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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2025

Development of a Flow Stabilization Algorithm Enabling Measurement of Low Oxygen Concentrations in Liquid Sodium

To enhance the automated control of the plugging meter (PM) and thereby enhance detection fidelity in ultralow oxygen environments [≤1 parts per million by weight (wppm)], a novel proportional derivative controller has been implemented with conventional PM hardware. This ramp sign stabilized flow (RSSF) controller manipulates the sign (heating or cooling direction) at a fixed rate, enabling precise temperature adjustment around the saturation temperature of the bulk sodium. This adjustment helps maintain flow stability in a partially formed sodium oxide plug, thus greatly reducing the temperature amplitude in the plugging cycle and promoting simple and accurate oxygen determinations in addition to an increased sampling rate. Rather than relying on the subjective nature of indexing the time when the flow rate changes due to the plugging or unplugging onset to the PM temperature, a running average of the correlated oxygen concentration with time over multiple plugging events can provide oxygen readings ranging from an absolute uncertainty of 500 wppb in real time to less than 50 wppb for a 24-h sampling window. Finally, the RSSF controller was tested at 508 ± 7 wppb with measured oxygen of 542 ± 179 wppb, further reducing the variance between the saturation temperature and the plugging temperature.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2022

The response of accident tolerant fuel cladding to LOCA burst testing: A comparative study of leading concepts

Accident tolerant fuel claddings seek to improve safety margins during loss-of-coolant accident (LOCA) scenarios by reducing cladding steam oxidation rates, hydrogen production, delaying or mitigating cladding burst, and reducing cladding deformation. After rapid and extensive progress in recent years, Cr coated Zr-based alloys, ferritic FeCrAl, and SiC/SiC ceramic matrix composites (CMCs) have emerged as the most promising cladding concepts, but there are few studies comparing the accident tolerance of all three concepts simultaneously. Here, in this study, LOCA burst testing has been conducted on Cr high impulse power magnetron sputtered Zry-4 (Cr/Zry-4), C26M (FeCrAl), and SiC/SiC SiGA (CMC). Experimental observations indicate Cr/Zry-4 burst at higher temperatures than Zry-4 however the effectiveness of the coating on mitigating ZrO 2 formation via Cr 2 O 3 formation depended on physical proximity to the burst opening. No dramatic improvement in diametrical strain nor opening geometry was observed. C26M burst at higher temperatures than Zry-4 at lower pressures, exhibiting small amounts of strain and smaller openings, and formed slow-growing Al 2 O 3 regardless of location. The CMCs did not burst or show any macroscopic signs of deformation, all the way up to an internal cladding pressure of 15.2 MPa. High temperature expanding Nb plug testing indicated that CMC room temperature strength may persist up to 1650°C, with an approximately 40% loss of strength at 1900°C. CMC steam oxidation was also compared to reference chemically vapor deposited SiC up to 1700°C, and CMCs were found to oxidize at slightly accelerated rates that were still orders of magnitude lower than bare Zry-4. Projected H 2 generation during LOCA burst testing showed that when accounting for cladding burst exposing inner diameters to steam, Cr coated Zry-4 reduced H 2 generation by a factor of two compared with bare Zry-4, while both C26M and SiC/SiC reduced H 2 generation by orders of magnitude relative to bare Zry-4.

36 MATERIALS SCIENCE↗
NASA NTRS1943

Operating Temperatures of a Sodium-Cooled Exhaust Valve as Measured by a Thermocouple

A thermocouple was installed in the crown of a sodium-cooled exhaust valve. The valve was then tested in an air-cooled engine cylinder and valve temperatures under various engine operating conditions were determined. A temperature of 1337 F was observed at a fuel-air ratio of 0.064, a brake mean effective pressure of 179 pounds per square inch, and an engine speed of 2000 rpm. Fuel-air ratio was found to have a large influence on valve temperature, but cooling-air pressure and variation in spark advance had little effect. An increase in engine power by change of speed or mean effective pressure increased the valve temperature. It was found that the temperature of the rear spark-plug bushing was not a satisfactory indication of the temperature of the exhaust valve.

