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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records

Solid-propellant rocket motor ballistic performance variation analyses

Results are presented of research aimed at improving the assessment of off-nominal internal ballistic performance including tailoff and thrust imbalance of two large solid-rocket motors (SRMs) firing in parallel. Previous analyses using the Monte Carlo technique were refined to permit evaluation of the effects of radial and circumferential propellant temperature gradients. Sample evaluations of the effect of the temperature gradients are presented. A separate theoretical investigation of the effect of strain rate on the burning rate of propellant indicates that the thermoelastic coupling may cause substantial variations in burning rate during highly transient operating conditions. The Monte Carlo approach was also modified to permit the effects on performance of variation in the characteristics between lots of propellants and other materials to be evaluated. This permits the variabilities for the total SRM population to be determined. A sample case shows, however, that the effect of these between-lot variations on thrust imbalances within pairs of SRMs is minor in compariosn to the effect of the within-lot variations. The revised Monte Carlo and design analysis computer programs along with instructions including format requirements for preparation of input data and illustrative examples are presented.

Sforzini, R. H.↗

Discrimination of hydrothermal alteration mineral assemblages at Virginia City, Nevada, using the airborne imaging spectrometer

The purpose of this study is to use airborne imaging spectrometer data to discriminate hydrothermal alteration mineral assemblages associated with silver and gold mineralization at Virginia City, NV. The data is corrected for vertical striping and sample gradients, and converted to flat-field logarithmic residuals. Log residual spectra from areas known to be altered are compared to field spectra for kaolinitic, illitic, sericitic, and propylitic alteration types. The areal distributions of these alteration types are estimated using a spectral matching technique. Both visual examination of spectra and the matching techniques are effective in distinguishing kaolinitic, illitic, and propylitic alteration types from each other. However, illitic and sericitic alteration cannot be separated using these techniques because the spectra of illite and sericite are very similar. A principal components analysis of 14 channels in the 2.14-2.38 micron wavelength region is also successful in discriminating and mapping illitic, kaolinitic, and propylitic alteration types.

Hutsinpiller, Amy↗

Spectral Gradients and u-v Sampling

I describe a systematic method for characterizing the effects of differences in u-v coverage in terms of inferred spectral gradients in interferometric images. This method is directly applicable to optical and radio interferometry; it is useful in situations when observations using scale arrays are not feasible.

u-v sampling spectral gradients interferometric im↗

Advanced Technology Development: Solid-Liquid Interface Characterization Hardware

Characterizing the solid-liquid interface during directional solidification is key to understanding and improving material properties. The goal of this Advanced Technology Development (ATD) has been to develop hardware, which will enable real-time characterization of practical materials, such as aluminum (Al) alloys, to unprecedented levels. Required measurements include furnace and sample temperature gradients, undercooling at the growing interface, interface shape, or morphology, and furnace translation and sample growth rates (related). These and other parameters are correlated with each other and time. A major challenge was to design and develop all of the necessary hardware to measure the characteristics, nearly simultaneously, in a smaller integral furnace compatible with existing X-ray Transmission Microscopes, XTMs. Most of the desired goals have been accomplished through three generations of Seebeck furnace brassboards, several varieties of film thermocouple arrays, heaters, thermal modeling of the furnaces, and data acquisition and control (DAC) software. Presentations and publications have resulted from these activities, and proposals to use this hardware for further materials studies have been submitted as sequels to this last year of the ATD.

Source record↗

Some characteristics of bypass transition in a heated boundary layer

Experimental measurements of both mean and conditionally sampled characteristics of laminar, transitional and low Reynolds number turbulent boundary layers on a heated flat plate are presented. Measurements were obtained in air over a range of freestream turbulence intensities from 0.3 percent to 6 percent with a freestream velocity of 30.5 m/s and zero pressure gradient. Conditional sampling performed in the transitional boundary layers indicate the existence of a near-wall drop in intermittency, especially pronounced at low intermittencies. Nonturbulent intervals were observed to possess large levels of low-frequency unsteadiness, and turbulent intervals had peak intensities as much as 50 percent higher than were measured at fully turbulent stations. Heat transfer results were consistent with results of previous researchers and Reynolds analogy factors were found to be well predicted by laminar and turbulent correlations which accounted for unheated starting length. A small dependence of the turbulent Reynolds analogy factors on freestream turbulence level was observed. Laminar boundary layer spectra indicated selective amplification of unstable frequencies. These instabilities appear to play a dominant role in the transition process only for the lowest freestream turbulence level studied, however.

