36 MATERIALS SCIENCE↗
NASA NTRS1992

A combined analytical-experimental tensile test technique for brittle materials

A semiconventional tensile test technique is developed for impact ices and other brittle materials. Accurate results have been obtained on ultimate strength and modulus of elasticity in a refrigerated ice test. It is noted that the technique can be used to determine the physical properties of impact ices accreted inside icing wind tunnels or other brittle materials.

Chu, M. L.↗
DOE OSTI2023

A robust interface finite element formulation for modeling brittle material failure problems

Abstract Failure of many brittle materials and structures can be modeled using interface‐oriented finite elements combined with intrinsic cohesive zone models. The discontinuous Galerkin (DG) finite element method provides an innovative framework for modeling brittle crack propagation with zero‐thickness interface elements, which can accommodate extrinsic cohesive laws to avoid the artificial compliance required in intrinsic cohesive models. However, robust formulations and implementations of DG methods are critical in alleviating the well‐known convergence issues for both crack nucleation and propagation with reduced instability. This paper presents a robust interface element formulation by modifying the incomplete interior penalty Galerkin (IIPG) method, which successfully avoids the initial element interface penetration across elements that occurs prior to crack nucleation, and thereby greatly reduces the instability issue as cracks open. We further verified and validated our implementation by using a bar tension test and a beam fracturing benchmark. The robustness of our proposed interface element method was demonstrated by a micromechanics fiber/matrix debonding problem with 64 fibers embedded in a bulk matrix.

Liu, Ruijie↗
NASA NTRS1976

Apparatus for measuring internal friction Q factors in brittle materials

A flexural analog of the torsion pendulum for measuring the Young's modulus and the internal friction Q factor of brittle materials has been developed for Q greater than 10 to the 3rd measurements at a zero static stress and at 10 to the -7th strains of brittle materials in the Hz frequency range. The present design was motivated by the desire to measure Q in fragile lunar return samples at zero static stress to shed light on the anomalously low attenuation of seismic waves on the moon. The use of the apparatus is demonstrated with data on fused silica and on a terrestrial analog of lunar basalt.

Tittmann, B. R.↗
NASA NTRS2002

Reliability Analysis of Brittle Material Structures - Including MEMS(?) - With the CARES/Life Program

Brittle materials are being used, or considered, for a wide variety of high tech applications that operate in harsh environments, including static and rotating turbine parts. thermal protection systems, dental prosthetics, fuel cells, oxygen transport membranes, radomes, and MEMS. Designing components to sustain repeated load without fracturing while using the minimum amount of material requires the use of a probabilistic design methodology. The CARES/Life code provides a general-purpose analysis tool that predicts the probability of failure of a ceramic component as a function of its time in service. For this presentation an interview of the CARES/Life program will be provided. Emphasis will be placed on describing the latest enhancements to the code for reliability analysis with time varying loads and temperatures (fully transient reliability analysis). Also, early efforts in investigating the validity of using Weibull statistics, the basis of the CARES/Life program, to characterize the strength of MEMS structures will be described as as well as the version of CARES/Life for MEMS (CARES/MEMS) being prepared which incorporates single crystal and edge flaw reliability analysis capability. It is hoped this talk will open a dialog for potential collaboration in the area of MEMS testing and life prediction.

