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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

High Precision, High Frequency Printed Antennas

An emerging trend in advanced manufacturing is printed electronics and sensors. The ability to print customized electronics and sensors integrated into functional packages is a growing need within a variety of growing markets such as smart manufacturing, internet of things (IoT), and the small satellite industry. Both Oak Ridge National Laboratory (ORNL) and the MITRE Corporation have seedling research efforts evaluating the potential for future printed electronic systems. High frequency, wide-bandwidth phased array antennas (i.e. >45 GHz) open the door to new applications. However, such sensors require currently prohibitively small feature sizes for commercial 3D printing technologies along with increasing challenges with connecting the driving electronics to such features. An additional finding with related advanced manufacturing challenges is the rapid production of 3D additive connectors for integration with commercial printed circuit boards (PCBs), primarily for advanced in-circuit inspection techniques. This work is developing additive manufacturing processes for producing connected and conductive fine scale 3D features. The primary focus was on aerosol-jet printing (AJP), which has a small minimum resolution (<50 µm) but is traditionally printed flat with small height/width aspect ratios <<1, and developing controls to enable fully 3D, high aspect ratio, and unsupported features. In Phase 1 of this effort, baselines of process performance were characterized, and test coupons produced for both ultra-high frequency antennas and microstructures to support reverse engineering of PCBs. In Phase 2, these efforts will be extended for system demonstration of ultra-high frequency antenna arrays, as well as reverse engineering circuitry for dense PCBs.

42 ENGINEERING↗
NASA NTRS1986

Off-line processing of ERS-1 synthetic aperture radar data with high precision and high throughput

The first European remote sensing satellite ERS-1 will be launched by the European Space Agency (ESA) in 1989. The expected lifetime is two to three years. The spacecraft sensors will primarily support ocean investigations and to a limited extent also land applications. Prime sensor is the Active Microwave Instrumentation (AMI) operating in C-Band either as Synthetic Aperture Radar (SAR) or as Wave-Scatterometer and simultaneously as Wind-Scatterometer. In Europe there will be two distinct types of processing for ERS-1 SAR data, Fast Delivery Processing and Precision Processing. Fast Delivery Proceessing will be carried out at the ground stations and up to three Fast Delivery products per pass will be delivered to end users via satellite within three hours after data acquisition. Precision Processing will be carried out in delayed time and products will not be generated until several days or weeks after data acquisition. However, a wide range of products will be generated by several Processing and Archiving Facilities (PAF) in a joint effort coordinated by ESA. The German Remote Sensing Data Center (Deutsches Fernerkundungsdatenzentrum DFD) will develop and operate one of these facilities. The related activities include the acquisition, processing and evaluation of such data for scientific, public and commercial users. Based on this experience the German Remote Sensing Data Center is presently performing a Phase-B study regarding the development of a SAR processor for ERS-1. The conceptual design of this processing facility is briefly outlined.

Gredel, J.↗
DOE OSTI2023

High precision control of laser energy for laser–matter interaction studies

Precise, highly reproducible control of the laser energy is required for high confidence laser–matter interaction research such as in dynamic compression science and high energy density physics. The energy must be adjustable without affecting the pulse shape (time varying intensity) or beam smoothness. We have developed a convenient two-stage energy tuning method for a nominal 100 J, 351 nm (UV) laser. The energy is adjusted in 10 J (10%) increments by operating the laser at full energy and inserting a beam splitter in the laser output. As the splitter is located after the final frequency tripling optics, the UV pulse shape is unchanged. The energy is varied by substituting a splitter of different reflectivity. For finer 3 J (3%) increments, the infrared pulse is attenuated inside the laser before the final amplifier. This requires modest tuning to preserve the pulse shape. The demonstrated variation in shot-to-shot reproducibility is less than +/–2.5 J (5% of the full energy), irrespective of the laser output energy. These approaches can be adapted to most ~100 J class lasers. We describe these techniques and show two examples where they have elucidated the underlying physics in laser shock compression experiments. One used only the beam splitters to establish the pressure for melting in iron. The other combined both techniques to finely increment the peak stress (~2 GPa steps) in germanium to precisely determine the onset and completion of melting—including the melting kinetics. Furthermore, these unambiguous results would not be possible without the developments described here.