Sohn, K. H.↗

Some characteristics of bypass transition in a heated boundary layer

Experimental measurements of both mean and conditionally sampled characteristics of laminar, transitional and low Reynolds number turbulent boundary layers on a heated flat plate are presented. Measurements were obtained in air over a range of freestream turbulence intensities from 0.3 percent to 6 percent with a freestream velocity of 30.5 m/s and zero pressure gradient. Conditional sampling performed in the transitional boundary layers indicate the existence of a near-wall drop in intermittency, especially pronounced at low intermittencies. Nonturbulent intervals were observed to possess large levels of low-frequency unsteadiness, and turbulent intervals had peak intensities as much as 50 percent higher than were measured at fully turbulent stations. Heat transfer results were consistent with results of previous researches and Reynolds analogy factors were found to be well predicted by laminar and turbulent correlations which accounted for unheated starting length. A small dependence of the turbulent Reynolds analogy factors on freestream turbulence level was observed. Laminar boundary layer spectra indicated selective amplification of unstable frequencies. These instabilities appear to play a dominant role in the transition process only for the lowest freestream turbulence level studied, however.

Sohn, K. H.↗

Sources of Variation in Creep Testing

Creep rupture is an important material characteristic for the design of rocket engines. It was observed during the characterization of GRCop-84 that the complete data set had nearly 4 orders of magnitude of scatter. This scatter likely confounded attempts to determine how creep performance was influenced by manufacturing. It was unclear if this variation was from the testing, the material, or both. Sources of variation were examined by conducting tests on identically processed specimens at the same specified stresses and temperatures. Significant differences existed between the five constant-load creep frames. The specimen temperature was higher than the desired temperature by as much as 43 C. It was also observed that the temperature gradient was up to 44 C. Improved specimen temperature control minimized temperature variations. The data from additional tests demonstrated that the results from all five frames were comparable. The variation decreased to 1/2 order of magnitude from 2 orders of magnitude for the baseline data set. Independent determination of creep rates in a reference load frame closely matched the creep rates determined after the modifications. Testing in helium tended to decrease the sample temperature gradient, but helium was not a significant improvement over vacuum.

Loewenthal, William S.↗

Low-Gravity Alloy Studies on Aircraft

Controlled solidification continued through many dives. Since each dive gives 20 to 30 seconds in which gravity is 0.001 to 0.1 its normal value, and aircraft may make about ten low-gravity maneuvers in mission, technique allows substantial time to conduct a low-gravity experiment. In directional solidification, liquid/solid interface advanced slowly through rod of sample alloy. Solidification continues during several aircraft maneuvers. Known solidification rate of sample correlated with accelerometer data to find gravity value during solidification for any point in sample. Thermal gradient and solidification rate controlled independently.

Curreri, P. A.↗

Overview of ACE-Asia Spring 2001 Investigations On Aerosol-Radiation Interactions

