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At least 19 records

Boundary-layer effects in composite laminates: Free-edge stress singularities, part 6

A rigorous mathematical model was obtained for the boundary-layer free-edge stress singularity in angleplied and crossplied fiber composite laminates. The solution was obtained using a method consisting of complex-variable stress function potentials and eigenfunction expansions. The required order of the boundary-layer stress singularity is determined by solving the transcendental characteristic equation obtained from the homogeneous solution of the partial differential equations. Numerical results obtained show that the boundary-layer stress singularity depends only upon material elastic constants and fiber orientation of the adjacent plies. For angleplied and crossplied laminates the order of the singularity is weak in general.

Wanag, S. S.↗

Acoustoelastic characterization of plates using zero group velocity Lamb modes

Acoustoelasticity, a characteristic of material anharmonicity, gives rise to a link between wave propagation velocity and the stress state in materials. Ultrasonic techniques to monitor this coupling, particularly with high sensitivity and in a noncontact manner, can have widespread application both in the quantification of applied and residual stress and in the characterization of nonlinear material behavior through measurement of higher order elastic constants. Here, we use a laser ultrasonic technique to excite and detect zero group velocity (ZGV) Lamb wave resonances in aluminum plates under uniaxial loading. A laser line source is used to excite these resonances at different orientations with respect to the applied load, and the signals are detected using an interferometer. The effects of stress and source orientation on ZGV resonance frequencies are validated using the theory of acoustoelastic Lamb wave propagation. In addition, a model-based inversion technique is used to extract Murnaghan's third-order elastic constants from measurements of the stress dependence of the first two ZGV modes generated parallel and perpendicular to the applied load. Laser generation and detection of ZGV resonances is shown to be an effective and powerful approach for the noncontact and nondestructive acoustoelastic characterization of elastic waveguides.

36 MATERIALS SCIENCE↗

Elastic constants at low temperatures - Recent measurements on technological materials at NBS

Solid-state low-temperature elastic properties have been experimentally studied at the NBS Cryogenic Division for four years. Most studies were between room temperature and liquid-helium temperature; some were only to liquid-nitrogen temperature. Two dynamic (high-frequency) experimental methods were used, pulse-echo and resonance, resulting in adiabatic elastic constants. The present paper reviews these studies for 47 technological materials - metals, alloys, and composites. The elastic constants primarily discussed are Young's modulus, the shear modulus, the bulk modulus (reciprocal compressibility), and Poisson's ratio. A summary table is presented to show which base metals tend to exhibit regular, irregular, or anomalous behavior in their elastic constant/temperature curves.

Ledbetter, H. M.↗

3D mapping of residual stresses in growing grains of partially recrystallized Gum Metal

The crystallographic orientations and residual stresses within recrystallizing grains in partially recrystallized beta titanium-Gum Metal-were examined non-destructively in 3D using synchrotron Differential Aperture X-ray Microscopy. Contrary to common assumptions, significant local stresses and stress variations are observed within the recrystallizing grains. The results reveal that the development of these local residual stresses depends on the plastic deformation mode and material's elastic constants, rather than grain properties such as size and orientation, or even the material's yield stress. This work provides insights valuable for the design of advanced materials with heterogeneous microstructures.

36 MATERIALS SCIENCE↗

High temperature materials characterization

A lab facility for measuring elastic moduli up to 1700 C was constructed and delivered. It was shown that the ultrasonic method can be used to determine elastic constants of materials from room temperature to their melting points. The ease in coupling high frequency acoustic energy is still a difficult task. Even now, new coupling materials and higher power ultrasonic pulsers are being suggested. The surface was only scratched in terms of showing the full capabilities of either technique used, especially since there is such a large learning curve in developing proper methodologies to take measurements into the high temperature region. The laser acoustic system does not seem to have sufficient precision at this time to replace the normal buffer rod methodology.

Workman, Gary L.↗

Thermo-acoustoelastic effect of Rayleigh wave: Theory and experimental verification

Previous studies showed that the thermally-induced ultrasonic bulk wave velocity change could be used to measure acoustoelastic coefficients and third-order elastic constants of elastic materials. This method is naturally immune from the ambient temperature effect and has improved sensitivity and a simpler test setup than the conventional acoustoelastic test. However, Rayleigh wave is preferred for thick components or structures with only one accessible surface. In this work, the thermo-hyperelastic constitutive equation, along with acoustoelastic theory, is used to derive the expression of the thermo-acoustoelastic coefficient (TAEC) of Rayleigh wave. The numerical relationship between the TAEC of Rayleigh wave and Murnaghan constants ( l, m and n ) are given for common metals. Further, the TAEC expressions for Rayleigh wave and shear wave are similar, and both are dominated by the constant m . The TAEC of Rayleigh wave was measured on an aluminum 6061 specimen using the thermal modulation experiment in a temperature range of 22 ~ 35°C. The measured TAEC shows good agreement with the theoretical calculation. Then the third-order elastic constants were calculated based on TAECs of bulk waves and Rayleigh wave.