47 OTHER INSTRUMENTATION↗
NASA NTRS2012

Lightweight Metal Matrix Composite Segmented for Manufacturing High-Precision Mirrors

High-precision mirrors for space applications are traditionally manufactured from one piece of material, such as lightweight glass sandwich or beryllium. The purpose of this project was to develop and test the feasibility of a manufacturing process capable of producing mirrors out of welded segments of AlBeMet(Registered Trademark) (AM162H). AlBeMet(Registered Trademark) is a HIP'd (hot isostatic pressed) material containing approximately 62% beryllium and 38% aluminum. As a result, AlBeMet shares many of the benefits of both of those materials for use in high performance mirrors, while minimizing many of their weaknesses.

Vudler, Vladimir↗
DOE OSTI2020

Status Update on the High Precision Isotopic Measurements on High Burnup LWR Fuel in 2020

The US Department of Energy (DOE) Office of Nuclear Energy (NE) is currently investigating the feasibility of directly disposing dual-purpose (storage and transportation) canisters (DPCs) in a spent nuclear fuel (SNF) repository. Criticality during the repository performance period (10,000 years or more) is one of the major concerns related to direct disposal of DPCs, specifically as the system undergoes degradation in the repository environment and timeframe. Oak Ridge National Laboratory (ORNL) is developing an as-loaded criticality analysis methodology using full (actinides + fission products) burnup credit that exploits the inherent criticality margin associated with actual canister-specific loading configuration. Burnup credit criticality analysis requires validation of the depletion/decay codes used to generate the burned isotopic inventory of an assembly by comparing the code-predicted inventory with experimentally determined isotopic data. Currently, isotopic measurement data for boiling water reactors (BWR) SNF are limited, and additional measurements will be highly beneficial for BWR burnup credit analysis, which is essential to demonstrate disposability of BWR DPCs. Moreover, new pressurized water reactor (PWR) samples of isotopic measurements will expand the PWR sample population and consequently will greatly improve sample statistics. In turn, this will reduce uncertainty in the computational determination of the isotopic composition of commercial SNF and eliminate additional penalties currently used for lack of data. As part of the isotopic analysis task, eight diverse, high burnup (HBU) samples from several PWR rods are being dissolved and isotopically analyzed to provide high-quality measurement data for PWR SNF to reducing the uncertainties associated with PWR isotopic depletion validation. The isotopics of interest focus on nuclides important to burnup credit, shielding, and decay heat in PWR SNF. Additionally, eight high burnup BWR fuel samples from the Limerick nuclear power plant have been identified for measurement to support reducing uncertainties associated with BWR isotopic depletion validation.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
NASA NTRS2010

Low-Cost High-Precision PIAA Optics for High Contrast Imaging with Exo-Planet Coronagraphs

PIAA optics for high contrast imaging present challenges in manufacturing and testing due to their large surface departures from aspheric profiles at the aperture edges. With smaller form factors and consequent smaller surface deformations (<50 microns), fabrication of these mirrors with diamond turning followed by electron beam lithographic techniques becomes feasible. Though such a design reduces the system throughput to approx.50%, it still provides good performance down to 2 lambda/D inner working angle. With new achromatic focal plane mask designs, the system performance can be further improved. We report on the design, expected performance, fabrication challenges, and initial assessment of such novel PIAA optics.

pupil remapping↗
DOE OSTI2026

Bayesian Inference of Hybrid Star Properties from Future High-precision Measurements of Their Radii