ACE-Asia's extensive measurements from land, ocean, air and space quantified aerosol-radiation interactions. Results from each platform type, plus satellite-suborbital combinations, include: 1. Time series of multiwavelength aerosol optical depth (ADD), Angstrom exponent (alpha), single-scattering albedo (SSA), and size distribution from AERONET radiometry at 13 stations. In China and Korea AOD and alpha were strongly anticorrelated (reflecting transient dust events); dust volume-size modes peaked near 8 microns diameter; and SSA(dust) greater than SSA(pollution). 2. Calculations and measurements of photosynthetically active radiation and aerosols in China yield 24-h average downward surface radiative forcing per AOD(500 nm) of -27 W/sq m (400-700 nm). 3. The Hawaii-Japan cruise sampled a gradient with AOD(500 nm) extremes of 0.1 and 1.1. Shipboard measurements showed that adding dust to pollution increased SSA(550 nm, 55% RH), typically from -0.91 to approx. 0.97. Downwelling 8-12 micron radiances showed aerosol effects, especially in the major April dust event, with longwave forcing estimated at -5 to 15 W/sq m. 4. Extinction profiles from airborne sunphotometry and total-direct-diffuse radiometry show wavelength dependence often varying strongly with height, reflecting layering of dust-dominated over pollution-dominated aerosols. Comparing sunphotometric extinction profiles to those from in situ measurements (number and composition vs size, or scattering and absorption) shows layer heights agree, but extinction sometimes differs. 5. Airborne solar spectral flux radiometry yields absorption spectra for layers. Combining with AOD spectra yields best-fit aerosol single scattering albedo spectra. 6. Visible, NIR and total solar fluxes combined with AOD give radiative forcing efficiencies at surface and aloft.

Russell, P. B.↗

Directional solidification of flake and nodular cast iron during KC-135 low-g maneuvers

Alloys solidified in a low-gravity environment can, due to the elimination of sedimentation and convection, form unique and often desirable microstructures. One method of studying the effects of low-gravity (low-g) on alloy solidification was the use of the NASA KC-135 aircraft flying repetitive low-g maneuvers. Each maneuver gives from 20 to 30 seconds of low-g which is between about 0.1 and 0.001 gravity. A directional solidification furnace was used to study the behavior of off eutectic composition case irons in a low-g environment. The solidification interface of hypereutectic flake and spheroidal graphite case irons was slowly advanced through a rod sample, 5 mm in diameter. Controlled solidification was continued through a number of aircraft parabolas. The known solidification rate of the sample was then correlated with accelerometer data to determine the gravity level during solidification for any location of the sample. The thermal gradient and solidification rate were controlled independently. Samples run on the KC-135 aircraft exhibited bands of coarser graphite or of larger nodules usually corresponding to the regions solidified under low-g. Samples containing high phosphorous (used in order to determine the eutectic cell) exhibited larger eutectic cells in the low-g zone, followed by a band of coarser graphite.

Curreri, P. A.↗

CLEAR: The Gas-phase Metallicity Gradients of Star-forming Galaxies at 0.6<z<2.6

We report on the gas-phase metallicity gradients of a sample of 238 star-forming galaxies at 0.6 < z < 2.6, measured through deep near-infrared Hubble Space Telescope slitless spectroscopy. The observations include 12 orbit depth Hubble/WFC3 G102 grism spectra taken as a part of the CANDELS Lyα Emission at Reionization (CLEAR) survey, and archival WFC3 G102+G141 grism spectra overlapping the CLEAR footprint. The majority of galaxies in this sample are consistent with having a zero or slightly positive metallicity gradient ( dZ/dR ≥ 0, i.e., increasing with radius) across the full mass range probed (8.5 < log M * / M ⊙ < 10.5). We measure the intrinsic population scatter of the metallicity gradients, and show that it increases with decreasing stellar mass—consistent with previous reports in the literature, but confirmed here with a much larger sample. To understand the physical mechanisms governing this scatter, we search for correlations between the observed gradient and various stellar population properties at fixed mass. However, we find no evidence for a correlation with the galaxy properties we consider—including star formation rates, sizes, star formation rate surface densities, and star formation rates per gravitational potential energy. We use the observed weakness of these correlations to provide material constraints for predicted intrinsic correlations from theoretical models.

Raymond C. Simons↗

Electric Field Containerless Processing Technology

The objective of this task is to develop the science and technology base required to design and construct a high temperature electric field positioning module that could be used by materials scientists to conduct containerless science experiments in a low gravity environment. Containerless science modules that employ electric fields to position and manipulate samples offer several advantages over acoustic or electromagnetic systems. The electric field system will operate not only at atmospheric pressures but also in a vacuum, in contrast to the acoustic modules which can only operate in atmosphere where the acoustic forces are sufficient. The electric field technique puts minimum energy into the sample, whereas the electromagnetic system can deposit energy into the sample through eddy current heat as well as physical mixing in the sample. Two types of electric field modules have been constructed and tested to date. One employs a charged sample and uses electrostatic forces to position and control the sample. The second type of module induces electrical polarization of the sample and electric field gradients to position and control the sample.