Nemeth, Noel N.↗
NASA NTRS2004

Ultrasonic Apparatus for Pulverizing Brittle Material

The figure depicts an apparatus that pulverizes brittle material by means of a combination of ultrasonic and sonic vibration, hammering, and abrasion. The basic design of the apparatus could be specialized to be a portable version for use by a geologist in collecting powdered rock samples for analysis in the field or in a laboratory. Alternatively, a larger benchtop version could be designed for milling and mixing of precursor powders for such purposes as synthesis of ceramic and other polycrystalline materials or preparing powder samples for x-ray diffraction or x-ray fluorescence measurements to determine crystalline structures and compositions. Among the most attractive characteristics of this apparatus are its light weight and the ability to function without need for a large preload or a large power supply: It has been estimated that a portable version could have a mass <0.5 kg, would consume less than 1 W h of energy in milling a 1-cm3 volume of rock, and could operate at a preload <10 N. The basic design and principle of operation of this apparatus are similar to those of other apparatuses described in a series of prior NASA Tech Briefs articles, the two most relevant being Ultrasonic/ Sonic Drill/Corers With Integrated Sensors (NPO-20856), Vol. 25, No. 1 (January 2001), page 38 and Ultrasonic/ Sonic Mechanisms for Deep Drilling and Coring (NPO-30291), Vol. 27, No. 9 (September 2003), page 65. As before, vibrations are excited by means of a piezoelectric actuator, an ultrasonic horn, and a mass that is free to move axially over a limited range. As before, the ultrasonic harmonic motion of the horn drives the free-mass in a combination of ultrasonic harmonic and lower-frequency hammering motion. In this case, the free-mass is confined within a hollow cylinder that serves as a crushing chamber, and the free-mass serves as a crushing or milling tool. The hammering of the free-mass against a material sample at the lower end of the chamber grinds the sample into powder in a relatively short time. The restriction of the free-mass to axial motion only makes the grinding very efficient. The free-mass can be fabricated to have teeth on its lower face to enhance the grinding effect. Optionally, there can be a hole at the bottom of the chamber covered with a sieve to tailor the size distribution of the powder leaving the crushing chamber.

Sherrit, Stewart↗
NASA NTRS1999

Slow Crack Growth Analysis of Brittle Materials with Finite Thickness Subjected to Constant Stress-Rate Flexural Loading

A two-dimensional, numerical analysis of slow crack growth (SCG) was performed for brittle materials with finite thickness subjected to constant stress-rate ("dynamic fatigue") loading in flexure. The numerical solution showed that the conventional, simple, one-dimensional analytical solution can be used with a maximum error of about 5% in determining the SCG parameters of a brittle material with the conditions of a normalized thickness (a ratio of specimen thickness to initial crack size) T > 3.3 and of a SCG parameter n > 10. The change in crack shape from semicircular to elliptical configurations was significant particularly at both low stress rate and low T, attributed to predominant difference in stress intensity factor along the crack front. The numerical solution of SCG parameters was supported within the experimental range by the data obtained from constant stress-rate flexural testing for soda-lime glass microslides at ambient temperature.

Chio, S. R.↗
NASA NTRS1978

A statistical, micromechanical theory of the compressive strength of brittle materials

A general theory of the compressive strength of brittle materials is presented. This theory proposes that failure is brought about by structural weakening from accumulated crack damage which increases with the stress level. The statistics of the flaw distribution and the mechanism of crack initiation and extension are important. A sample calculation using the theory is given to demonstrate its application

Adams, M.↗
DOE OSTI2023

A probabilistic-phase field model for the fracture of brittle materials

Abstract We develop a computational method to determine the failure probability of brittle materials under general mechanical loading conditions. The method is a combination of two parts: (1) numerical simulations of materials with multiple cracks using phase field theory, where the complete fracture process is viewed as ‘damage percolation’ along critical paths or clusters of cracks, rather than the traditional weak-link failure mechanism of Weibull, and (2) an extension of the Batdorf statistical theory of fracture to finite domains, where it is implemented within the finite element framework. The results of phase-field simulations at the ‘percolation threshold’ are used as failure data in the Batdorf theory to determine the overall probability of failure. The input to this approach is the size distribution of cracks in a pristine material. An example is shown, where alumina samples that were previously tested by Abe and coworkers (Abeet al2003J. Am. Ceram. Soc.861019–21) in four-point loading are compared to the results of our numerical simulations. The approach developed here has the advantage of being extendable to more complex thermomechanical loading.

Materials Science↗