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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2017

Failure Diameter Resolution Study

Previously the SURFplus reactive burn model was calibrated for the TATB based explosive PBX 9502. The calibration was based on fitting Pop plot data, the failure diameter and the limiting detonation speed, and curvature effect data for small curvature. The model failure diameter is determined utilizing 2-D simulations of an unconfined rate stick to find the minimum diameter for which a detonation wave propagates. Here we examine the effect of mesh resolution on an unconfined rate stick with a diameter (10mm) slightly greater than the measured failure diameter (8 to 9 mm).

45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEF↗
DOE OSTI2019

PBX 9502 Failure Diameter: Addendum

In previous reports, the SURFplus reactive burn model was used to study a propagating detonation wave for PBX 9502 in an unconfined rate stick just above the failure diameter. Simulations showed that the sonic boundary condition at the HE interface leads to a boundary layer. Here we provide additional details on the steady-state flow with emphasis on the boundary layer. This confirms the previous conclusion that within the boundary layer the lead shock, which initiates the hot-spot reaction, is largely supported by transverse energy flow in the reaction zone from the interior towards the boundary. Consequently, the reactive wave along a boundary layer streamline does not correspond to a 1-D detonation wave in the sense of detonation shock dynamics; i.e. , the lead shock which initiates the reaction is not driven by the reaction energy along the streamline.

45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEF↗
DOE OSTI2017

SURFplus Model Calibration for PBX 9502

The SURFplus reactive burn model is calibrated for the TATB based explosive PBX 9502 at three initial temperatures; hot (75 C), ambient (23 C) and cold (-55 C). The CJ state depends on the initial temperature due to the variation in the initial density and initial specific energy of the PBX reactants. For the reactants, a porosity model for full density TATB is used. This allows the initial PBX density to be set to its measured value even though the coeffcient of thermal expansion for the TATB and the PBX differ. The PBX products EOS is taken as independent of the initial PBX state. The initial temperature also affects the sensitivity to shock initiation. The model rate parameters are calibrated to Pop plot data, the failure diameter, the limiting detonation speed just above the failure diameters, and curvature effect data for small curvature.

45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEF↗
NASA NTRS1980

The NOL Gap Test: Past, present, and future

A brief history of the development of the gap test is presented with emphasis on accumulated knowledge of how best to use it as a tool to assess relative shock sensitivity of explosives and propellants. Present information about the detonation process in build-up, steady state, and failure is used to show that failure diameter cannot give the desired shock sensitivity assessment. Suggestions are made for improving the test to an experiment. The use of spherical donors, water as attenuator, and camera instrumentation are briefly discussed.

Jacobs, S. J.↗
DOE OSTI2026

Hoop Tensile Failure Stress of 500 µm-Diameter Ceramic Spheres

The tensile failure stress of a brittle-material sphere is important to the survival of the sphere itself but is particularly relevant to systems that employ such spheres for applications in which the sphere exterior is subjected to tension during system fabrication or operation. That maximum hoop or tangential stress can be measured by diametrally compressing a C-sphere specimen directly machined from such spheres. This combination of specimen geometry and test method was conceived at Oak Ridge National Laboratory around 20 years ago. Although the C-sphere geometry has been tested with larger spheres, the ease and efficacy of its testing are unknown for submillimeter sphere diameters. To consider this, C-sphere specimens were machined from yttria-stabilized zirconia (YSZ) spheres of ∼500 µm diameter. The maximum (hoop or tangential) tensile stress was determined as a function of compressive failure force and specimen dimensions using finite element analysis. Companion effective area and volume as a function of Weibull modulus were computed. Hoop tensile failure stresses were then measured and fractography conducted to examine flaw type and location and to estimate the mirror constant of this YSZ grade. This novel study demonstrates that hoop tensile failure stress can be determined with sub-millimeter brittle-material spheres.

Delia, Daniel [ORNL] (ORCID:0000000209023239)↗
NASA NTRS1990

Analysis and experiments for composite laminates with holes and subjected to 4-point bending

Analytical and experimental results are presented for composite laminates with a hole and subjected to four-point bending. A finite-plate analysis is used to predict moment and strain distributions for six-layer quasi-isotropic laminates and transverse-ply laminates. Experimental data are compared with the analytical results. Experimental and analytical strain results show good agreement for the quasi-isotropic laminates. Failure of the two types of composite laminates is described, and failure strain results are presented as a function of normalized hole diameter. The failure results suggest that the initial failure mechanism for laminates subjected to four-point bending are similar to the initial failure mechanisms for corresponding laminates subjected to uniaxial inplane loadings.

