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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Chemical-Induced Slippage in Bulk WSe 2

Layered transition metal dichalcogenides (TMDs) are the focus of intense research owing to their semiconducting properties and applications in many fields of research. In addition to intercalation and exfoliation, physical strain modulation has been reported as a way to mechanically-induce the slippage of layers and influence the properties of TMDs. Here, we report the chemically-induced slippage of layers in bulk tungsten diselenide (WSe 2 ). Powder X-ray diffraction, Raman spectroscopy, electron microscopy, and thermal analysis suggest that slippage is easily achieved by grinding in the presence of common solvents. Chemically-induced slippage of TMDs may represent an intermediate step leading to the exfoliation of these materials. We anticipate that chemical slippage will widen the synthetic utility and advance our understanding of the mechanical and optoelectronic properties of layered materials.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2026

Endpoint Slippage Analysis in the Presence of Impedance Rise and Loss of Active Material

Endpoint slippage analysis can be used to quantify the reduction and oxidation side-reactions occurring in rechargeable batteries. Application of this technique often disregards the interference of additional aging modes, such as impedance rise and loss of active material (LAM). Here, we show that these modes can themselves induce slippage of endpoints, making the direct determination of parasitic reactions more difficult. We provide equations that describe the slippages caused by LAM and impedance rise. We show that these equations can, in principle, account for the contribution of these additional modes to endpoint slippage, enabling “correction” of testing data to quantify the side-reactions of interest. However, the challenge with this approach is that it requires information about the average Li+ content of disconnected active material domains, which is, in many cases, unknowable. The present work explores mathematical connections between measurable quantities (such as capacity fade and endpoint slippages) and the extent of LAM or impedance rise endured by the cell, and discuss how the tracking of endpoints can better serve battery diagnostics.

Rodrigues, Marco-Tulio F. [Argonne National Labora↗
NASA NTRS2021

Magnetic Reconnection in a Sheared Magnetic Flux Tube: Slippage Versus Tearing

The process of magnetic reconnection in a flux tube can occur in a time-stationary fashion as slippage reconnection or in a time-dependent manner based on, for example, the tearing instability. However, it is not well known under which conditions a system can sustain slippage reconnection. Likewise, it is unclear whether systems can exhibit slippage reconnection and time-dependent reconnection simultaneously. In order to investigate these questions, we employ a set of 3D magnetohydrodynamic simulation. Using these simulations, we model a twisted flux tube with a spatially localized resistive region in the center of the simulation box, and an applied driver on one end plane of the simulation box. As a result, the Poynting flux injected at the boundary propagates to the resistive region and dissipates there. If the driver is nearly circular, we find a predominance of slippage reconnection, which decouples the applied driver entirely from one half of the flux tube. Second, a tearing-like instability occurs with slippage reconnection in the resistive region when the resistivity is strong enough and the cross section of the flux tube, as defined by the shape of the applied velocity perturbation, is elliptical enough. In this case we find the surprising feature that magnetic field perturbation generated by the tearing-like instability radiates away from the resistive region to influence the entire flux tube shape.

Hidetaka Kuniyoshi↗
DOE OSTI2024

Addressing Limitations of the Endpoint Slippage Analysis

Some rate of oxidation and reduction side-reactions will inevitably coexist in most rechargeable batteries. While parasitic reduction traps electrons, parasitic oxidation donates electrons to the cell’s inventory and may cause temporary capacity gain. Consequently, capacity measurements can provide unreliable information about the total extent of side-reactions occurring in the cell. The most widely used method to determine the rate of both these parasitic processes involves analyzing the slippage of endpoints, which consists in tracking the termination of cell charge and discharge when data is represented along a cumulative capacity axis. Here, we argue that this approach could lead to inaccuracies when applied to certain systems, which includes Si electrodes in Li-ion batteries and hard carbon in Na-ion batteries. This inaccuracy originates from the smooth nature of the voltage profiles of these materials at low and high alkali-ion content, causing the termination of charge and discharge to be dictated by voltage changes at both the positive and negative electrodes. We analyze this issue in quantitative terms and propose equations that can provide true rates of parasitic processes from experimental endpoint slippage data. This work shows that, in battery science, well-established analytical approaches may not be directly transferrable to new electrode systems.

