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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records

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NASA NTRS1981

Statistical distribution of mechanical properties for three graphite-epoxy material systems

Graphite-epoxy composites are playing an increasing role as viable alternative materials in structural applications necessitating thorough investigation into the predictability and reproducibility of their material strength properties. This investigation was concerned with tension, compression, and short beam shear coupon testing of large samples from three different material suppliers to determine their statistical strength behavior. Statistical results indicate that a two Parameter Weibull distribution model provides better overall characterization of material behavior for the graphite-epoxy systems tested than does the standard Normal distribution model that is employed for most design work. While either a Weibull or Normal distribution model provides adequate predictions for average strength values, the Weibull model provides better characterization in the lower tail region where the predictions are of maximum design interest. The two sets of the same material were found to have essentially the same material properties, and indicate that repeatability can be achieved.

Reese, C.↗

NASA NTRS1988

Fracture analysis of local delaminations in laminated composites

A shear deformation model was developed to analyze local delaminations growing from transverse cracks in 90 degree plies located around the mid plane of symmetric laminates. The predictions of the model agree reasonably with experimental data from T300/934 graphite epoxy laminates. The predicted behavior is such that, in combination with an edge delamination model, the critical loads can be predicted accurately in the range of n from .5 to 8.

Sriram, P.↗

NASA NTRS1989

Fracture analysis of local delaminations in laminated composites

Armanios, E. A.↗

NASA NTRS1984

An elastic potential for the nonlinear response of unidirectional graphite composites

An elastic potential is proposed that is capable of modeling the reversible portion of the observed nonlinear response of unidirectional graphite fiber composites. The model includes both the stiffening stress-strain behavior as well as the softening Poisson's response for loading in the fiber direction. The model is compared with experimental results for Celion 6000/PMR-15 graphite-polyimide.

Pindera, M.-J.↗

NASA NTRSDate not supplied

Study of Graphite Ablation at Arc-Jet Conditions using Finite-Rate and Equilibrium Chemistry Models

Moving at hypersonic speeds through the atmosphere generates immense amount of heat that triggers thermo-chemical non-equilibrium effects in the flow approaching the vehicle and leads to surface chemical reactions that cause ablation and consume the material mass. This complex behavior and interaction of the aerothermal environment with a graphite surface is com- putationally modeled in the present work using a fully-coupled simulation between flow solver CHAMPS NBS-Cart and material response solver KATS-MR. In this study, we account for the thermo-chemical non-equilibrium effects occurring in the flow and use an 11-species air-carbon re- action model to simulate the ablation of the material. The reactions at the surface such oxidation, nitridation and recombination are modeled with a newly developed air-carbon reaction model. The coupled simulation is applied to study two experimental cases performed at IHF arc-jet facility at NASA Ames research center. The obtained results are compared against the measured data of surface recession, as well as surface and in-depth temperatures. Additionally, uncoupled sim- ulations, performed with equilibrium chemistry at the wall, point out the substantial differences between the coupled and uncoupled solutions, leading to higher deviation of the predicted temper- atures. Overall, we show excellent agreement between the coupled simulation predictions and the experimental data in all measured quantities.

EDL↗

NASA NTRS1985

Evaluation and prediction of long-term environmental effects of nonmetallic materials

The properties of a number of nonmetallic materials were evaluated experimentally in simulated space environments in order to develop models for accelerated test methods useful for predicting such behavioral changes. Graphite-epoxy composites were exposed to thermal cycling. Adhesive foam tapes were subjected to a vacuum environment. Metal-matrix composites were tested for baseline data. Predictive modeling designed to include strength and aging effects on composites, polymeric films, and metals under such space conditions (including the atomic oxygen environment) is discussed. The Korel 8031-00 high strength adhesive foam tape was shown to be superior to the other two tested.

Papazian, H.↗

NASA NTRS1988

Prediction of high temperature metal matrix composite ply properties

The application of the finite element method (superelement technique) in conjunction with basic concepts from mechanics of materials theory is demonstrated to predict the thermomechanical behavior of high temperature metal matrix composites (HTMMC). The simulated behavior is used as a basis to establish characteristic properties of a unidirectional composite idealized an as equivalent homogeneous material. The ply properties predicted include: thermal properties (thermal conductivities and thermal expansion coefficients) and mechanical properties (moduli and Poisson's ratio). These properties are compared with those predicted by a simplified, analytical composite micromechanics model. The predictive capabilities of the finite element method and the simplified model are illustrated through the simulation of the thermomechanical behavior of a P100-graphite/copper unidirectional composite at room temperature and near matrix melting temperature. The advantage of the finite element analysis approach is its ability to more precisely represent the composite local geometry and hence capture the subtle effects that are dependent on this. The closed form micromechanics model does a good job at representing the average behavior of the constituents to predict composite behavior.