Shuart, M. J.↗
DOE OSTI2023

Size effects in 3D–printed polymer–derived, zirconium diboride–reinforced ceramic composites

Preceramic polymers are of interest for use in many manufacturing techniques such as injection molding, ceramic fiber infiltration, and additive manufacturing. However, off-gassing of low molecular weight oligomers occurs when these polymers cure, potentially leading to porosity in the cured part. Here to study how porosity and strength are affected by the size of the printed part, and the presence of a high surface area nano-scale filler, polycarbosilane (PCS) microrods of varying diameter were fabricated via direct ink writing (DIW), an additive manufacturing technique, with two ink formulations containing either zirconium diboride (ZrB 2 ) alone, or ZrB 2 and fumed alumina (FA). Sets of microrods were printed in a range of sizes by using print nozzles of 450, 634, 979, 1 346, or 1 702 μm in diameter, which were thermally cured, pyrolyzed to form ceramic composite microrods, and tested in 3-pt flexure. Porosity increased with increasing diameter, while failure strength decreased. For a given nozzle size, the microrods containing FA displayed lower porosity and higher strength (up to ~500 MPa) compared to the microrods containing only ZrB 2 . Weibull strength analysis was performed on each group of microrods and shows that the addition of FA increased Weibull modulus from 4.63 ± 1.56 to 9.35 ± 0.601. In conjunction with optical microscopy, this analysis indicates two distinct flaw populations in the printed materials, porosity which arises during the curing step and cracking which arises during pyrolysis of the larger specimens.

36 MATERIALS SCIENCE↗
NASA NTRS1985

Ductility in rapidly solidified NiAl

An attempt is made to refine the grain structure of equiatomic NiAl by means of rapid solidification processing, and to examine the effect of small grain size on room temperature ductility. Free melt spinning was used to produce the rapidly solidified material. Room temperature bend testing of both as-spun and heat-treated NiAl ribbon was conducted by free bending the ribbon around a mandrel of successively smaller diameter until failure occurred. Room-temperature plastic deformation was exhibited both before and after a 1-h heat treatment at 1000 C. Heat treatment increased the observed ductility.

Gaydosh, D. J.↗
NASA NTRS1984

Effect of Impact Damage and Open Holes on the Compression Strength of Tough Resin/high Strain Fiber Laminates

Tests to assess the performance of composite structures damaged by impact or containing local discontinuities such as cutouts are discussed. In particular, two plate specimen test configurations which were developed to define the serverity of compression strength reduction are described; one for impact damage and the other open hole specimens. The test technique for impact specimens involves damaging the plate at selected energies, measuring the size of damage by ultrasonic C-scan techniques and measuring the residual strength in a compression load test. Open-hole specimen compression tests are conducted for several different hole diameters and the failure strain and load and mode of failure recorded. The plate specimen used in these tests is designed with length, width, thickness and laminate stiffness to ensure that overall plate buckling is not responsible for initiating failure.

Williams, J. G.↗
NASA NTRS1978

Interior morphology of fresh Martian craters - The effects of target characteristics

The interior morphology of 183 fresh Martian craters observed on Viking imagery was studied. Freshness was determined by rim sharpness and continuity according to the scheme used to classify lunar and Mercurian craters. Results indicate that central-peak and wall degradation features are more common than previously thought. Central peaks are observed in craters as small as 2 km in diameter and in nearly all fresh craters with diameters greater than 10 km. Scallops or terraces are found to occur in all craters with diameters greater than 20 km, and wall slumping seems common in craters from 5 to 10 km in diameter. The ratio of crater diameter to crater floor diameter is significantly larger than for lunar craters. Central peaks and pits are more frequent in craters formed in cratered terrain than in those formed on plains; wall failure occurs at smaller diameters in plains craters. It is suggested that these peculiarities of crater interior morphologies may be due to a subsurface volatile layer. The influence of target variations on the interior morphologies observed in fresh craters was studied. Preliminary results indicate well-defined effects due to target differences.

Wood, C. A.↗
DOE OSTI2021

Topographical shifts in fine root lifespan in a mixed, mesic temperate forest

Root lifespan, often is estimated in landscape- and ecosystem-level carbon models using linear approximations. In water manipulation experiments, fine root lifespan can vary with soil water content. Soil water content is generally structured by complex topography, which is largely unaccounted for in landscape- and ecosystem-scale carbon models. Topography governs the range of soil water content experienced by roots which may impact their lifespan. We hypothesized that root lifespan varied nonlinearly across a temperate, mesic, forested catchment due to differences in soil water content associated with topographic position. We expected regions of the landscape that were too wet or too dry would have soils that were not optimal for roots and thus result in shorter root lifespans. Specifically, we hypothesized that root lifespan would be longest in areas that consistently had soil water content in the middle of the soil water content spectrum, while in soils at either very low or very high soil water content, root lifespan would be relatively short. We tested this hypothesis by collecting and analyzing two years of minirhizotron and soil moisture data in plots widely distributed in the Shale Hills catchment of the Susquehanna-Shale Hills Critical Zone Observatory in Pennsylvania. We found that fine root lifespans were longer in traditionally wetter topographic regions, but detected no short term (biweekly) effect of soil moisture on root lifespan. Additionally, depth in soil, soil series, slope face orientation, and season of birth strongly affected root lifespans across the catchment. In contrast, lifespan was unaffected by root diameter or mycorrhizal association. Failure to account for these variables could result in erroneous estimates of fine root lifespan and, consequentially, carbon flux in temperate forested regions.