25 ENERGY STORAGE↗
DOE OSTI2021

Modulation-slippage trade-off in resonant four-wave upconversion

Following up on a proposal to use four-wave mixing in an underdense plasma at mildly relativistic laser intensities to produce vastly more energetic x-ray pulses [V. M. Malkin and N. J. Fisch, Phys. Rev. E, 101, 023211 (2020)], we perform the first numerical simulations in one dimension to illustrate amplification of a short high frequency seed through four-wave mixing. Here, we illustrate how parasitic processes including phase modulation and spatial pulse slippage limit the amplification efficiency. Although the regimes studied were not where the optimal efficiencies were expected, these regimes do expose the basic physical processes at play, while still yielding not insignificant spectral power upshift.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
NASA NTRS1975

Correction of burst errors containing bit slippages for cyclic block codes

A technique is presented for correction of an (n,k) cyclic block code subjected to a noise disturbance consisting of an arbitrary number of both bit deletions and bit inversions contained within a single error burst. Following the procedure described by Meggitt (1961), the correction of a b-bit burst is attempted by first loading the initial error syndrome into an (n-k) order feedback shift register with taps selected for the code's generating polynomial; the register is then successively shifted one bit position in the direction of lower order. The discussion covers burst correction with m-bit deletion, burst/deletion decoder implementation, false correction probability, and bit slippage involving bit insertions. The principal elements of the burst/deletion correction decoder are presented in schematic form.

Green, E. P.↗
NASA NTRS2018

Restore-L Satellite Servicing Internship Final Report

An experiment was conducted to determine whether a sample of shorter flexible metal hoses could sustain tensile loads of up to 200 lbf and continue to meet the minimum mission requirements. The purpose of this experiment was to determine if tension loads during the processing of the hoses compromise performance. With this information, it will be decided whether the flight flex-hose manufacturer should proceed with the testing of the full-scale flex-hoses. To reduce the time and funding required for this test, a test fixture was designed and assembled in the Engineering Development & Operations (EDO) test facility. In this test fixture, two Engineering Development Unit (EDU) flex-hoses were loaded with free floating weights up to 350 lbf. A load of 200 lbf equates to the maximum expected loading with a margin of safety, thus all data recorded after 200 lbf was purely for reference. Measurements were taken using a tape measure and a custom datum measurement system to record the loaded and unloaded length of each flex-hose at various loads. Any permanent stretching beyond a 1/8th of an inch was indicative of inelastic yielding. The loading of each flex-hose was done with an initial weight 80 lbf and was increased to 100 lbf. Additional loading up to 350 lbf was done by 50 lbf increments thereafter. During the performance of the test, slippage occurred in the mounting of the flex-hoses in the test fixture. The first slippage occurred during the testing of the first flex-hose due to the collar of the flex-hose slipping within the collet of the top Kellem. As a result, the first flex-hose test was terminated early to modify the fixture. Due to the flex-hose not inelastically yielding, the test was repeated on the first flex hose. This test resulted in another instance of slippage in the upper collar of the Kellem due to tape interfering with the securing of a collet around the collar of the flex-hose. The test was then continued with one more slippage of the flex-hose within the collet of the bottom Kellem. Preventive measures were taken for future slippage, and the second hose remained secure during testing.Once the tests were concluded, the elongation of each hose was analyzed for inelastic yielding. Both flex-hoses stretched a measurable and repeatable amount under loading, however, this stretching was recovered once each hose was unloaded. As a result, both EDU flex-hoses did not experience any inelastic yielding during the tension testing. Once received, one additional flex-hose will be tested for yielding, but at the time of this paper, the recommendation is to proceed with testing of the full-scale flex-hoses at the flex-hose manufacturer.