Future high-precision X-ray and gravitational-wave observations of neutron stars (NSs) are expected to constrain NS radii with uncertainties as small as σ ≃ 0.1 km. Such unprecedented precision offers a unique opportunity to extract new information about the nature and equation of state (EOS) of supradense matter in NS cores. Using mock radius data with uncertainties ranging from σ = 1.0 to 0.1 km, together with a flexible meta-model NS EOS that allows for a first-order hadron–quark phase transition, we perform a Bayesian statistical analysis to assess the impact of radius measurements on EOS constraints. We find that high-precision radius measurements, particularly for massive NSs, significantly tighten constraints on the hadron–quark transition density ρ t , the quark matter mass fraction in NS cores, and several parameters characterizing the EOS of supranuclear hadronic matter, although the degree of improvement depends on the assumed prior range of ρ t . In contrast, even with the highest precision considered, NS radii—including those of massive stars—remain largely insensitive to the stiffness of quark matter, independent of the measurement accuracy or the prior range adopted for ρ t .

Neutron stars↗
NASA NTRS2012

High Precision, Absolute Total Column Ozone Measurements from the Pandora Spectrometer System: Comparisons with Data from a Brewer Double Monochromator and Aura OMI

We present new, high precision, high temporal resolution measurements of total column ozone (TCO) amounts derived from ground-based direct-sun irradiance measurements using our recently deployed Pandora single-grating spectrometers. Pandora's small size and portability allow deployment at multiple sites within an urban air-shed and development of a ground-based monitoring network for studying small-scale atmospheric dynamics, spatial heterogeneities in trace gas distribution, local pollution conditions, photochemical processes and interdependencies of ozone and its major precursors. Results are shown for four mid- to high-latitude sites where different Pandora instruments were used. Comparisons with a well calibrated double-grating Brewer spectrometer over a period of more than a year in Greenbelt MD showed excellent agreement and a small bias of approximately 2 DU (or, 0.6%). This was constant with slant column ozone amount over the full range of observed solar zenith angles (15-80), indicating adequate Pandora stray light correction. A small (1-2%) seasonal difference was found, consistent with sensitivity studies showing that the Pandora spectral fitting TCO retrieval has a temperature dependence of 1% per 3K, with an underestimation in temperature (e.g., during summer) resulting in an underestimation of TCO. Pandora agreed well with Aura-OMI (Ozone Measuring Instrument) satellite data, with average residuals of <1% at the different sites when the OMI view was within 50 km from the Pandora location and OMI-measured cloud fraction was <0.2. The frequent and continuous measurements by Pandora revealed significant short-term (hourly) temporal changes in TCO, not possible to capture by sun-synchronous satellites, such as OMI, alone.

Ozone↗
DOE OSTI2024

Development of a Platform for High-Resolution Ion Mobility Separations Coupled with Messenger Tagging Infrared Spectroscopy for High-Precision Structural Characterizations

The ability to uniquely identify a compound requires highly precise and orthogonal measurements. Here we describe a newly developed analytical platform that integrates high resolution ion mobility and cryogenic vibrational ion spectroscopy for high-precision structural characterizations. This platform allows for the temporal separation of isomeric/isobaric ions and provides a highly sensitive description of the ion’s adopted geometry in the gas phase. The combination of these orthogonal structural measurements yields precise descriptors that can be used to resolve between and confidently identify highly similar ions. The unique benefits of our instrument, which integrates a structures for lossless ion manipulations ion mobility (SLIM IM) device with messenger tagging infrared spectroscopy, include the ability to perform high-resolution ion mobility separations and to record the IR spectra of all ions simultaneously. The SLIM IM device, with its 13 m separation path length, allows for multipass experiments to be performed for increased resolution as needed. It is integrated with an Agilent qTOF MS where the collision cell was replaced with a cryogenically held (30 K) TW-SLIM module. The cryo-SLIM is operated in a novel manner that allows ions to be streamed through the device and collisionally cooled to a temperature where they can form noncovalently bound N 2 complexes that are maintained as they exit the device and are detected by the TOF mass analyzer. The instrument can be operated in two modes: IMS+IR where the IR spectra for mobility-selected ions can be recorded and IR-only mode where the IR spectra for all mass-resolved ions can be recorded. In IR-only mode, IR spectra (400 cm –1 spectral range) can be recorded in as short as 2 s for high throughput measurements. Further, this work details the construction of the instrument and modes of operation. It provides initial benchmarking of CCS and IR measurements to demonstrate the utility of this instrument for targeted and untargeted approaches.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1977

