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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records

Utah FORGE: Direct Shear Test Data for Investigating Seismic Precursors to Shear Failure of Fractures

This dataset includes results of direct shear tests to investigate the mechanical and geophysical response of dry and saturated fractures in Indiana limestone and Sierra White granite. Direct shear tests were performed on tensile-induced fractures in Indiana limestone and Sierra White granite in a custom water-pressurized chamber. The provided Excel files include the representative seismic wave signals and the normalized wave amplitudes of ultrasonic wave transducers. A link to the published journal article presenting the data and describing the experiment in detail is provided as well.

15 GEOTHERMAL ENERGY↗

Utah FORGE: Results of Direct Shear Tests on Saturated Joints in Sierra White Granite

This dataset includes an Excel file with the results of direct shear tests to investigate the mechanical and geophysical response of saturated joints. Tests were conducted on induced tension-fractured Sierra White granite joints in a custom water pressurized chamber. The preparation of granite joints is summarized in the PDF file. The PDF file also includes a description of the direct shear tests, experimental procedure, and results.

15 GEOTHERMAL ENERGY↗

Triaxial Shear Tests on Simulated Sierra White Fault Gouge & Borehole Simulation in Sierra White Gouge

Laboratory shear tests were conducted on pulverized Sierra White granite (SWG) to investigate slip mechanisms in naturally occurring faults. Synthetic fault geometries were constructed by sandwiching fine grained SWG powder in between steel forcing blocks. For dry experiments, ~3.5 g of SWG powder was poured onto the face of the lower steel forcing block and leveled. For saturated experiments, enough fluid was added to the ~3.5 g of Sierra White granite powder to form a slurry. This slurry was applied to the lower forcing block and leveled. Inclined forcing blocks with 25.4 mm diameter and 35° faces, which were machined from ground steel rods with fine teeth on the faces, help to hold the gouge in place and prevent delamination at the interface. The top forcing block had a 2.03 mm centered hole to allow pore fluid access to the gouge. A fine steel mesh prevented back flow of the gouge into pore fluid lines. Samples were isolated from the confining medium using three layers of heat shrink polyolefin, as shown in Figure 1. The outer layer was shrunk over the o-rings on the end caps to form an impermeable seal, which was reinforced with steel tie wires on both sides of the o-rings. Hardened steel spacers and copper shim stock was placed between the steel forcing blocks and the end caps to preserve the parallelism of the Hastelloy wetted parts. For dry samples, the end caps were plugged, while the end caps for the saturated samples were connected to pore lines.

58 GEOSCIENCES↗

Permeability and Direct Shear Test Determinations of Barnwell Core in Support of UNESE

A critical component of the Underground Nuclear Explosion Signatures Experiment (UNESE) program is a realistic understanding of the post-detonation processes and changes in the environment that produce observable physical and radio-chemical signatures. Rock and fracture properties are essential parameters for any UNESE test bed. In response to the need for accurate modeling scenarios of these observations, an experimental program to determine the permeability and direct shear fracture properties of Barnwell core was developed. Room temperature gas permeability measurements of Barnwell core dried at 50degC yield permeability ranging from 6.24E-02 Darcys to 6.98E-08 Darcys. Friction angles from the direct shear tests vary from 28.1deg to 44.4deg for residual shear strength and average 47.9deg for peak shear strength. Cohesion averaged 3.2 psi and 13.3 psi for residual and peak shear strength values respectively. The work presented herein is the initial determination of an ongoing broader material characterization effort.

45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEF↗

Direct Shear and Triaxial Shear test Results on Core from Borehole U-15n and U-15n#10, NNSS in support of SPE

Direct Shear (DS) and Triaxial Shear (FCT) tests from Core holes U-15n and U-15n#10 are part of a larger material characterization effort for the Source Physics Experiment (SPE) project. This larger effort encompasses characterizing a granite body from Nevada both before and after each SPE shot. Core hole U-15n is the vertically oriented source hole for all SPE shots; pre shot core was taken from this hole for DS and FCT testing. After two SPE shots were executed, an inclined core hole (U-15n#10) was drilled; both DS and FCT tests were conducted from this core hole. The first shot (SPE-1) conducted on May 3, 2011 was a calibration shot. SPE-1 was an order of magnitude smaller than the second shot (SPE-2). After SPE-2 was conducted on October 25, 2011 the aforementioned inclined core hole (U-15n#10) was drilled. At its bottom, the inclined core hole intersects the source hole. The third shot (SPE-3) occurred on July 24, 2012. Vertical and inclined core holes were drilled post SPE-3 and specimens will soon be selected for geomechanical characterization. At the time of this writing, work is ongoing at Nevada in preparation for the fourth SPE shot (SPE-4).

