Hermetic seal evaluation for electronic components Final report
Leakage rate limits of hermetically sealed spacecraft electronic components, and correlation of radioactive gas and helium mass spectrometer detection methods
SEARCH · Search NASA
Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.
Leakage rate limits of hermetically sealed spacecraft electronic components, and correlation of radioactive gas and helium mass spectrometer detection methods
The primary goal of the Resource Prospector Neutron Spectrometer System (NSS) is to locate and characterize hydrogen-bearing volatile deposits, especially subsurface ice, that may exist at the lunar poles. A key objective is to detect water-equivalent hydrogen concentrations of 0.5 wt% or greater while on a moving rover. A second objective is to determine approximate burial depth of enhanced hydrogen-bearing materials up to 1 meter below otherwise dry regolith. The instrument will be carried aboard a landed mobility system at the lunar poles. The instrument operates by measuring the changes in the leakage flux of low energy neutrons out of the regolith. These neutrons are produced by galactic cosmic rays, which are so energetic that they shatter the nuclei in surface materials. The neutrons interact with other nuclei and lose energy, becoming thermalized in the process. Hydrogen is most efficient at thermalizing neutrons owing to protons' similar mass - statistically, neutrons lose half their energy per collision with protons. With hydrogen in the soil, leakage fluxes of neutrons in the 0.5 eV to 500 keV energy range are reduced. A concentration of only1-2 wt% water-equivalent hydrogen results in a decrease in epithermal leakage flux of a factor of two. The leakage flux of thermal neutrons, from 0 to 0.5 eV in energy, can either increase or decrease depending on the hydrogen abundance and stratigraphy. As with the highly successful Lunar Prospector Neutron Spectrometer, the RP NSS detects both thermal and epithermal neutrons by using two helium-3 gas proportional counters, one covered by cadmium and the other uncovered. The former detects only epithermal neutrons with energies above approximately 0.5 eV, the latter detects both thermal (less than 0.5 eV) and epithermal energies (greater than 0.5 eV). When a neutron enters the detector tube and interacts with a helium-3 nucleus, the resulting reaction produces an energetic proton and triton that ionize the gas. The resulting electrons are accelerated toward a high-voltage anode and cascade, amplifying the net charge, which is collected at the anode. The number of electrons produced is proportional to the energy that the triton and proton deposit in the gas. A charge sensitive pre-amplifier converts the total charge to a step voltage output. A shaper amplifier then shapes this step into a uni-polar waveform with peaking time appropriate for the detection depending on the event rate. The integrated shaped waveform, representing the deposited triton/proton energy, is then measured. A histogram, or pulse height analysis, is performed to record the main capture peak and wall effect pulses. A threshold for detection is also required to limit the low amplitude counting rate such as noise floor. The system electronics consists of 2 modules - the Sensor Module (SM) front-end and the Data Processing Module (DPM) back-end circuits. SM is designed as a light-weight and low power front-end housing the two helium-3 proportional counter detectors, preamp and HVPS. It is mounted external to the rover body to detect the thermalized neutron flux with a minimum of host background. The DPM is located inside the rover; it digitizes the SM signals, performs pulse height analysis and accumulates the count rate for each spectral channel. The DPM controls high voltage and thresholding, and sends the science data to the host craft via an RS422 serial asynchronous protocol. The payload host provides all thermal management and control for the SM and DPM.
NASA, military, and commercial satellite users need launch services that are highly reliable, less complex, easier to test, and cost effective. This project has developed a tapered optical fiber sensor for detecting hydrogen. The invention involves incorporating chemical indicators on the tapered end of an optical fiber using organically modified silicate nanomaterials. The Hazardous Gas Detection Lab (HGDL) at Kennedy Space Center is involved in the design and development of instrumentation that can detect and qualify various mission-critical chemicals. Historically, hydrogen, helium, nitrogen, oxygen, and argon are the first five gases of HGDL focus. The use of these cryogenic fluids in the area of propulsion offers challenges. Due to their extreme low temperatures, these fluids induce contraction of the materials they contact, a potential cause of leakage. Among them, hydrogen is of particular concern. Small sensors are needed in multiple locations without adding to the structural weight. The most vulnerable parts of the engine are the connection flanges on the transfer lines, which have to support cycles of large thermal amplitude. The thermal protection of the engine provides a closed area, increasing the likelihood of an explosive atmosphere. Thus, even a small leak represents an unacceptable hazardous condition during loading operations, in flight, or after an aborted launch. Tapered fibers were first fabricated from 1/1.3-mm core/cladding (silica/ plastic) optical fibers. Typically a 1-ft (approx. 30- cm) section of the 1-mm fiber is cut from the bundle and marked with a pen into five 2-.-in. (.5.7-cm) sections. A propane torch is applied at every alternate mark to burn the jacket and soften the glass core. While the core is softening, the two ends of the fiber are pulled apart slowly to create fine tapers of .- to .-in. (.6- to 12-mm) long on the 1-mm optical fiber. Following this, the non-tapered ends of the fibers are polished to a 0.3-micron finish. Then these fibers were coated with indicators sensitive to hydrogen. The tapered hydrogen detection system with its unique flexibility is the only system that can be placed in many locations inside the vehicles and detect the exact location of leaks, saving millions of dollars for launch vehicle industries.
The figure schematically depicts a portable microleak-detection system that has been built especially for use in testing hydrogen tanks made of polymer-matrix composite materials. (As used here, microleak signifies a leak that is too small to be detectable by the simple soap-bubble technique.) The system can also be used to test for microleaks in tanks that are made of other materials and that contain gases other than hydrogen. Results of calibration tests have shown that measurement errors are less than 10 percent for leak rates ranging from 0.3 to 200 cm3/min. Like some other microleak-detection systems, this system includes a vacuum pump and associated plumbing for sampling the leaking gas, and a mass spectrometer for analyzing the molecular constituents of the gas. The system includes a flexible vacuum chamber that can be attached to the outer surface of a tank or other object of interest that is to be tested for leakage (hereafter denoted, simply, the test object). The gas used in a test can be the gas or vapor (e.g., hydrogen in the original application) to be contained by the test object. Alternatively, following common practice in leak testing, helium can be used as a test gas. In either case, the mass spectrometer can be used to verify that the gas measured by the system is the test gas rather than a different gas and, hence, that the leak is indeed from the test object.
In the Powder River Basin, Wyo., narrow geologic units having thermal inertias which contrast with their surroundings can be discriminated in optimal images. A few subtle thermal inertia anomalies coincide with areas of helium leakage believed to be associated with deep oil and gas concentrations. The most important results involved delineation of tectonic framework elements some of which were not previously recognized. Thermal and thermal inertia images also permit mapping of geomorphic textural domains. A thermal lineament appears to reveal a basement discontinuity which involves the Homestake Mine in the Black Hill, a zone of Tertiary igneous activity and facies control in oil producing horizons. Applications of these data to the Cabeza Prieta, Ariz., area illustrate their potential for igneous rock type discrimination. Extension to Yellowstone National Park resulted in the detection of additional structural information but surface hydrothermal features could not be distinguished with any confidence. A thermal inertia mapping algorithm, a fast and accurate image registration technique, and an efficient topographic slope and elevation correction method were developed.