Caruso, J. J.↗

NASA NTRS1984

Coefficient of restitution for low velocity transverse impact of thin graphite-epoxy laminates

A simple model is presented for the low velocity impact behavior of thin plates composed of T300/5208 graphite/epoxy. The model, which is constructed on the assumption that the plate is inextensible in the fiber direction and that the material is incompressible in the z direction, is able to predict the energy absorbed by the target during an impact event, or the 'coefficient of restitution'. The plate essentially deforms by shear, allowing the model to neglect bending deformations. The coefficient of restitution is predicted to increase with large interlaminar shear strength and low transverse shear modulus of the laminate. The coefficient's experimentally measured values agree with model-predicted values within a reasonable error.

Lal, K. M.↗

NASA NTRS1990

Scaling effects in the static and dynamic response of graphite-epoxy beam-columns

Scale model technology represents one method of investigating the behavior of advanced, weight-efficient composite structures under a variety of loading conditions. It is necessary, however, to understand the limitations involved in testing scale model structures before the technique can be fully utilized. These limitations, or scaling effects, are characterized. in the large deflection response and failure of composite beams. Scale model beams were loaded with an eccentric axial compressive load designed to produce large bending deflections and global failure. A dimensional analysis was performed on the composite beam-column loading configuration to determine a model law governing the system response. An experimental program was developed to validate the model law under both static and dynamic loading conditions. Laminate stacking sequences including unidirectional, angle ply, cross ply, and quasi-isotropic were tested to examine a diversity of composite response and failure modes. The model beams were loaded under scaled test conditions until catastrophic failure. A large deflection beam solution was developed to compare with the static experimental results and to analyze beam failure. Also, the finite element code DYCAST (DYnamic Crash Analysis of STructure) was used to model both the static and impulsive beam response. Static test results indicate that the unidirectional and cross ply beam responses scale as predicted by the model law, even under severe deformations. In general, failure modes were consistent between scale models within a laminate family; however, a significant scale effect was observed in strength. The scale effect in strength which was evident in the static tests was also observed in the dynamic tests. Scaling of load and strain time histories between the scale model beams and the prototypes was excellent for the unidirectional beams, but inconsistent results were obtained for the angle ply, cross ply, and quasi-isotropic beams. Results show that valuable information can be obtained from testing on scale model composite structures, especially in the linear elastic response region. However, due to scaling effects in the strength behavior of composite laminates, caution must be used in extrapolating data taken from a scale model test when that test involves failure of the structure.

Jackson, Karen E.↗

NASA NTRSDate not supplied

Macro-scale Testing and Micromechanics Modeling of Fracture Behaviors for Boron Carbide Composites with Hierarchical Microstructures

With a unique combination of properties including high hardness, low density, wear and corrosion resistance, thermal stability, high neutron absorption, and semi-conductivity, boron carbide (B4C) is a candidate material for various engineering applications that involve extreme environment. The current applications of boron carbide, however, are limited by its intrinsic brittleness due to its strong covalent bonding. To toughen boron carbide, in this work hierarchical microstructure designs was used to provide multiple toughening mechanisms including crack deflection/bridging, micro-crack toughening, etc. Using field assisted sintering, B4C composites with hierarchical microstructure features including graphite platelets, micron and sub-micron sized TiB2 reinforcements were fabricated. The fracture toughness of fabricated B4C composites were previously measured at micro-scale using micro-indentation followed by post-testing microstructure inspection. However, questions including whether the fracture toughness enhancement measured at micro-scale can translate to macro-scale mechanical properties, and what are the fundamental mechanisms behind observed fracture toughness enhancement, remain to be answered. In this study, the fabricated B4C composites were tested using standardized four-point bending method to obtain fracture toughness at macro-scale. In addition, micromechanics modeling was conducted using MAC/GMC code and crack-band model to study the effect of residual stress and weak interphases on fracture behaviors of B4C composites reinforced with TiB2 particles. Through standardized four-point bending tests, fracture toughness enhancements up to 2.85, 3.32, and 3.65 MPa∙m(exp 1/2) (from 2.38 MPa∙m(exp 1/2)) were achieved for B4C composites with graphite platelets addition (micro/nano B4C), with TiB2 formation (micro B4C-TiB2), and with both graphite and TiB2 addition (micro/nano B4C-TiB2) respectively. Micromechanics modeling indicated that introduction of thermal residual stress and weak interphases caused enhanced micro-cracking behavior and resulted in the observed fracture toughness enhancement. These results furthered understanding about the mechanical behaviors at macro-scale and the mechanisms behind observed fracture toughness enhancement for B4C composites with hierarchical microstructures and can provide reference data for the future design of B4C composites with optimized microstructures for further fracture toughness enhancement.