Optical timing receiver for the NASA laser ranging system. Part 2: High precision time interval digitizer

The development of a high precision time interval digitizer is described. The time digitizer is a 10 psec resolution stop watch covering a range of up to 340 msec. The measured time interval is determined as a separation between leading edges of a pair of pulses applied externally to the start input and the stop input of the digitizer. Employing an interpolation techniques and a 50 MHz high precision master oscillator, the equivalent of a 100 GHz clock frequency standard is achieved. Absolute accuracy and stability of the digitizer are determined by the external 50 MHz master oscillator, which serves as a standard time marker. The start and stop pulses are fast 1 nsec rise time signals, according to the Nuclear Instrument means of tunnel diode discriminators. Firing level of the discriminator define start and stop points between which the time interval is digitized.

Leskovar, B.↗
NASA NTRS2004

Interferometric apparatus for ultra-high precision displacement measurement

A high-precision heterodyne interferometer measures relative displacement by creating a thermally-insensitive system generally not subject to polarization leakage. By using first and second light beams separated by a small frequency difference (.DELTA.f), beams of light at the first frequency (f.sub.0) are reflected by co-axial mirrors, the first mirror of which has a central aperture through which the light is transmitted to and reflected by the second mirror. Prior to detection, the light beams from the two mirrors are combined with light of the second and slightly different frequency. The combined light beams are separated according to the light from the mirrors. The change in phase (.DELTA..phi.) with respect to the two signals is proportional to the change in distance of Fiducial B by a factor of wavelength (.lambda.) divided by 4.pi. (.DELTA.L=.lambda..DELTA..phi.1/(4.pi.)). In a second embodiment, a polarizing beam splitting system can be used.

Zhao, Feng↗
NASA NTRSDate not supplied

Assessment of Sensor Data Accuracy within Gazebo/ROS for High-Precision Autonomous In-Space Robotic Operations

Modeling high-precision in-space servicing, assembly, and manufacturing operations in a simulated environment is a critical step in the development of robotic systems that will be used to autonomously assemble large-scale structures in space. Limited facility size and high costs for manufacturing prototypes make it challenging to conduct full-scale operational testing under appropriate environmental conditions; therefore, testing in a modular, high-fidelity simulation environment is necessary for verification and validation of technology and architecture designs prior to launch. Several modeling and simulation environments exist both within NASA and industry that can be used to test robotic system design and operations, including the widely used commercial tool Gazebo integrated with Robotic Operating System software. Because the performance of autonomous robotic systems relies heavily on the quality of sensor input data, this paper focuses on assessing the accuracy of pose data from an optical sensor model in the Gazebo environment against the behavior of real hardware. The results of the tests will help developers using Gazebo for large-scale, high-precision simulation to account for modeling inaccuracies within their robotic control system algorithms.