Elleman, D. D.↗

The use of the ion probe mass spectrometer in the measurement of hydrogen concentration gradients in Monel K 500

The ion probe mass spectrometer was used to measure hydrogen concentration gradients in cathodically charged Monel K 500. Initial work with the ion probe involved the calibration of the instrument and the establishment of a suitable experimental procedure for this application. Samples of Monel K 500 were cathodically charged in a weak sulfuric acid solution. By varying the current density, different levels of hydrogen were introduced into the samples. Hydrogen concentration gradients were taken by ion sputtering on the surface of these samples and monitoring the behavior of the hydrogen mass peak as a function of time. An attempt was made to determine the relative amounts of hydrogen in the bulk and grain boundaries by analyzing a fresh fracture surface with a higher proportion of grain boundary area. It was found that substantially more hydrogen was detected in the grain boundaries than in the bulk, confirming the predictions of previous workers. A sputter rate determination was made in order to establish the rate of erosion.

Truhan, J. J., Jr.↗

Thermal-infrared remote sensing and Kirchhoff's Law. 1: Laboratory measurements

By the end of this century the Earth Observing System (EOS) will provide worldwide, thermal infrared, multispectral images of the Earth, presenting geologists with a new kind of remote sensing data for interpretation. Thus it has become essential to understand the spectral emittance behavior of terrestrial surface materials. Perhaps the most fundamental question to be answereed is the extent to which such materials follow Kirchhoff's law (epsilon = 1 -R) under laboratory and field conditions, especially when a sample displays a thermal gradient. We present the first rigorous quantitative comparison of directional and hemispherical reflectance and directional emittance of rock and soil samples in the laboratory, with thermal gradients induced by heating them from below and allowing them to radiate to a colder background. The results show that only an extemeley low density sample composed of fine particles sifted into a 'fairy castle' structure displays a thermal gradient steep enough within the infrared skin depth to cause significant (6%) departure from Kirchhoff's law. There is no detectable effect on the more normal terrestrial samples, such as soils and rocks measured in the laboratory, even when semitransparent coatings are involved. Thus both emittance and reflectance measurements can be used to calculate sample emissivity for most terrestrial surface materieals. However, the effect on Kirchhoffian behavior of different field environments, which may induce a steeper thermal gradient in particulate samples, has yet to be determined, and some low-density surface materials like newly fallen snow, frost, and efflorescent salts on playas have yet to be measured in emittance.

Salisbury, John W.↗

Characterization of the Heat Extraction Capability of a Compliant, Sliding, Thermal Interface for Use in a High Temperature, Vacuum Microgravity Furnace