Boron Carbide↗

NASA NTRS1988

A fiber-resin micromechanics analysis of the delamination front in a DCB specimen

A 3-D finite element model was developed to analyze the fiber-resin behavior near the delamination front in a graphite-epoxy double cantilever beam (DCB) specimen. The specimen interior was analyzed using a typical one-fiber slice, represented by a local 3-D fiber-resin model. The resin stresses were computed for the resin-rich layer at the ply interface as well as for the regions between the fibers close to the delamination front. However, the computed strain energy release rate G sub I along the delamination front varied by less than two percent, and was within about four percent of the plane-strain value. The von Mises yield criterion was used to estimate the extent of yielding near the delamination front. The yielding extended ahead of the delamination and also developed between the fibers. Although the fibers had only a negligible effect on G sub I, they caused yielding within the ply and therefore could influence delamination fracture toughness. The normal and shear stresses at the fiber-resin interface were computed near the delamination front. These results suggest that multi-axial stress criteria may be required to analyze fiber-resin interfaces.

Crews, J. H.↗

NASA NTRS1981

Durability/life of fiber composites in hygrothermomechanical environments

Statistical analysis and multiple regression were used to determine and quantify the significant hygrothermomechanical variables which infuence the tensile durability/life (cycle loading, fatigue) of boron-fiber/epoxy-matrix (B/E) and high-modulus-fiber/epoxy-matrix (HMS/E) composites. The use of the multiple regression analysis reduced the variables from fifteen, assumed initially, to six or less with a probability of greater than 0.999. The reduced variables were used to derive predictive models for compression an intralaminar shear durability/life of B/E and HMS/E composites assuming isoparametric fatigue behavior. The predictive models were subsequently generalized to predict the durability/life of graphite-fiber-r generalized model is of simple form, predicts conservative values compared with measured data and should be adequate for use in preliminary designs.

Chamis, C. C.↗

NASA NTRS1976

Fundamental analysis of the failure of polymer-based fiber reinforced composites

A mathematical model is described which will permit predictions of the strength of fiber reinforced composites containing known flaws to be made from the basic properties of their constituents. The approach was to embed a local heterogeneous region (LHR) surrounding the crack tip into an anisotropic elastic continuum. The model should (1) permit an explicit analysis of the micromechanical processes involved in the fracture process, and (2) remain simple enough to be useful in practical computations. Computations for arbitrary flaw size and orientation under arbitrary applied load combinations were performed from unidirectional composites with linear elastic-brittle constituent behavior. The mechanical properties were nominally those of graphite epoxy. With the rupture properties arbitrarily varied to test the capability of the model to reflect real fracture modes in fiber composites, it was shown that fiber breakage, matrix crazing, crack bridging, matrix-fiber debonding, and axial splitting can all occur during a period of (gradually) increasing load prior to catastrophic fracture. The computations reveal qualitatively the sequential nature of the stable crack process that precedes fracture.

Kanninen, M. F.↗

NASA NTRS1977

Preliminary development of a fundamental analysis model for crack growth in a fiber reinforced composite material

A mathematical model for the strength of fiber reinforced composites containing specific flaws is described. The approach is to embed a local heterogeneous region surrounding the crack tip in an anisotropic elastic continuum. By consideration of the individual failure events activated near the flaw tip, a strength prediction can be made from basic properties of the composite constituents. Computations for arbitrary flaw size and orientation have been performed for unidirectional composites with linear elastic-brittle constituent behavior. The mechanical properties were those of graphite epoxy. With the rupture properties arbitrarily varied to test the capability of the model to reflect real fracture modes in fiber composites, it is shown that fiber breakage, matrix crazing, crack bridging, matrix-fiber debonding, and axial splitting all can occur during gradually increasing load prior to catastrophic fracture. Qualitative comparisons with experimental results on edge-notched unidirectional graphite epoxy specimens have also been made.