Dziekan, Joseph↗
NASA NTRS2005

Path Following with Slip Compensation for a Mars Rover

A software system for autonomous operation of a Mars rover is composed of several key algorithms that enable the rover to accurately follow a designated path, compensate for slippage of its wheels on terrain, and reach intended goals. The techniques implemented by the algorithms are visual odometry, full vehicle kinematics, a Kalman filter, and path following with slip compensation. The visual-odometry algorithm tracks distinctive scene features in stereo imagery to estimate rover motion between successively acquired stereo image pairs, by use of a maximum-likelihood motion-estimation algorithm. The full-vehicle kinematics algorithm estimates motion, with a no-slip assumption, from measured wheel rates, steering angles, and angles of rockers and bogies in the rover suspension system. The Kalman filter merges data from an inertial measurement unit (IMU) and the visual-odometry algorithm. The merged estimate is then compared to the kinematic estimate to determine whether and how much slippage has occurred. The kinematic estimate is used to complement the Kalman-filter estimate if no statistically significant slippage has occurred. If slippage has occurred, then a slip vector is calculated by subtracting the current Kalman filter estimate from the kinematic estimate. This slip vector is then used, in conjunction with the inverse kinematics, to determine the wheel velocities and steering angles needed to compensate for slip and follow the desired path.

Helmick, Daniel↗
NASA NTRS2013

Characterizing Wheel-Soil Interaction Loads Using Meshfree Finite Element Methods: A Sensitivity Analysis for Design Trade Studies

A wheel experiencing sinkage and slippage events poses a high risk to planetary rover missions as evidenced by the mobility challenges endured by the Mars Exploration Rover (MER) project. Current wheel design practice utilizes loads derived from a series of events in the life cycle of the rover which do not include (1) failure metrics related to wheel sinkage and slippage and (2) performance trade-offs based on grouser placement/orientation. Wheel designs are rigorously tested experimentally through a variety of drive scenarios and simulated soil environments; however, a robust simulation capability is still in development due to myriad of complex interaction phenomena that contribute to wheel sinkage and slippage conditions such as soil composition, large deformation soil behavior, wheel geometry, nonlinear contact forces, terrain irregularity, etc. For the purposes of modeling wheel sinkage and slippage at an engineering scale, meshfree nite element approaches enable simulations that capture su cient detail of wheel-soil interaction while remaining computationally feasible. This study implements the JPL wheel-soil benchmark problem in the commercial code environment utilizing the large deformation modeling capability of Smooth Particle Hydrodynamics (SPH) meshfree methods. The nominal, benchmark wheel-soil interaction model that produces numerically stable and physically realistic results is presented and simulations are shown for both wheel traverse and wheel sinkage cases. A sensitivity analysis developing the capability and framework for future ight applications is conducted to illustrate the importance of perturbations to critical material properties and parameters. Implementation of the proposed soil-wheel interaction simulation capability and associated sensitivity framework has the potential to reduce experimentation cost and improve the early stage wheel design proce

terramechanics↗
NASA NTRS1989

Corotation lag of the Jovian atmosphere, ionosphere, and magnetosphere

The Jovian ionosphere-magnetosphere coupling model of Hill (1979) was modified to include the rotational slippage of the neutral atmosphere at ionospheric heights, relative to a frame of reference corotating rigidly with Jupiter. Equations were derived for the altitude distributions of ionospheric neutral and ion velocities, and a generalized expression was obtained for the corotation lag of the magnetosphere. The results of calculations provide independent support for the expectation that vertical mixing in Jupiter's atmosphere is much more vigorous at high latitudes than near the equator. They also indicate that the observed corotation lag in the magnetosphere and the Io torus is largely attributable to the slippage of the neutral atmosphere itself, rather than to the slippage of ionospheric ions relative to ionospheric neutrons, as previously suggested.

Huang, T. S.↗
NASA NTRS2012

Determining Wheel-Soil Interaction Loads Using a Meshfree Finite Element Approach Assisting Future Missions with Rover Wheel Design

A wheel experiencing sinkage and slippage events poses a high risk to rover missions as evidenced by recent mobility challenges on the Mars Exploration Rover (MER) project. Because several factors contribute to wheel sinkage and slippage conditions such as soil composition, large deformation soil behavior, wheel geometry, nonlinear contact forces, terrain irregularity, etc., there are significant benefits to modeling these events to a sufficient degree of complexity. For the purposes of modeling wheel sinkage and slippage at an engineering scale, meshfree finite element approaches enable simulations that capture sufficient detail of wheel-soil interaction while remaining computationally feasible. This study demonstrates some of the large deformation modeling capability of meshfree methods and the realistic solutions obtained by accounting for the soil material properties. A benchmark wheel-soil interaction problem is developed and analyzed using a specific class of meshfree methods called Reproducing Kernel Particle Method (RKPM). The benchmark problem is also analyzed using a commercially available finite element approach with Lagrangian meshing for comparison. RKPM results are comparable to classical pressure-sinkage terramechanics relationships proposed by Bekker-Wong. Pending experimental calibration by future work, the meshfree modeling technique will be a viable simulation tool for trade studies assisting rover wheel design.

Contreras, Michael T.↗
DOE OSTI2025

Life Cycle Greenhouse Gas Emissions of Biogas Upgrading for Fuel Production

Waste-to-Renewable Natural Gas (RNG) offers a promising solution to alleviating waste management challenges by converting waste into renewable fuels. Here, this process can significantly reduce greenhouse gas (GHG) emissions, as demonstrated through a comprehensive life cycle analysis. Biogas upgrading is essential to enhance the methane concentration, though it could be energy-intensive and susceptible to methane slippage. Four commonly adopted biogas upgrading technologies, including pressure swing adsorption, membrane separation, chemical absorption, and water scrubbing, are considered. Our study evaluates the life cycle GHG emissions of RNG production from major sources of waste in the U.S. including wastewater sludge, food waste, landfill gas, dairy cow manure, and swine manure. Meta-analysis was conducted to assess methane slippage and energy consumption of biogas upgrading and associated GHG emissions, while accounting for potential avoided emissions from conventional waste management, which vary widely (ranging from −481.0 to 101.8 g CO 2 -eq/MJ). Under default upstream assumptions, representative carbon intensity of RNG varies from about −125 g of CO 2 -eq/MJ (dairy cow manure) to about 41 g of CO 2 -eq/MJ (wastewater sludge). We also explored RNG applications in producing hydrogen, ammonia, and compressed/liquefied forms. These findings highlight the potential of RNG and RNG-derived fuels to reduce GHG emissions and bolster the U.S. energy supply.

Biogas upgrades↗
DOE OSTI2022

Mitigation of rapid capacity decay in silicon-LiNi 0.6 Mn 0.2 Co 0.2 O 2 full batteries

Silicon (Si)-based materials have been considered as the most promising anode materials for high-energy-density lithium-ion batteries because of their higher storage capacity and similar operating voltage, as compared to the commercial graphite (Gr) anode. But the use of Si anodes including silicon-graphite (Si-Gr) blended anodes often leads to rapid capacity decay in Si-Gr/LiNixMnyCo z O 2 (x+y+z=1) full cells, which has been attributed to surface instability of the Si component. In addition to stabilizing the surface, this work investigates the potential of the Si-Gr blended anodes in a full-cell configuration and its impact on the capacity contribution from active components. Using dQ/dV plots of the full cells, a powerful but simple-to-implement differential potential approach is developed to decouple the capacity contribution and degradation from the graphite and silicon components. