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Results for “differential analysis”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
NASA NTRS1972

Comparison of neutron spectra measured with three sizes of organic liquid scintillators using differentiation analysis

Proton recoil distributions were obtained by using organic liquid scintillators of different size. The measured distributions are converted to neutron spectra by differentiation analysis for comparison to the unfolded spectra of the largest scintillator. The approximations involved in the differentiation analysis are indicated to have small effects on the precision of neutron spectra measured with the smaller scintillators but introduce significant error for the largest scintillator. In the case of the smallest cylindrical scintillator, nominally 1.2 by 1.3 cm, the efficiency is shown to be insensitive to multiple scattering and to the angular distribution to the incident flux. These characteristics of the smaller scintillator make possible its use to measure scalar flux spectra within media high efficiency is not required.

Shook, D. F.↗
NASA NTRS1974

Differential analysis for the turbulent boundary layer on a compressor blade element (including boundary-layer separation)

A two-dimensional differential analysis is developed to approximate the turbulent boundary layer on a compressor blade element with strong adverse pressure gradients, including the separated region with reverse flow. The predicted turbulent boundary layer thicknesses and velocity profiles are in good agreement with experimental data for a cascade blade, even in the separated region.

Schmidt, J. F.↗
NASA NTRS1991

Differential thermal analysis of lunar soil simulant

Differential thermal analysis of a lunar soil simulant, 'Minnesota Lunar Simulant-1' (MLS-1) was performed. The MLS-1 was tested in as-received form (in glass form) and with another silica. The silica addition was seen to depress nucleation events which lead to a better glass former.

Tucker, D.↗
NASA NTRS1995

Search for life on Mars: Evaluation of techniques

An important question for exobiology is, did life evolve on Mars? To answer this question, experiments must be conducted on the martian surface. Given current mission constraints on mass, power, and volume, these experiments can only be performed using proposed analytical techniques such as: electron microscopy, X-ray fluorescence, X-ray diffraction, a-proton backscatter, g-ray spectrometry, differential thermal analysis, differential scanning calorimetry, pyrolysis gas chromatography, mass spectrometry, and specific element detectors. Using prepared test samples consisting of 1% organic matter (bovine serum albumin) in palagonite and a mixture of palagonite, clays, iron oxides, and evaporites, it was determined that a combination of X-ray diffraction and differential thermal analysis coupled with gas chromatography provides the best insight into the chemistry, mineralogy, and geological history of the samples.

Schwartz, D. E.↗
NASA NTRS1974

Post-flight differential correction analysis using Vinti's spheroidal method for the small astronomy satellite orbit

The results of an intensive analysis of a differential orbit improvement method utilizing observational data for a 550-kilometer altitude, near-circular, near-equatorial satellite orbit are presented. Observations of the Small Astronomy Satellite (SAS-1) are in the form of direction cosines as measured at two ground interferometer tracking stations near the Equator during the first 22 orbital revolutions (approximately 37 hours) after launch of the spacecraft. Numerical results, in both tabular and graphical form, are displayed for numerous iterated fittings of various observational arcs by differential correction of the orbital elements. Parameters varied in these comparative cases include the time duration of the observational data block, the number of pairs of direction cosine data and the number of tracking station passes included in the solution, the distribution of such passes between the two available tracking stations, and the acceptance criterion for the observational residuals in the least squares fitting procedure. It was found that three observational pairs of direction cosine data, the minimum number possible for a uniquely determined solution in theory, are sufficient to promote covergence to an accurate solution, if properly selected.

Walden, H.↗
NASA NTRS1974

Recent results on parametric analysis of differential Omega error

Previous tests of the differential Omega concept and an analysis of the characteristics of VLF propagation make it possible to delineate various factors which might contribute to the variation of errors in phase measurements at an Omega receiver site. An experimental investigation is conducted to determine the effect of each of a number of parameters on differential Omega accuracy and to develop prediction equations. The differential Omega error form is considered and preliminary results are presented of the regression analysis used to study differential error.

Baxa, E. G., Jr.↗
NASA NTRS1973

Thermomechanical behavior of a polynorbornadiene

A high-temperature linear amorphous hydrocarbon polymer synthesized cationically from 2,5-norbornadiene was studied thermomechanically with respect to physical transitions and stability in nitrogen. The glass transition temperature was determined to be 320 C (at less than 1 cps), which is probably the highest known for a linear hydrocarbon addition polymer. The thermomechanical technique of torsional braid analysis, together with thermogravimetric analysis, differential thermal analysis, infrared analysis, and solubility studies, was used to investigate the sequential events of the glass transition and degradation. The polymer is of particular interest since it is a high-temperature plastic which in the bulk form would probably need to be processed at high speeds in the vicinity of the glass transition temperature in an inert atmosphere. The presence of tertiary hydrogen atoms should render it amenable to degradation by the earth's environment.

Roller, M. B.↗
NASA NTRS1972

Fast differential thermal analysis.

A study is conducted of the limits of time-dependent differential thermal analysis (DTA). Applications of DTA to the hysteresis phenomena of glasses are also reported. The computation of DTA sample temperatures is discussed, giving attention to feasible heating rates, transient effects to be measured, and the simulation of DTA responses to changes in thermal diffusivity similar to hysteresis phenomena in glasses. The reproducibility of temperature recording is checked with zone-refined organic chemicals.

Wunderlich, B.↗
NASA NTRS1989

A study of microstructural characteristics and differential thermal analysis of Ni-based superalloys

The objective of this work is to correlate the mechanical properties of the Ni-based superalloy MAR M246(Hf) used in the Space Shuttle Main Engine with its structural characteristics by systematic study of optical photomicrographs and differential thermal analysis. The authors developed a method of predicting the liquidus and solidus temperature of various nickel based superalloys (MAR-M247, Waspaloy, Udimet-41, polycrystalline and single crystals of CMSX-2 and CMSX-3) and comparing the predictions with the experimental differential thermal analysis (DTA) curves using Perkin-Elmer DTA 1700. The method of predicting these temperatures is based on the additive effect of the components dissolved in nickel. The results were compared with the experimental values.

Aggarwal, M. D.↗
NASA NTRS1985

Theoretical interpretation of thermal arrest data from differential thermal analysis measurements

A theory was developed to interpret the thermal arrest data of HgCdTe system from differential thermal analysis measurements. A nonlinear regression program is used to model fit the data. The purpose is to obtain a set of parameters which will give the information about average radiation coefficient, latent heat of fussion, and specific heat of the HgCdTe system at various compositions. The liquidus and solidus at various compositions are also obtained. The heat radiation from the furnace, heat radiation from the system, heat capacity from both the system and the quartz tube and the heat of fusion of the system are considered, however, it neglects heat transfer through conduction and convection.

Wang, J. C.↗
NASA NTRS1990

Determining the nucleation rate curve for lithium disilicate glass by differential thermal analysis

The crystallization of lithium disilicate (Li2O+2SiO2) glass nucleated at various temperatures was studied by differential thermal analysis (DTA). A plot of the DTA crystallization peak height versus nucleation temperature closely resembles the classical nucleation rate curve for lithium disilicate glass whose maximum is at 453 C. The glass becomes saturated with internal nuclei when heated at 453 C for 10 h. The activation energy for crystallization and the heat of crystallization are independent of the concentration of nuclei and are 249 + or - 10 and 67 + or - 3 kJ/mol, respectively. The Avrami exponent, n, depends strongly on the concentration of nuclei in the glass.

Ray, Chandra S.↗