54 ENVIRONMENTAL SCIENCES↗
NASA NTRS1973

Buckling tests of two 4.6-meter-diameter, magnesium ring-stiffened conical shells loaded under external pressure

Two ring-stiffened magnesium conical shells with a 120 deg apex angle and a 4.6-meter diameter were loaded to failure by a uniform external pressure. The cones differed from one another only in the number of internal stiffening rings. Test specimen details, test procedure, and test results are discussed. Both buckling and prebuckling data are compared with appropriate theoretical predictions. Measured strains in skin and rings agreed well with theoretical predictions. Extensive imperfection measurements were made and reported on both cones in the as fabricated condition.

Anderson, J. K.↗
NASA NTRS1975

Buckling tests of three 4.6 meter diameter aluminum honeycomb sandwich conical shells loaded under external pressure

Three aluminum honeycomb sandwich conical shells with a 120 apex angle and a 4.6-m (15.0-ft) base diameter were loaded to failure by a uniform external pressure. The cones differed from one another only in the thickness of their respective face sheets. Test specimen details, test procedure, and test results are discussed. Both buckling and prebuckling data are compared with appropriate theoretical predictions, and good agreement was obtained between test and theory. Extensive imperfection measurements were made and reported on the three cones in the as fabricated condition.

Anderson, J. K.↗
DOE OSTI2023

Guidelines for predicting stress in cemented doublets undergoing temperature change

This work explores quick predictive methods for calculating potentially risky stresses and deflections in cemented doublets experiencing temperature change that agree well with finite element analysis. There are three failure modes of interest: cohesive failure of the adhesive, delamination (surface bond failure or debonding), and glass fracture. Adhesive theory, confirmed by finite element analysis, predicts stress singularities that complicate interpretation of the stress calculations. The presence of a stress singularity indicates the breakdown of linear elastic assumptions, but damage initiation and stress singularities are related. The authors find that geometry details near a bond edge can exacerbate or minimize damage initiation and stress concentrations. Because the interpretation of the stress results is complicated, the authors investigated predicted stresses in doublets that have been successfully tested between -40 and 85 °C. This study found that the product (ΔT ∙ Δα) should be less than 189 ppm, where ΔT is the temperature excursion and Δα is the difference in glass coefficient of thermal expansion. If the product (ΔT ∙ Δα) is equal to or greater than 189 ppm, further analysis and testing is warranted. But the authors also show that the fabrication process can significantly influence stress failure, particularly with large diameter doublets.

47 OTHER INSTRUMENTATION↗
DOE OSTI2023

Guidelines for predicting stress in cemented doublets undergoing temperature change

This work explores quick predictive methods for calculating potentially risky stresses and deflections in cemented doublets experiencing temperature change that agree well with finite element analysis. There are three failure modes of interest: cohesive failure of the adhesive, delamination (surface bond failure or debonding), and glass fracture. Adhesive theory, confirmed by finite element analysis, predicts stress singularities that complicate interpretation of the stress calculations. The presence of a stress singularity indicates the breakdown of linear elastic assumptions, but damage initiation and stress singularities are related. The authors find that geometry details near a bond edge can exacerbate or minimize damage initiation and stress concentrations. Because the interpretation of the stress results is complicated, the authors investigated predicted stresses in doublets that have been successfully tested between -40 and 85 °C. This study found that the product (∆T ∙ ∆α) should be less than 189 ppm, where ∆T is the temperature excursion and ∆α is the difference in glass coefficient of thermal expansion. If the product (∆T ∙ ∆α) is equal to or greater than 189 ppm, further analysis and testing is warranted. But the authors also show that the fabrication process can significantly influence stress failure, particularly with large diameter doublets

42 ENGINEERING↗
NASA NTRS1981

The compressive failure of graphite/epoxy plates with circular holes

The results of an experimental investigation of the compressive behavior of T300/5203 graphite/epoxy laminated plates measuring 127.0 by 254.0 mm and containing circular holes ranging to 38.1 mm are reported. Two thicknesses, 24-ply and 48-ply, were chosen to differentiate between stability failures resulting from buckling and strength failures caused by the hole. Both quasi-isotropic and orthotropic stacking arrangements were used. The critical buckling load of the 24-ply panels was independent of hole size. Bifurcation occurred in the two half-wave mode longitudinally and one half-wave mode laterally in the quasi-isotropic panels. For the orthotropic 24-ply panels, bifurcation began in the one half-wave mode shape in each direction, but changed to the two half-wave mode before failure. Consistent post-buckling strength was exhibited by both laminated configurations. Panels with hole diameters below 3.175 mm displayed buckling before failure; those with holes larger than 6.35 mm experienced material failure around the hole before panel collapse.

Knauss, J. F.↗