36 MATERIALS SCIENCE↗

Additively Manufactured Carbon Fiber and Fused Deposition Modeling PLA Interlaminar Shear Testing Report

This test report summarizes the torsional test setup, procedure, and results for interlaminar shear (ILS) failure of additively manufactured carbon fiber (CFAM) material developed at LLNL. In addition, the report also includes testing of fused deposition modeled (FDM) polylactic acid (PLA), including ILS test standard D7078 and the same torsional test mentioned above. The test hopes to characterize ILS properties of CFAM, however substantial further testing and improvements still need to be done to induce a proper failure mode. This testing was performed by Sundi Win as part of her summer internship project in Kinetic Technologies.

36 MATERIALS SCIENCE↗

Fabrication and Mechanical Testing of Block Shear Joints to Measure Ultimate Shear Strength in Adhesive-Bonded High Explosive (HE) Joints (Progress Summary)

Small-scale adhesive-bonded HE joints were designed, using roughly 4% of the HE mass required by fixtures described in the ASTM D905 standard. Custom 3D-printed bonding fixtures were designed, fabricated, and used to generate reproducible joints with programmable bondline thickness. A custom 3D-printed block shear testing fixture was designed, fabricated, and employed to measure the shear strength of test joints.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Discrete and Continuum Plane-Hopper Flow Simulations with Experimental Validation Using X-Ray Imaging, Arch Profilometry and Wall Pressure Measurements

The flow of spherical glass beads, approximately cubic wood crumbles®, and wood microchips are investigated using a combination of discrete element modeling (DEM), finite element analysis (FEA), and physical experiments using a custom plane-flow hopper in which the flow is characterized using x-ray imaging, profilometry to measure arching geometry and pressure measurements at the wall. The purpose of this study is to investigate fundamental flow behavior, and for this purpose the simulations and physical tests are specially designed. During the physical tests and simulations, the hopper geometry begins as a V shape with the two opposing side walls touching at the bottom of the V. Basic tests are performed by first filling the hopper with material, and then rotating the opposing side walls inward about their common intersection axis to cause an approximately uniform stress condition throughout most of the hopper. The side walls then slide upward to effectively increase the size of the opening at the bottom of the hopper until the arch of material in the hopper breaks, and all of the material falls out of the hopper. More advanced tests are also performed in which the initial rotation of the walls is slightly reversed to decrease the pressure in the hopper, corresponding to “preshear” and “shear” conditions in standard shear tests. Shear tests of the materials are also performed using a Schulze automated ring shear tester with a standard size M shear cell, and the shear tests of the glass beads and wood crumbles® are also simulated using DEM to calibrate the DEM with the FEA. Reasonable agreement between predicted and measured flow behavior is obtained indicating that this type of physical tests and modeling shows promise for characterizing and predicting the flow behavior of compressible and anisotropic materials.

09 BIOMASS FUELS↗

Rheological behavior of neat and carbon fiber-reinforced poly(ether ketone ketone) for extrusion deposition additive manufacturing

To develop new materials for extrusion additive manufacturing (AM) systems, a fundamental understanding of rheological properties is essential to correlate the effect of processing on material structure and its properties. In this work, the rheological properties of five different grades of neat and carbon fiber (CF)-reinforced poly(ether ketone ketone) are reported. Rheological properties are essential to understand the effect of reinforcing fibers and AM process parameters such as time, temperature, environment, and shear rate on flow behavior during processing. Small-amplitude oscillatory shear tests and steady shear tests indicated neat grades to exhibit less increase in viscosity over time when processed in air than the CF-filled grades. The filled grades showed greater shear thinning and lower sensitivity to temperature. Altogether, this rheological analysis provides a broad framework for determining appropriate processing conditions for extrusion deposition AM of such high-temperature polymer systems.

36 MATERIALS SCIENCE↗

Shear Punch Testing on ATR Irradiated MA956 FeCrAl Alloy

The shear punch testing of irradiated and control MA956 (FeCrAl) Alloy from the NSUF-ATR-UCSB irradiation is presented. This is the first data taken on a new shear punch fixture design to test three 1.5mm punches from each 8mm x 0.5mm Disc Multipurpose Coupon (DMC). Samples were irradiated to 6.1dpa at a temperature of 315°C and 6.2 dpa at 400°C.