Much of the material science gained in microgravity research requires processing a sample in a high performance furnace. One such furnace currently being designed is the Quench Module Insert (QMI). The Principle Investigators, for whom the furnace is proposed, require high temperature gradients in their cylindrical samples to achieve the science objectives. One of the components critical to achieving high sample axial temperature gradients in the Quench Module Insert is a high performance cold zone to extract the heat from the sample. This cold zone employs a compliant, sliding thermal interface based on a Vel-Therm felt. This felt provides a conductive path between the Sample Cartridge Assembly (SCA) exterior surface and the interior surface of the water cooled chill block while allowing movement of the sample relative to the chill block. The Vel-Therm felt is composed of long polymer-based fibers affixed to a thin flexible substrate layer. The fibers are oriented perpendicular to this substrate giving the felt the appearance of a velvet fabric. The Vel-Therm felt heat extraction capability was quantified in earlier tests performed in an inert gas environment. The current activity, described in this paper, is intended to characterize the extraction capability of Vel-Therm felt in a vacuum environment similar to the QMI environment. This testing is necessary to quantify the thermal performance of the Vel-Therm felt and the sensitivity of that performance to key variables. The data derived from these tests will be incorporated into the current thermal models to improve the quality of the models and reduce uncertainty of the analytical results. In addition, the data will be used to help select the appropriate Vel-Therm felt and set proper operating limits as well as assess the performance range of the furnace. The objective of this test is to measure the heat extraction rate of the Vel-Therm felt as specified by the effective heat transfer coefficient. Therefore, the test setup was designed to force the bulk of the heat transfer through the area where the Vel-Therm felt was applied. A heat source, consisting of a ceramic heating element encased in a Copper (Cu) housing is mounted on four isolated support rods. A 6-layer molybdenum radiation shield is used to insulate against heat loss from the heater and prevent heat exchange between the hot and cold sides of the test apparatus. The Vel-Therm felt is affixed to the surface of the cold sink, a water-cooled Cu chill block. An adjustable plate supports and isolates the cold sink from above and is used to control the amount of the deflection of the Vel- Therm when in contact with the Cu heating element housing. The primary means of establishing the power being conducted through the felt is to measure the energy being transferred to the water passing through the chill block. Analysis was performed to support the assumption that the source and sink surfaces were approximately isothermal under the specific test conditions. As a check on the amount of power passing through the felt, the power supplied to the heater was also measured. Thermocouples were strategically located throughout the test apparatus for measurement purposes. A bell jar was lowered over the assembly to impose vacuum conditions. Currently, variables tested have been fiber compression and fiber type and surface temperatures (both the hot and cold side temperatures are hypothesized to be important to the performance of the Vel-Therm.) Selected runs were repeated to ensure consistency and repeatability. Results obtained thus far reveal that Vel-Therm performance is significantly degraded by fibers being exposed to high compression. It also shows that performance is somewhat negatively impacted by previous compression, thereby, raising the question of repeatability. In addition, early results show a significant dependence on temperature. A computer aided mathematical analysis of the test setup is ongoing. The results will be correlated to actual results. The correlation will examine such details as parasitic loses, conduction down the power leads and many other concerns.

Bellomy-Ezell, Jenny↗

Early Results and Spaceflight Implications of the SWAB Flight Experiment

Microbial monitoring of spacecraft environments provides key information in the assessment of infectious disease risk to the crew. Monitoring aboard the Mir space station and International Space Station (ISS) has provided a tremendous informational baseline to aid in determining the types and concentrations of microorganisms during a mission. Still, current microbial monitoring hardware utilizes culture-based methodology which may not detect many medically significant organisms, such as Legionella pneumophila. We hypothesize that evaluation of the ISS environment using non-culture-based technologies would reveal microorganisms not previously reported in spacecraft, allowing for a more complete health assessment. To achieve this goal, a spaceflight experiment, operationally designated as SWAB, was designed to evaluate the DNA from environmental samples collected from ISS and vehicles destined for ISS. Results from initial samples indicate that the sample collection and return procedures were successful. Analysis of these samples using denaturing gradient gel electrophoresis and targeted PCR primers for fungal contaminants is underway. The current results of SWAB and their implication for in-flight molecular analysis of environmental samples will be discussed.

Ott, C. Mark↗

Method for Processing Lunar Regolith Using Microwaves

A paper describes a method of using microwave heating experiments on lunar simulants to determine the mechanism that causes lunar regolith to be such an excellent microwave absorber. The experiments initially compared the effects of sharp particle edges to round particle edges on the heating curves. For most compositions, sharp particle edged samples were more effective in being heated by microwaves than round particle edged materials. However, the experiments also showed an unexpected effect for both types of particles. Upon heating the sample surface above 400 C, the sample experienced some sort of internal structure change that caused it to heat much more efficiently. This enhancement may be associated with the unique microwave volumetric heating that can produce a large temperature gradient within the sample leading to melting of some components at the center of the sample. This new effect that may also be happening in lunar regolith samples is probably the cause of the previously observed enhanced heating of a sample of lunar regolith. Properly designed microwave applicators could heat and solidify the lunar regolith to form roads and building blocks for structures needed on the Moon

Barmatz, Martin B.↗