FUEL-AIR MIXTURES↗
NASA NTRS1943

Operating Temperatures of a Sodium-Cooled Exhaust Valve as Measured by a Thermocouple

Report presents the results of a thermocouple installed in the crown of a sodium-cooled exhaust valve. The valve was tested in an air-cooled engine cylinder and valve temperatures under various engine operating conditions were determined. A temperature of 1337 degrees F. was observed at a fuel-air ratio of 0.064, a brake mean effective pressure of 179 pounds per square inch, and an engine speed of 2000 r.p.m. Fuel-air ratio was found to have a large influence on valve temperature, but cooling-air pressure and variation in spark advance had little effect. An increase in engine power by change of speed or mean effective pressure increased the valve temperature. It was found that the temperature of the rear-spark-plug bushing was not a satisfactory indication of the temperature of the exhaust valve.

Sanders, J C↗
NASA NTRS1946

Effect of Fuel Composition, Engine Operating Variables, and Spark-Plug Type and Condition on Preignition-Limited Performance of an R-2800 Cylinder

The preignition characteristics of the R-2800 cylinder, as effected by fuel consumption, engine operating variables, and spark plug type and condition, were evaluated. The effects on preignition-limited performance of various percentages of aromatics (benzene, toluene, cumene, xylene) in a base fuel of triptane were investigated. Two paraffins (triptane and S + 6.0 ml TEL/gal) and two refinery blends (28-R and 33-R) were preignition rated. The effect of changes in the following engine operating variables on preignition limit was determined: inlet-air temperature, rear spark plug gasket temperature, engine speed, spark advance, tappet clearance, and oil consumption. Preignition limits of the R-2800 cylinder using Champion C34S and C35S and AC-LS86, LS87, and LS88 spark plugs were established and the effect of spark plug deterioration was investigated. No definite trends in preignition-limited indicated mean effective pressure were indicated for aromatics as a class when increased percentages of different aromatics were added to a base fuel of triptane. Three types of fuel (aromatics, paraffins, and refinery blends) showed a preignition range for this cylinder from 65 to 104 percent when based on the performance of S plus 6.0 ml TEL per gallon as 100 percent. The R-2800 cylinder is therefore relatively insensitive to fuel composition when compared to a CFR F-4 engine, which had a pre-ignition range from 72 to 100 percent for the same fuels. Six engine operating variables were investigated with the following results: preignition-limited indicated mean effective pressure decreased, with increases in engine speed, rear spark plug gasket temperature, inlet-air temperature, and spark advance beyond 20 F B.T.C. and was unaffected by rate of oil consumption or by tappet clearance. Spark plugs were rated over a range of preignition-limited indicated mean effective pressure from 200 to 390 pounds per square inch at a fuel-air ratio of 0.07 in the following order of increased resistance to preignition: AC-LS97, AC-LS88, Champion C358, AC-LS86, and Champion C34S. Spark plug deterioration in the form of cracks in the porcelain had been broken away from the center electrode and were retained in the spark plug cavity, the preignition limit was decreased as much as 57 percent. When the broken pieces had been removed, the preignition limit increased from that of the undamaged porcelain as the weight of removed porcelain was increased.

Pfender, John F.↗
NASA NTRS1940

Correlation of knocking characteristics of fuels in an engine having a hemispherical combustion chamber

Data are presented to show the effects of inlet-air pressure, inlet-air temperature, and compression ratio on the maximum permissible performance obtained with having a hemispherical-dome combustion chamber. The five aircraft-engine fuels used have octane numbers varying from 90 to 100 plus 2 ml of tetraethyl lead per gallon. The data were obtained on a 5 1/4-inch by 4 3/4-inch liquid-cooled engine operating at 2,500 r.p.m. The compression ratio was varied from 6.0 to 8.9. The inlet-air temperature was varied from 110 to 310 F. For each set of conditions, the inlet-air pressure was increased until audible knock occurred and then reduced 2 inches of mercury before data were recorded. The results for each fuel can be correlated by plotting the calculated end-gas density factor against the calculated end-gas temperature. Measurements of spark-plugs, cutting off the switch to one spark plug lowered the electrode temperature of that plug from a value of 1,365 F to a value of 957 F. The results indicate that the surface temperatures of combustion-chamber areas which become new sources of ignition markedly increase after ignition.