36 MATERIALS SCIENCE↗

Shear Behavior of Artificial Clay Seams within Bedded Salt Structures

Bedded salt contains thin layers of clay, also known as clay seams, in-between far thicker layers of salt. These inhomogeneities are thought to have first-order effects on the closure of nearby drifts and potential roof collapses. Despite their importance, characterizations of the peak shear strength and residual shear strength of clay seams in salt are extremely rare in the published literature. A previous paper reported results from laboratory direct shear experiments on clay seam samples from the Permian Basin in New Mexico. These clay seams behaved similar to intact salt, which was attributed to the abundance of salt crystals intersecting the clay seams. None of those specimens contained a distinct ¼" - ½" (6 -12 mm) thick clay seam, as has been observed in drifts at the Waste Isolation Pilot Plant (WIPP). Due to the difficulty in obtaining WIPP samples with these types of clay seams, artificial seams of bentonite and brine sandwiched between sections of salt were created and shear tested. Eight 4" diameter samples were created with either a ¼" or ½" a thick seam and then consolidated at 3000 psi prior to shear testing. The direct shear tests on these samples were performed at nominal normal stresses representative of expected WIPP in-situ conditions (500 to 1500 psi). The resulting shear stress vs. shear displacement curves exhibited a peak followed by a gradual decay of shear strength. The shear stress never transitioned to a true residual shear stress plateau, so the final shear strength at the end of each test (0.75" of shear displacement) was analyzed instead. Both the peak shear strength and the final shear strength conformed to Mohr- Coulomb behavior with friction angles and cohesion strengths consistent with a saturated, highly consolidated, clay. These new artificial clay seam results and the previous clay-interspersed-with-salt results likely bound the expected shear behavior of WIPP clay seams.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Microstructural evolution in shear-punch tests: A comparative study of pure Cu and Cu-Cr alloy

Understanding the mechanisms behind microstructural evolution during shear deformation has been a long-standing area of interest. However, establishing a connection between microstructure, mechanical properties, and extent of shear deformation is challenging and requires refined experimental approaches. Shear-punch testing (SPT) provides a controlled method to introduce shear into small volumes of material that later can be subjected to detailed microstructural characterization. In this study, we utilize an SPT device to induce shear deformation to pure copper and a binary copper-chromium alloy. Electron backscatter diffraction and transmission electron microscopy were used to study the mechanisms of plastic deformation after SPT. Our results indicate that shear deformation of pure Cu produces a dense network of intercepting microshear bands upon sustained deformation. Twin boundaries undergo degradation into high angle grain boundaries due to simultaneous deviation from the axis-angle pair condition of 60° misorientation on [111] direction. The presence of 50% volume Cr particles in the soft Cu matrix fundamentally altered the shear deformation mechanism. Preferential deformation of the Cu matrix led to accelerated shear-induced formation of low and high angle grain boundaries, and subsequent grain refinement. Comparatively, no grain refinement occurred in pure Cu at a strain ~10 times larger (ϵ = 4.73) than that of the copper-chromium case (ϵ = 0.42). Overall, our study sheds light on the microstructural evolution during shear deformation and highlights the significant influence of particle reinforcements on the shear deformation mechanisms of metals.

36 MATERIALS SCIENCE↗

Material Testing of PH13-8MO H950 Steel for Xue-Wierzbicki Fracture Criterion Determination

Four tensile coupon designs of PH13-8Mo H950 steel were tested to failure using quasi-static rates to obtain data to calibrate the Xue-Wierzbicki failure model for ductile fracture. The tests recorded the force-displacement, location of the first crack, displacement to fracture, area reduction, and crack propagation path. The test method and coupon designs were adopted from Tomasz Wierzbicki’s “Calibration and evaluation of seven fracture models” report. The XueWierzbicki model predicts fracture based on accumulated equivalent plastic strain, stress triaxiality, and deviatoric state parameter. Calibrating the Xue-Wierzbicki failure model required testing four coupon designs to calculate the four free parameters in the model. The coupon designs tested a range of stress triaxialities with two axisymmetric tests, one shear test, and one plane stress test. The data obtained and presented in this report can be used to develop a Xue-Wierzbicki fracture model for PH13-8Mo H950 steel.

36 MATERIALS SCIENCE↗

Shear Punch Testing of Neutron-Irradiated HT-9 and 14YWT

Shear punch mechanical testing was performed on neutron-irradiated HT-9 and 14YWT alloys, comparing the traditional ferritic/martensitic steel with the advanced oxide dispersion strengthened nanostructured ferritic alloy. The samples were irradiated at various temperatures between 380°C and 520°C. In HT-9, on increasing the irradiation temperature, the 1% offset shear stress and maximum shear stress decreased. The advanced 14YWT alloy was less sensitive to irradiation temperature with respect to irradiation hardening. However, it still exhibited irradiation hardening at each temperature.

36 MATERIALS SCIENCE↗