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At least 19 records

The Terrestrial Organism and Biogeochemistry Spatial Sampling Design for the National Ecological Observatory Network

The National Ecological Observatory Network (NEON) seeks to facilitate ecological prediction at a continental scale by measuring processes that drive change and responses at sites across the United States for thirty years. The spatial distribution of observations of terrestrial organisms and soil within NEON sites is determined according to a “design‐based” sample design that relies on the randomization of sampling locations. Development of the sample design was guided by high‐level NEON objectives and the multitude of data products that will be subjected to numerous analytical approaches to address the causes and consequences of ecological change. A requirement framework permeates the NEON design, ensuring traceability from each facet of the design to the high‐level requirements that make the NEON mission statement actionable. Requirements were developed for the terrestrial sample design to guide the key components of the design: Randomizing the sample locations ensures the unbiased collection of data, is appropriate for organisms and soil, and provides data suitable for a variety of analyses. Stratification increases efficiency and allows sampling to focus on those parts of the landscape measured by other NEON observation platforms. Attention to the sample size and spatial plot allocation ensures that data products will be sufficient to inform questions asked of the data and the NEON objectives. Establishing a framework with the capacity for re‐evaluate and design iteration allows for adaption to unexpected challenges and optimization of the sample design based on early data returns. The utility of the NEON sampling design is highlighted by its application across terrestrial systems. The data generated from this unique design will be used to quantify patterns in: the abundance and diversity of small mammals, breeding birds, insects, and soil microbes; vegetation structure, biomass, productivity, and diversity; and soil biogeochemistry.

National Ecological Observatory Network↗

LACIE sampling design

The sampling design in LACIE consisted of two major components, one for wheat acreage estimation and one for wheat yield prediction. The acreage design was basically a classical survey for which the sampling unit was a 5- by 6-nautical mile segment; however, there were complications caused by measurement errors and loss of data. Yield was predicted by sampling meteorological data from weather stations within a region and then using those data as input to previously fitted regression equations. Wheat production was not estimated directly, but was computed by multiplying yield and acreage estimates. The allocation of samples to countries is discussed as well as the allocation and selection of segments in strata/substrata.

Feiveson, A. H.↗

Development of rotation sample designs for the estimation of crop acreages

The idea behind the use of rotation sample designs is that the variation of the crop acreage of a particular sample unit from year to year is usually less than the variation of crop acreage between units within a particular year. The estimation theory is based on an additive mixed analysis of variance model with years as fixed effects, (a sub t), and sample units as a variable factor. The rotation patterns are decided upon according to: (1) the number of sample units in the design each year; (2) the number of units retained in the following years; and (3) the number of years to complete the rotation pattern. Different analytic formulae for the variance of (a sub t) and the variance comparisons in using a complete survey of the rotation patterns.

Lycthuan-Lee, T. G.↗

Missing observations in multiyear rotation sampling designs

Because Multiyear estimation of at-harvest stratum crop proportions is more efficient than single year estimation, the behavior of multiyear estimators in the presence of missing acquisitions was studied. Only the (worst) case when a segment proportion cannot be estimated for the entire year is considered. The effect of these missing segments on the variance of the at-harvest stratum crop proportion estimator is considered when missing segments are not replaced, and when missing segments are replaced by segments not sampled in previous years. The principle recommendations are to replace missing segments according to some specified strategy, and to use a sequential procedure for selecting a sampling design; i.e., choose an optimal two year design and then, based on the observed two year design after segment losses have been taken into account, choose the best possible three year design having the observed two year parent design.