Rothrock, A M↗
NASA NTRS2008

NaK Plugging Meter Design for the Feasibility Test Loops

The design and predicted performance of a plugging meter for use in the measurement of NaK impurity levels are presented. The plugging meter is incorporated into a Feasibility Test Loop (FTL), which is a small pumped-NaK loop designed to enable the rapid, small-scale evaluation of techniques such as in situ purification methods and to permit the measurement of bulk material transport effects (not mechanisms) under flow conditions that are representative of a fission surface power reactor. The FTL operates at temperatures similar to those found in a reactor, with a maximum hot side temperature of 900 K and a corresponding cold side temperature of 860 K. In the plugging meter a low flow rate bypass loop is cooled until various impurities (primarily oxides) precipitate out of solution. The temperatures at which these impurities precipitate are indicative of the level of impurities in the NaK. The precipitates incrementally plug a small orifice in the bypass loop, which is detected by monitoring changes in the liquid metal flow rate.

Pearson, J. Boise↗
NASA NTRS2016

Boundary Layer Transition During the Orion Exploration Flight Test 1 (EFT-1)

Boundary layer transition was observed in the thermocouple data on the windside backshell of the Orion reentry capsule. Sensors along the windside centerline, as well as off-centerline, indicated transition late in the flight at approximately Mach 4 conditions. Transition progressed as expected, beginning at the sensors closest to the forward bay cover (FBC) and moving towards the heatshield. Sensors placed in off-centerline locations did not follow streamlines, so the progression of transition observed in these sensors is less intuitive. Future analysis will include comparisons to pre-flight predictions and expected transitional behavior will be investigated. Sensors located within the centerline and off-centerline launch abort system (LAS) attach well cavities on the FBC also showed indications of boundary layer transition. The transition within the centerline cavity was observed in the temperature traces prior to transition onset on the sensors upstream of the cavity. Transition behavior within the off centerline LAS attach well cavity will also be investigated. Heatshield thermocouples were placed within Avcoat plugs to attempt to capture transitional behavior as well as better understand the aerothermal environments. Thermocouples were placed in stacks of two or five vertically within the plugs, but the temperature data obtained at the sensors closest to the surface did not immediately indicate transitional behavior. Efforts to use the in depth thermocouple temperatures to reconstruct the surface heat flux are ongoing and any results showing the onset of boundary layer transition obtained from those reconstructions will also be included in this paper. Transition on additional features of interest, including compression pad ramps, will be included if it becomes available.

Kirk, Lindsay C.↗
NASA NTRS2011

Online Oxide Contamination Measurement and Purification Demonstration

Liquid metal sodium-potassium (NaK) has advantageous thermodynamic properties indicating its use as a fission reactor coolant for a surface (lunar, martian) power system. A major area of concern for fission reactor cooling systems is system corrosion due to oxygen contaminants at the high operating temperatures experienced. A small-scale, approximately 4-L capacity, simulated fission reactor cooling system employing NaK as a coolant was fabricated and tested with the goal of demonstrating a noninvasive oxygen detection and purification system. In order to generate prototypical conditions in the simulated cooling system, several system components were designed, fabricated, and tested. These major components were a fully-sealed, magnetically-coupled mechanical NaK pump, a graphite element heated reservoir, a plugging indicator system, and a cold trap. All system components were successfully demonstrated at a maximum system flow rate of approximately 150 cc/s at temperatures up to 550 C. Coolant purification was accomplished using a cold trap before and after plugging operations which showed a relative reduction in oxygen content.

Bradley, D. E.↗
NASA NTRS2003

Catalyzed Combustion of Bipropellants for Micro-Spacecraft Propulsion

This paper addresses the need to understand the physics and chemistry involved in propellant combustion processes in micro-scale combustors for propulsion systems on micro-spacecraft. These spacecraft are planned to have a mass less than 50 kilograms with attitude control estimated to be in the 10 milli-Newton thrust class. These combustors are anticipated to be manufactured using Micro Electrical Mechanical Systems (MEMS) technology and are expected to have diameters approaching the quenching diameter of the propellants. Combustors of this size are expected to benefit significantly from surface catalysis processes. Miniature flame tube apparatus is chosen for this study because microtubes can be easily fabricated from known catalyst materials and their simplicity in geometry can be used in fundamental simulations for validation purposes. Experimentally, we investigated the role of catalytically active surfaces within 0.4 and 0.8 mm internal diameter microtubes, with special emphases on ignition processes in fuel rich gaseous hydrogen and gaseous oxygen. Flame thickness and reaction zone thickness calculations predict that the diameters of our test apparatus are below the quenching diameter of the propellants in sub-atmospheric tests. Temperature and pressure rise in resistively heated platinum and palladium microtubes was used as an indication of exothermic reactions. Specific data on mass flow versus preheat temperature required to achieve ignition are presented. With a plug flow model, the experimental conditions were simulated with detailed gas-phase chemistry, thermodynamic properties, and surface kinetics. Computational results generally support the experimental findings, but suggest an experimental mapping of the exit temperature and composition is needed.

Schneider, Steven J.↗
NASA NTRS2008

Igniters for Liquid Oxygen/Liquid Methane Technology Development

As part of NASA's technology development of liquid methane / liquid oxygen engines for future exploration missions, two different igniters were recently studied at NASA Marshall Space Flight Center. The first igniter tested was an impinging injection, spark-initiated torch igniter, and the second was a microwave-generated plasma igniter. The purpose of the ignition tests was to define the ignition limits under vacuum conditions and characterize the transient start-up performance as a function of propellant mixture ratio (MR), mass flow rates, inlet temperatures, and pre-ignition chamber pressure. In addition, for the impinging igniter two different spark plugs were tested, and for the microwave igniter the magnetron filament warm-up time and the magnetron input power were both varied. The results gathered from these tests indicated that the impinging igniter is capable of operating over an MR range of 2 - 27, with methane and oxygen inlet temperatures as low as -161 F and -233 F, respectively. The microwave igniter was tested over an MR range of 2 - 9, with methane and oxygen inlet temperatures as low as -90 F and -200 F, respectively. The microwave igniter achieved ignition over this range, although an upper ignition limit was determined for the oxidizer mass flow rate. In general, the torch exhaust temperatures for the microwave igniter were not as high as those attained with the impinging igniter. The microwave igniter, however, was hot-fired 17 times and was still operational, whereas the impinging igniter spark plugs experienced thermal shock and erosion over nine hot-fire tests. It was concluded that for the microwave igniter better mixing of the propellants might be required in order to both raise the torch exhaust temperature and decrease the required magnetron input power, and for the impinging igniter the spark plug position within the igniter chamber should be varied in future tests to identify a more optimal location. All of the igniter tests were supported by the Propulsion & Cryogenics Advanced Development project, which is part of NASA's Exploration Technology Development Program.

Osborne, Robin J.↗
NASA NTRS2011

Isotherm Sensor Calibration Program for Mars Science Laboratory Heat Shield Flight Data Analysis

Seven instrumented sensor plugs were installed on the Mars Science Laboratory heat shield in December 2008 as part of the Mars Science Laboratory Entry, Descent, and Landing Instrumentation (MEDLI) project. These sensor plugs contain four in-depth thermocouples and one Hollow aErothermal Ablation and Temperature (HEAT) sensor. The HEAT sensor follows the time progression of a 700 C isotherm through the thickness of a thermal protection system (TPS) material. The data can be used to infer char depth and, when analyzed in conjunction with the thermocouple data, the thermal gradient through the TPS material can also be determined. However, the uncertainty on the isotherm value is not well defined. To address this uncertainty, a team at NASA Ames Research Center is carrying out a HEAT sensor calibration test program. The scope of this test program is described, and initial results from experiments conducted in the laboratory to study the isotherm temperature of the HEAT sensor are presented. Data from the laboratory tests indicate an isotherm temperature of 720 C 60 C. An overview of near term arc jet testing is also given, including preliminary data from 30.48cm 30.48cm PICA panels instrumented with two MEDLI sensor plugs and tested in the NASA Ames Panel Test Facility. Forward work includes analysis of the arc jet test data, including an evaluation of the isotherm value based on the instant in time when it reaches a thermocouple depth.

Santos, Jose A.↗
DOE OSTI2021

Fast wide-field upconversion luminescence lifetime thermometry enabled by single-shot compressed ultrahigh-speed imaging

Photoluminescence lifetime imaging of upconverting nanoparticles is increasingly featured in recent progress in optical thermometry. Despite remarkable advances in photoluminescent temperature indicators, existing optical instruments lack the ability of wide-field photoluminescence lifetime imaging in real time, thus falling short in dynamic temperature mapping. Here, we report video-rate upconversion temperature sensing in wide field using single-shot photoluminescence lifetime imaging thermometry (SPLIT). Developed from a compressed-sensing ultrahigh-speed imaging paradigm, SPLIT first records wide-field luminescence intensity decay compressively in two views in a single exposure. Then, an algorithm, built upon the plug-and-play alternating direction method of multipliers, is used to reconstruct the video, from which the extracted lifetime distribution is converted to a temperature map. Using the core/shell NaGdF 4 :Er 3+ ,Yb 3+ /NaGdF 4 upconverting nanoparticles as the lifetime-based temperature indicators, we apply SPLIT in longitudinal wide-field temperature monitoring beneath a thin scattering medium. SPLIT also enables video-rate temperature mapping of a moving biological sample at single-cell resolution.

47 OTHER INSTRUMENTATION↗
NASA NTRS1991

Visualization of the freeze/thaw characteristics of a copper/water heat pipe - Effects of non-condensible gas

The freeze/thaw characteristics of a copper/water heat pipe of rectangular cross section were investigated experimentally to determine the effect of variations in the amount of non-condensible gases (NCG) present. The transient internal temperature profiles in both the liquid and vapor channels are presented along with contours of the frozen fluid configuration obtained through visual observation. Several interesting phenomena were observed including total blockage of the vapor channel by a solid plug, evaporator dryout during restart, and freezing blowby. In addition, the restart characteristics are shown to be strongly dependent upon the shutdown procedure used prior to freezing, indicating that accurate prediction of the startup or restart characteristics requires a complete thermal history. Finally, the experimental results indicate that the freeze/thaw characteristics of room temperature heat pipes may be significantly different from those occurring in higher temperature, liquid metal heat pipes due to differences in the vapor pressures in the frozen condition.

Ochterbeck, J. M.↗
NASA NTRS2013

Alternate Methods in Refining the SLS Nozzle Plug Loads

Numerical analysis has shown that the SLS nozzle environmental barrier (nozzle plug) design is inadequate for the prelaunch condition, which consists of two dominant loads: 1) the main engines startup pressure and 2) an environmentally induced pressure. Efforts to reduce load conservatisms included a dynamic analysis which showed a 31% higher safety factor compared to the standard static analysis. The environmental load is typically approached with a deterministic method using the worst possible combinations of pressures and temperatures. An alternate probabilistic approach, utilizing the distributions of pressures and temperatures, resulted in a 54% reduction in the environmental pressure load. A Monte Carlo simulation of environmental load that used five years of historical pressure and temperature data supported the results of the probabilistic analysis, indicating the probabilistic load is reflective of a 3-sigma condition (1 in 370 probability). Utilizing the probabilistic load analysis eliminated excessive conservatisms and will prevent a future overdesign of the nozzle plug. Employing a similar probabilistic approach to other design and analysis activities can result in realistic yet adequately conservative solutions.