42 ENGINEERING↗

Skyrmion lattice creep at ultra-low current densities

Abstract Magnetic skyrmions are well-suited for encoding information because they are nano-sized, topologically stable, and only require ultra-low critical current densities j c to depin from the underlying atomic lattice. Above j c skyrmions exhibit well-controlled motion, making them prime candidates for race-track memories. In thin films thermally-activated creep motion of isolated skyrmions was observed below j c as predicted by theory. Uncontrolled skyrmion motion is detrimental for race-track memories and is not fully understood. Notably, the creep of skyrmion lattices in bulk materials remains to be explored. Here we show using resonant ultrasound spectroscopy—a probe highly sensitive to the coupling between skyrmion and atomic lattices—that in the prototypical skyrmion lattice material MnSi depinning occurs at $${j}_{c}^{* }$$ j c * that is only 4 percent of j c . Our experiments are in excellent agreement with Anderson-Kim theory for creep and allow us to reveal a new dynamic regime at ultra-low current densities characterized by thermally-activated skyrmion-lattice-creep with important consequences for applications.

36 MATERIALS SCIENCE↗

Nondestructive determination of mechanical properties

The sensitivity of the velocity of ultrasonic waves to the elasticity of the materials (acousto-elastic constant - AEC) as controlled by the microstructure of the materials was examined experimentally. Rolled-plate specimens of five different Al alloys were subjected to tensile tests while being monitored for the velocity change of a 10 MHz longitudinal wave as a function of the applied tensile stress. The acoustic propagation velocity was measured perpendicularly to the stress. Determinations were made of the yield strength and the hardnesses of the specimens. Samples of the plate materials examined microscopically to characterize the solid phases. The AECs varied linearly with the percentage of solid solution phase of the alloys. The trend for strain-hardened samples was, however, opposite from that in the precipitation-hardened alloys. The results underscore the necessity of considering the microstructural dependencies of the AECs when using ultrasonic NDE methods, and also opened the potential of determining some mechanical properties with NDE techniques.

Schneider, E.↗

Effect of stress and temperature on zero group velocity Lamb modes

Zero group velocity (ZGV) Lamb wave resonances are highly localized and sensitive to changes in material properties, making them a viable option for probing residual stresses and elastic nonlinearity through acoustoelastic effects. Temperature changes also influence ZGV modes and need to be accounted for, particularly when measuring the small frequency shifts associated with acoustoelastic effects. We use a laser-based ultrasonic system to measure the third-order elastic constants of several materials. A temperature compensation scheme is devised to remove the effects of temperature fluctuations from the measurements. Furthermore, the measured third-order elastic constants are used to predict the temperature dependence of the ZGV resonances using thermo-acoustoelasticity theory, and these predictions are compared to experimental measurements. We find that thermo-acoustoelasticity theory was unable to reliably predict the shift in ZGV resonances with temperature. These results could have important implications in understanding the limitations of thermo-acoustoelasticity theory and in developing precision ZGV resonance-based systems to detect and quantify residual stress in parts, a particularly relevant problem in additive manufacturing techniques including powder bed fusion and directed energy deposition.

Engineering↗

An exactly solvable model for calculating critical misfit and thickness in epitaxial superlattices - Layers of equal elastic constants and thicknesses

A parabolic interaction potential has been used to develop a model for calculating the misfit dislocation (MD) energy in the case of a superlattice of alternating layers of materials with equal elastic constants and thicknesses. The model, which is believed to be a good one for small misfits and to have some merit for covalent bonded materials, is exactly solvable for the critical thickness above which it is energetically favorable to lose coherency by the introduction of MDs into the interfaces. It was found, for a given misfit f, that the critical thickness for epitaxial superlattices free from their substrate is somewhat more than four times that for a single epilayer on a thick substrate. Furthermore, the critical thickness varies almost inversely with misfit to the power 1.22 when Poisson's ratio is 1/3. It was also shown that the critical misfit f(c) obtained by equating maximal misfit strain and MD energies is a significant overestimate of f(c). The results for a superlattice are compared with those of a thin layer on a thick substrate.

Van Der Merwe, Jan H.↗

Composite Materials NDE Using Enhanced Leaky Lamb Wave Dispersion Data Acquisition Method

The leaky Lamb wave (LLW) technique is approaching a maturity level that is making it an attractive quantitative NDE tool for composites and bonded joints. Since it was first observed in 1982, the phenomenon has been studied extensively, particularly in composite materials. The wave is induced by oblique insonification using a pitch-catch arrangement and the plate wave modes are detected by identifying minima in the reflected spectra to obtain the dispersion data. The wave behavior in multi-orientation laminates has been well documented and corroborated experimentally with high accuracy. The sensitivity of the wave to the elastic constants of the material and to the boundary conditions led to the capability to measure the elastic properties of bonded joints. Recently, the authors significantly enhanced the LLW method's capability by increasing the speed of the data acquisition, the number of modes that can be identified and the accuracy of the data inversion. In spite of the theoretical and experimental progress, methods that employ oblique insonification of composites are still not being applied as standard industrial NDE methods. The authors investigated the issues that are hampering the transition of the LLW to industrial applications and identified 4 key issues. The current capability of the method and the nature of these issues are described in this paper.

Bar-Cohen, Yoseph↗

An In-Depth Tutorial on Constitutive Equations for Elastic Anisotropic Materials

An in-depth tutorial on the constitutive equations for elastic, anisotropic materials is presented. Basic concepts are introduced that are used to characterize materials, and notions about how anisotropic material deform are presented. Hooke s law and the Duhamel-Neuman law for isotropic materials are presented and discussed. Then, the most general form of Hooke s law for elastic anisotropic materials is presented and symmetry requirements are given. A similar presentation is also given for the generalized Duhamel-Neuman law for elastic, anisotropic materials that includes thermal effects. Transformation equations for stress and strains are presented and the most general form of the transformation equations for the constitutive matrices are given. Then, specialized transformation equations are presented for dextral rotations about the coordinate axes. Next, concepts of material symmetry are introduced and criteria for material symmetries are presented. Additionally, engineering constants of fully anisotropic, elastic materials are derived from first principles and the specialized to several cases of practical importance.

Nemeth, Michael P.↗

Estimation of the engineering elastic constants of a directionally solidified superalloy for finite element structural analysis

The temperature-dependent engineering elastic constants of a directionally solidified nickel-base superalloy were estimated from the single-crystal elastic constants of nickel and MAR-MOO2 superalloy by using Wells' method. In this method, the directionally solidified (columnar-grained) nickel-base superalloy was modeled as a transversely isotropic material, and the five independent elastic constants of the transversely isotropic material were determined from the three independent elastic constants of a cubic single crystal. Solidification for both the single crystals and the directionally solidified superalloy was assumed to be along the (001) direction. Temperature-dependent Young's moduli in longitudinal and transverse directions, shear moduli, and Poisson's ratios were tabulated for the directionally solidified nickel-base superalloy. These engineering elastic constants could be used as input for performing finite element structural analysis of directionally solidified turbine engine components.

Abdul-Aziz, Ali↗

Irradiation Behavior of Piezoelectric Materials for Nuclear Reactor Sensors

In-situ measurement of surface acoustic wave (SAW) resonators were used to characterize piezoelectric materials behavior in a nuclear reactor environment. Lithium niobate and aluminum nitride devices were tested up to 500°C temperature and 450 kW reactor power (1.9x10 12 n/cm 2 s). The resonant frequency responds to step changes in temperature and power. Materials’ response are inferred from the observed resonant frequency changes, in particular the kinetic behavior is used to determine mechanisms responsible for observed changes. The observed response is attributed to two mechanisms: temperature increase from gamma heating and accumulation of radiation-induced defects. Both of these mechanisms alter the physical properties of the piezoelectric materials, particularly the elastic constants. The demonstrated repeatability and reliability of SAW devices are attractive for sensor applications in extreme environments.

36 MATERIALS SCIENCE↗

Multiplexed ultrasonic system

A system which rapidly determines the elastic stiffness constants of materials in plate shape as well as characterize material flaws that are affecting these constants. Rapid (below a minute) nondestructive evaluation system allow for the determination of material stiffness constants, low noise data acquisition algorithm for measuring spectral data. A real time method of displaying leaky Lamb wave spectral data.

Bar-Cohen, Yoseph↗