Gbur, E. E.↗

Plutonium Age Dating Interlaboratory Comparison Overview - Project Design, Sample Preparation, and Results [Slides]

Project Design – How do you validate measured Pu model age? There are no certified reference materials (CRMs) that are certified for Pu model age or purification dates. There are no Am isotopic CRMs - IRMM 0243 243 Am spike has 241 Am impurity that can be used; Community working toward "consensus ages." This project executed and evaluated results from a Pu age dating interlaboratory comparison with six IAEA NWAL participant laboratories. It also ran the first quality control evaluation of single-picogram to sub-picogram scale interlaboratory 241 Am assay measurements from cotton swipe matrices. Results are promising, with a majority of 241 Am/ 241 Pu model age results agree to within 1 to 4 years. The calculated 241 Am assay results show interlaboratory variability, expanded percent uncertainties on calculated consensus 241 Am concentrations were: PuAge-S1 = 3.1 %, PuAge-S2 = 23 %, and PuAge-S3 = 26 %. Data can be used to investigate laboratory methods and improve precision and accuracy of 241 Pu and 241 Am assay for future campaigns.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Magnetic Shield Design Modeling and Validation on SWOT Spacecraft Applied to Mars Flux Pinning Orbiting Sample Design

A modeling methodology was developed for use on the Surface Water and Ocean Topography (SWOT) mission for the computational modeling and design of a magnetic shield for a 63 A-sq m source. Shield options were modeled and tested across various design parameters and validated with measurement. Measurement results fell within 10% of simulation in most cases of concern with sources of error well understood. These methods results informed a subsequent modeling activity for a future Mars Sample Return (MSR) mission concept with stringent magnetic cleanliness requirements to retain geologic integrity of the samples. One option for capturing the sample from orbit requires rare earth magnets in close proximity to the Martian samples. Magnetic modeling with a finite-element method solver estimated the magnetic environment and established the need for shielding. Further modeling then determined the shielding necessary to meet magnetic requirements, followed by the design of a mass-optimized solution.

Gonzales, Edward↗

Adaptation of G-TAG Software for Validating Touch-and-Go Comet Surface Sampling Design Methodology

The G-TAG software tool was developed under the R&TD on Integrated Autonomous Guidance, Navigation, and Control for Comet Sample Return, and represents a novel, multi-body dynamics simulation software tool for studying TAG sampling. The G-TAG multi-body simulation tool provides a simulation environment in which a Touch-and-Go (TAG) sampling event can be extensively tested. TAG sampling requires the spacecraft to descend to the surface, contact the surface with a sampling collection device, and then to ascend to a safe altitude. The TAG event lasts only a few seconds but is mission-critical with potentially high risk. Consequently, there is a need for the TAG event to be well characterized and studied by simulation and analysis in order for the proposal teams to converge on a reliable spacecraft design. This adaptation of the G-TAG tool was developed to support the Comet Odyssey proposal effort, and is specifically focused to address comet sample return missions. In this application, the spacecraft descends to and samples from the surface of a comet. Performance of the spacecraft during TAG is assessed based on survivability and sample collection performance. For the adaptation of the G-TAG simulation tool to comet scenarios, models are developed that accurately describe the properties of the spacecraft, approach trajectories, and descent velocities, as well as the models of the external forces and torques acting on the spacecraft. The adapted models of the spacecraft, descent profiles, and external sampling forces/torques were more sophisticated and customized for comets than those available in the basic G-TAG simulation tool. Scenarios implemented include the study of variations in requirements, spacecraft design (size, locations, etc. of the spacecraft components), and the environment (surface properties, slope, disturbances, etc.). The simulations, along with their visual representations using G-View, contributed to the Comet Odyssey New Frontiers proposal effort by indicating problems and/or benefits of different approaches and designs.

Mandic, Milan↗

Spatial structure, sampling design and scale in remotely-sensed imagery of a California savanna woodland

This article describes research related to sampling techniques for establishing linear relations between land surface parameters and remotely-sensed data. Predictive relations are estimated between percentage tree cover in a savanna environment and a normalized difference vegetation index (NDVI) derived from the Thematic Mapper sensor. Spatial autocorrelation in original measurements and regression residuals is examined using semi-variogram analysis at several spatial resolutions. Sampling schemes are then tested to examine the effects of autocorrelation on predictive linear models in cases of small sample sizes. Regression models between image and ground data are affected by the spatial resolution of analysis. Reducing the influence of spatial autocorrelation by enforcing minimum distances between samples may also improve empirical models which relate ground parameters to satellite data.