Burbank, Scott↗
NASA NTRSDate not supplied

Noise of Internally Mixed Exhaust Systems With External Plug For Supersonic Transport Applications

Internally mixed exhaust systems produce more noise than would be expected from an equivalent fully mixed flow. This ‘excess noise’ has never been fully explained and has not been researched recently as it is not as much of a problem for high bypass-ratio exhaust systems. Commercial supersonic vehicles, however, will use more moderate bypass ratio engines. Their exhaust systems will also likely feature external plugs to improve boat tail angle for cruise performance. Thus the problem of excess noise will need to be addressed along with the impacts of having an external plug. Recently, acoustic tests of dual-stream jet flows from both internal and external plug nozzles have been conducted. Measurements of noise from flows with an axisymmetric splitter and lobed forced mixer were made. These measurements show the baseline ‘excess noise’ previously found in forced mixer exhaust systems, and show how this noise source differs depending upon the plug geometry. Background-oriented schlieren measurements acquired simultaneously document the differences in shock structures over the transonic flow regime tested. The far-field acoustic measurements indicate that an external plug can slightly reduce the mixing noise of the jet plume when the flow is completely mixed, e.g. when the core and bypass streams have the same temperature and the flow is a single-stream jet. However, when the flow is not fully mixed, e.g. the usual case of an internally mixed exhaust system, the plug seems to amplify the ‘excess noise’ associated with the mixer. This additional noise source presents a challenge for nozzle designers wanting to use internally mixed exhaust systems with external plug nozzles.

Jet noise↗
DOE OSTI2022

Waste Control Specialists Technical Review Team Report

1. Modeling of Drum 68660 and the WCS Drums: A calibrated model of Los Alamos National Laboratory (LANL) Drum 68660 indicates that pressurization of the drum by restriction of drum venting could have led to the thermal runaway reaction at the Waste Isolation Pilot Plant (WIPP) in 2014, supporting the hypothesis that the contents of the drum were not fundamentally different from the overall remediated nitrate salt (RNS) waste stream. 2. Nitric Acid Reactions and Aging of the Waste: The stability of the WCS RNS waste with respect to autocatalytic thermal runaway due to nitric acid chemistry should increase over time as the nitric acid is depleted from chemical reactions in the drum. However, this cannot be confirmed because of the lack of long-term experimental data on the impact of aging on the reactivity of RNS waste. The calibrated model indicates that the waste drums retain most of their reactive components, metal nitrate salts and sWheat Scoop ® , even after eight years. 3. Pressure Effects and Runaway Reactions: The calibrated model indicates that if the drums and standard waste boxes (SWBs) are not allowed to pressurize during transport or storage and they are stored at historical WIPP repository temperatures, then an autocatalytic thermal runaway event is not expected to occur. Since the cause of Drum 68660 pressurization is not known, decision makers are not able to tailor mitigating strategies to the initiating event. Consequently, mitigating strategies must consider all feasible internal and external events that could lead to the pressurization of the drums. 4. Temperature Effects and Runaway Reactions: Temperature also has a strong influence on the stability of the waste. The calibrated model indicates that cooling the drums or SWBs can reduce the possibility of autocatalytic thermal runaway reactions. Simulations suggest that for a drum with a plugged vent, the probability of thermal runaway may be reduced or eliminated if wastes are maintained at or below 43 °F through active cooling measures from the initiation of transport until emplacement at WIPP.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
NASA NTRS1924

The effect of electrode temperature on the sparking voltage of short spark gaps

This report presents the results of an investigation to determine what effect the temperature of spark plug electrodes might have on the voltage at which a spark occurred. A spark gap was set up so that one electrode could be heated to temperatures up to 700 degrees C., while the other electrode and the air in the gap were maintained at room temperature. The sparking voltages were measured both with direct voltage and with voltage impulse from ignition coil. It was found that the sparking voltage of the gap decreased materially with increase of temperature. This change was more marked when the hot electrode was of negative polarity. The phenomena observed can be explained by the ionic theory of gaseous conduction, and serve to account for certain hitherto unexplained actions in the operation of internal combustion engines. These results indicate that the ignition spark will pass more readily when the spark-plug design is such as to make the electrodes run hot. This possible gain is, however, very closely limited by the danger of producing preignition. These experiments also show that sparking is somewhat easier when the hot electrode (which is almost always the central electrode) is negative than when the polarity is reversed.

Silsbee, F B↗