simulation↗
DOE OSTI2021

New Capability at ORNL: High Precision Uranium Titration

Destructive analytical measurements establish a nuclear facility’s nuclear material inventory and inventory differences for Nuclear Material Accountancy and Control. A nuclear laboratory’s ability to perform accurate high-precision analytical measurements is key for tracking large inventories within a facility’s material balance areas and during production to track material movement through dynamic processes. For uranium, these measurements are made by using several established high-precision measurement protocols. These include isotope dilution mass spectrometry, gravimetry, and potentiometric titrations. Whatever measurement technique a nuclear lab chooses to use, reference materials (RMs) with certified attributes and accompanying uncertainties are used to calibrate measurement systems, and are the cornerstone for accurate results. In addition to calibration, RMs provide for metrological traceability, are used for method development and validation, and thus provide critical evaluations of the appropriateness and performance of analytical processes used. Evaluations may include validation that a method is fit-for-purpose, quantification of systematic and random biases, and the evaluation of long-term and short-term performance metrics. High-precision measurement techniques require that measured attributes be certified to a high degree of precision in the RMs used—ultimately, to a higher degree than that of the measurement technique itself. The US authority on the production of special nuclear material Certified Reference Materials is the NBL Program Office (NBLPO), formally known as New Brunswick Laboratory (NBL). The NBLPO is responsible for the sales and distribution of existing NBL certified reference materials (CRMs) and for the production of the next generation of nuclear RMs. To accomplish its mission, NBLPO is establishing key base capabilities within the DOE laboratory complex that formerly existed at the NBL laboratory. The Nuclear Analytical Chemistry (NAC) section within the Chemical Sciences Division (CSD) at Oak Ridge National Laboratory (ORNL) is currently working with NBLPO to set up laboratory and measurement capabilities to provide measurements and capabilities for production and/or recertification of existing and future CRMs for uranium assay. The NBL-developed high-precision titration (HPT) method is a critically-evaluated, extremely precise and accurate primary method utilized for the determination of uranium content in a variety of uranium materials. The HPT method, combined with detailed balance weighing protocols, provides for an analytical methodology that is unsurpassed in precision and one in which all sources of error have been evaluated, a requirement of CRM certification. HPT capability within the United States was lost with the closure of the labs at NBL. The NAC has been collaborating with NBLPO to stand up and demonstrate the capability to perform uranium assay via HPT at ORNL. HPT can produce results with an expanded uncertainty of approximately 0.01% for pure uranium compounds, with typical precisions of <0.006%. The major tasks required to stand up the method at ORNL were the refurbishment of a dedicated lab and equipment setup, procedure development, analyst training, establishing method-specific quality assurance, and qualification of an analyst to perform the method. This report summarizes these tasks, outlines the documents drafted, and gives the outcome of the qualification titrations.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗
NASA NTRS1990

High-precision orbit determination for high-earth elliptical orbiters using the Global Positioning System

Orbit covariance analyses pertaining to the Japanese VLBI Space Observatory Program (VSOP) MUSES-B satellite and to the International VLBI Satellite are presented. It is determined that a combination of Doppler and GPS measurements can provide the orbit accuracy required to support advanced radio interferometric experiments. For the VSOP, the required orbit accuracy of 130 m is easily met with two-way Doppler as the primary type of data; the 0.4 cm/s VSOP velocity requirement is also feasible provided that precise ground calibrations of tropospheric delays and station coordinates are available. It is concluded that combining the data from a VSOP GPS flight instrument with the ground GPS and two-way Doppler data will significantly enhance orbit determination accuracy in position and velocity.

Lichten, S. M.↗
NASA NTRS2007

High-Precision Nd Isotopes in Picrites from Hawaii and Iceland - No Evidence for an Early-Formed Enriched Reservoir

New high-precision Nd isotope measurements have shown that the present-day Nd-142/Nd-144 for average chondrites is approximately 20 ppm lower than that for the terrestrial standard and all recent mantle-derived samples measured to date. One explanation for these differences is that an enriched missing reservoir with lower Nd-142/Nd-144 resides in the mantle to balance the bulk Earth to chondritic. Data from Archean Greenland rocks show anomalies in Nd-142/Nd-144 of up to 40 ppm higher than the proposed average for chondrites. This difference between the Archean Greenland rocks and present-day mantle-derived samples has been interpreted to result from remixing of an early-formed enriched reservoir into the convecting mantle during the Archean. If so, the implication from this is that remixing of the enriched reservoir largely shut down some time in the past such that it must at present reside in a region in the mantle that infrequently participates dynamically and leading to volcanism at the surface. Several studies have suggested that the missing reservoir may be present just above the coremantle boundary (CMB). Depending on the size of this reservoir it could potentially make up all of D or exist as distinct domains within it. If such a reservoir does exist, then mantle-derived samples from plume systems that are thought to come from the CMB may be the best opportunity to identify this component using high-precision Nd isotope measurements. To test this, picrites from Hawaii with coupled enrichments in Os-186-Os-187 that has been proposed to be a signature of core-mantle interaction were measured on the JSC Triton for high-precision Nd-142/Nd-144. For comparison, picrites from Hawaii and Iceland that do not show coupled enrichments in Os-186-Os-187 were measured. We have established an external precision for Nd-142/Nd-144 of 3.6 ppm (2 sigma) during the analytical campaign. The Iceland (n=5) and Hawaiian data (n=9) have Nd-142 ranging from -0.01 plus or minus 0.03 to +0.03 plus or minus 0.03 (2 sigma) and there is no resolvable difference between samples with Os isotope enrichments versus those without. The average epsilon Nd-142 of +0.011 plus or minus 0.034 (2 sigma ) for all of the samples (n=14) is not resolvable from the Ames and La Jolla standards with epsilon Nd-142 of +0.000 plus or minus 0.036 (n=16, 2 sigma). These data confirm recent measurements on lavas for the absence of an ancient enriched Nd-142 isotopic signature in plume systems likely derived from D and indicates that such a reservoir, if existing, must now reside in areas of the deep mantle that plumes do not sample.