Mcgwire, K.↗

The Dual-Rasp Sampling System Design with Closed Pneumatic Sample Transfer

The novel Dual-Rasp sampling system has been developed for landed missions to low gravity planetary bodies and is particularly well suited for the unique environment of Saturn’s moon Enceladus. The Dual-Rasp sampling system has two counter-rotating rasp cutters that remove material from the surface and direct it into a guide. The cuttings follow the guide into a sample collection cup. When the sampling collection completes, the tool reconfigures by rotating the guide to create a closed circuit for pneumatic sample transfer from the collection cup to science instruments on the lander. A valve opens a gas tank and the gas flows from that tank into the sample collection cup and down rigid tubing to the science instruments chamber on the lander. A two degree of freedom arm with base actuators is used to deploy the sampler and control its sampling location.

Heness, Andrew B.↗

Preliminary EDS Liquid Sample Adapter Design Assurance Testing

A new liquid sample adapter design for the Explosive Destruction Systems has been developed. The design features a semi-transparent fluoropolymer tube coupled to the vessel high pressure sample valve with a closing quick connect fitting. The sample tubes are the pressure-limiting component. The tubes were hydrostatically tested to establish failure characteristics and pressure limits at ambient and operational temperatures. A group of tubes from two manufacturing lots were tested to determine the consistency of the commercial part. An upper pressure limit was determined for typical operations.

42 ENGINEERING↗

Design of Sample Holder for Plutonium Coupon Studies

In order to gain better understanding of the plutonium (Pu) corrosion behaviors and reaction kinetics, it is imperative that coupon experiments must be performed on well-defined surfaces. The reactions at the samples’ surfaces have to be properly monitored in terms of reactive gaseous pressures and temperatures. The pressure can be measured by using a pressure gauge, the temperature can be detected with calibrated thermal couples and/or pyrometric camera. These devices do not interfere with the chemistry of the surface reaction. However, to obtain information from the surface reaction, the aggressively machined edge and the back side of the Pu coupons need to be shielded from the applied gases. The coupons are typically made to 5/8 inch in diameter and 0.065 inch in thickness. To this end, a sample holder was designed which can seal the machined edge and the back side of coupons from the exposed gases, thus allowing proper surface reaction. The holder design was fabricated and had been tested with several coupon samples. We have achieved perfect sealing of the machined edge and the back side of the coupons, even when the coupons’ thicknesses are vastly different than the nominal thickness for which the sample holders were fabricated for. This write-up is to document the design of the holder and provide a description of the procedures to properly put the components together.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Accounting for Training Data Error in Machine Learning Applied to Earth Observations

Remote sensing, or Earth Observation (EO), is increasingly used to understand Earth system dynamics and create continuous and categorical maps of biophysical properties and land cover, especially based on recent advances in machine learning (ML). ML models typically require large, spatially explicit training datasets to make accurate predictions. Training data (TD) are typically generated by digitizing polygons on high spatial-resolution imagery, by collecting in situ data, or by using pre-existing datasets. TD are often assumed to accurately represent the truth, but in practice almost always have error, stemming from (1) sample design, and (2) sample collection errors. The latter is particularly relevant for image-interpreted TD, an increasingly commonly used method due to its practicality and the increasing training sample size requirements of modern ML algorithms. TD errors can cause substantial errors in the maps created using ML algorithms, which may impact map use and interpretation. Despite these potential errors and their real-world consequences for map-based decisions, TD error is often not accounted for or reported in EO research. Here we review the current practices for collecting and handling TD. We identify the sources of TD error, and illustrate their impacts using several case studies representing different EO applications (infrastructure mapping, global surface flux estimates, and agricultural monitoring), and provide guidelines for minimizing and accounting for TD errors. To harmonize terminology, we distinguish TD from three other classes of data that should be used to create and assess ML models: training reference data, used to assess the quality of TD during data generation; validation data, used to iteratively improve models; and map reference data, used only for final accuracy assessment. We focus primarily on TD, but our advice is generally applicable to all four classes, and we ground our review in established best practices for map accuracy assessment literature. EO researchers should start by determining the tolerable levels of map error and appropriate error metrics. Next, TD error should be minimized during sample design by choosing a representative spatio-temporal collection strategy, by using spatially and temporally relevant imagery and ancillary data sources during TD creation, and by selecting a set of legend definitions supported by the data. Furthermore, TD error can be minimized during the collection of individual samples by using consensus-based collection strategies, by directly comparing interpreted training observations against expert-generated training reference data to derive TD error metrics, and by providing image interpreters with thorough application-specific training. We strongly advise that TD error is incorporated in model outputs, either directly in bias and variance estimates or, at a minimum, by documenting the sources and implications of error. TD should be fully documented and made available via an open TD repository, allowing others to replicate and assess its use. To guide researchers in this process, we propose three tiers of TD error accounting standards. Finally, we advise researchers to clearly communicate the magnitude and impacts of TD error on map outputs, with specific consideration given to the likely map audience.