Kanninen, M. F.↗

NASA NTRSDate not supplied

Toughening of Boron Carbide Composites by Hierarchical Microstructuring

Due to a unique combination of properties including high hardness, low density, chemical and thermal stability, semi-conductivity, and high neutron absorption, boron carbide (B4C) is a potential candidate for various applications involving extreme environment. However, B4C’s current application is limited because of its low fracture toughness. In this study, a hierarchical microstructure design with features including TiB2 grains and graphite platelets was used to toughen B4C by simultaneously utilizing multiple toughening mechanisms including crack deflection, bridging, and micro-crack toughening. Using field-assisted sintering technology (FAST), B4C composites with dense and hierarchical microstructure were fabricated. Previously, the fracture toughness of fabricated B4C composites was measured at micro-scale using micro-indentation to have up to 56% improvement. In this work, the B4C composites’ fracture toughness was characterized at macro-scale using four-point bending methods and compared with previous results obtained at micro-scale. Micromechanics modeling of fracture behaviors for B4C-TiB2 composites was also performed to evaluate the contributions from experimentally observed toughening mechanisms. From four-point bending tests, B4C composites reinforced with both TiB2 grains (~15 vol%) and graphite platelets (~8.7 vol%) exhibited the highest fracture toughness enhancement from 2.38 to 3.65 MPa∙m^(1/2). The measured values were lower than those obtained using micro-indentation but maintained the general trends. The discrepancy between the indentation and four-point bending test results originated from the complex deformation behaviors triggered by the high contact load during indentation tests. Through micromechanics modeling, introduced thermal residual stress due to thermal expansion mismatch between B4C and TiB2, and weak interphases at B4C-TiB2 boundaries were identified as the main causes for experimentally observed toughness enhancement. These results proved the effectiveness of hierarchical microstructure designs for B4C toughening and can provide reference for the future design of B4C composites with optimized microstructures for further fracture toughness enhancement.

composites↗

NASA NTRS1984

Compression failure mechanisms in unidirectional composites

Compression failure mechanisms in unidirectional composites were examined. Possible failure modes of constituent materials are summarized and analytical models for fiber microbuckling are reviewed from a unified viewpoint. Due to deficiencies in available models, a failure model based on nonlinear properties and initial fiber curvature is proposed. The effect of constituent properties on composite compression behavior was experimentally investigated using two different graphite fibers and four different epoxy resins. The predominant microscopic scale failure mode was found to be shear crippling. In a soft resin, shear crippling was in the form of buckling of fibers on a microscopic scale. However, stiff resins failure was characterized by the formation of a kink band. For unidirectional laminates, compressive strength, and compressive modulus to a less extent, were found to increase with increasing magnitude of resin modulus. The change in compressive strength with resin modulus was predicted using the proposed nonlinear model.

Hahn, H. T.↗

NASA NTRS1986

Compression failure mechanisms in unidirectional composites

Hahn, H. T.↗

NASA NTRS1980

Manufacture of fiber-epoxy test specimens: Including associated jigs and instrumentation

Experimental work on the manufacture and strength of graphite-epoxy composites is considered. The correct data and thus a true assessment of the strength properties based on a proper and scientifically modeled test specimen with engineered design, construction, and manufacture has led to claims of a very broad spread in optimized values. Such behavior is in the main due to inadequate control during manufacture of test specimen, improper curing, and uneven scatter in the fiber orientation. The graphite fibers are strong but brittle. Even with various epoxy matrices and volume fraction, the fracture toughness is still relatively low. Graphite-epoxy prepreg tape was investigated as a sandwich construction with intermittent interlaminar bonding between the laminates in order to produce high strength, high fracture toughness composites. The quality and control of manufacture of the multilaminate test specimen blanks was emphasized. The dimensions, orientation and cure must be meticulous in order to produce the desired mix.

Mathur, S. B.↗