Brandon, A. D.↗
DOE OSTI2026

Creating high-precision reference gas standards of 85Kr for groundwater age-dating

Absolute gas counting (AGC) was applied to two gas blends of 85Kr in argon-methane (P10) counting gas to establish a high-precision specific activity (Bq/cm3) reference value for characterizing 85Kr detection efficiency for groundwater age dating measurements. The AGC or length-compensated technique has been utilized by the metrology community for decades and is an accepted method for developing radioactive gas standards. The AGC capability at Pacific Northwest National Laboratory (PNNL) uses a set of nine unequal-length proportional counters with precisely-measured internal volumes, and a gas loading system with high-precision pressure and temperature sensors. A series of AGC measurements were collected at multiple pressures to determine the inverse pressure relationship (1/P) for 85Kr and define a wall-effect correction that accounts for events decaying into the detector wall and not depositing sufficient energy in the gas to be detected. In addition to the wall-effect, two additional corrections were evaluated and are discussed in detail. Specifically, the threshold effect which accounts for events deposited below the analysis threshold and a detection efficiency as a function of detector volume effect that was observed during analysis. A robust uncertainty model was developed using the Guide to the expression of Uncertainty in Measurements (GUM) approach. The combination of carefully scrutinized correction factors, precise measurements of pressure, temperature and detector volume, and robust counting statistics resulted in the determination of high-precision specific activity values with 0.50% or less total combined uncertainty for two Kr-in-P10 reference gas standards (KP10) that will enable new groundwater age-dating measurements at PNNL.

Kr-85↗
DOE OSTI2024

3D Reconstruction of a High-Energy Diffraction Microscopy Sample Using Multi-modal Serial Sectioning with High-Precision EBSD and Surface Profilometry

High-energy diffraction microscopy (HEDM) combined with in situ mechanical testing is a powerful nondestructive technique for tracking the evolving microstructure within polycrystalline materials during deformation. This technique relies on a sophisticated analysis of X-ray diffraction patterns to produce a three-dimensional reconstruction of grains and other microstructural features within the interrogated volume. However, it is known that HEDM can fail to identify certain microstructural features, particularly smaller grains or twinned regions. Characterization of the identical sample volume using high-resolution surface-specific techniques, particularly electron backscatter diffraction (EBSD), can not only provide additional microstructure information about the interrogated volume but also highlight opportunities for improvement of the HEDM reconstruction algorithms. In this study, a sample fabricated from undeformed “low solvus, high refractory” nickel-based superalloy was scanned using HEDM. The volume interrogated by HEDM was then carefully characterized using a combination of surface-specific techniques, including epi-illumination optical microscopy, zero-tilt secondary and backscattered electron imaging, scanning white light interferometry, and high-precision EBSD. Custom data fusion protocols were developed to integrate and align the microstructure maps captured by these surface-specific techniques and HEDM. The raw and processed data from HEDM and serial sectioning have been made available via the Materials Data Facility (MDF) at https://doi.org/10.18126/4y0p-v604 for further investigation.

36 MATERIALS SCIENCE↗