58 GEOSCIENCES↗

The effect of prefilter design on sample rate selection in digital flight control systems

The effect of prefilters on sample rate selection is examined and design procedures are determined for obtaining the best combination of prefilter breakpoint and sample rate. The employed approach involves a quantitative comparison of the output noise response of systems originating from the same basic plant and designed over a wide range of prefilters and sample rates. Each system design was carefully tailored so that it exhibited approximately identical responses to commands. The results presented augment the criteria for sample rate selection which have been discussed by Powell and Katz (1975). Attention is given to system characteristics, an integrator as a plant, and the short period motion of the F-8 aircraft.

Peled, U.↗

Design procedures for fiber composite structural components: Panels subjected to combined in-plane loads

Step by step procedures are described which can be used to design panels made from fiber composite angleplied laminates and subjected to combined in plane loads. The procedures are set up as a multistep sample design. Steps in the sample design procedure range from selection of the laminate configuration to the subsequent analyses required to check design requirements for: (1) displacement, (2) ply stresses, and (3) buckling. The sample design steps are supplemented with appropriate tabular and graphical data which can be used to expedite the design process.

Chamis, C. C.↗

Improved quantitation of SIMS depth profile measurements of niobium via sample holder design improvements and characterization of grain orientation effects

The importance of SIMS analyses for “N-doped” impurity alloyed niobium and other surface-alloyed materials continues to increase. A major hurdle is the uncertainty of instrument calibration due to changes in sample height either from sample surface topography or from the sample holder itself. The CAMECA sample holder design allows for many types of samples to be analyzed. However, a drawback is that the holder faceplate can bend, contributing an uncertainty in the relative sensitivity factor (RSF) used to quantify the SIMS results. Here, we describe an improved sample holder having a reinforced faceplate, which prevents deflection and reduces uncertainty. Simulations show that the new design significantly reduces deflection from 10 μm to 5 nm. Sample measurements show a reduction of RSF uncertainty from this source from 4.1% to 0.95%. Grain orientation has long been suspected to affect RSF measurement as well. A bicrystal implant standard, consisting of randomly oriented and [001] grains, was successively rotated 15° between analyses. It was observed that 20% of the analyses performed on the randomly oriented grain exhibited anomalously high RSF values as well as slow sputter rates. These features were associated with the changing grain normal orientation with respect to the primary Cs + beam. The grain orientation associated with the rise in RSF was simulated and determined to be the [101] crystallographic plane, thus indicating that ion channeling was responsible for the significantly increased RSF. Focused ion beam analysis confirmed slower sputter rates for the cardinal crystallographic orientations, indicating that ion channeling occurred for each.

43 PARTICLE ACCELERATORS↗

Estimating regression coefficients from clustered samples: Sampling errors and optimum sample allocation

A number of surveys were conducted to study the relationship between the level of aircraft or traffic noise exposure experienced by people living in a particular area and their annoyance with it. These surveys generally employ a clustered sample design which affects the precision of the survey estimates. Regression analysis of annoyance on noise measures and other variables is often an important component of the survey analysis. Formulae are presented for estimating the standard errors of regression coefficients and ratio of regression coefficients that are applicable with a two- or three-stage clustered sample design. Using a simple cost function, they also determine the optimum allocation of the sample across the stages of the sample design for the estimation of a regression coefficient.

Kalton, G.↗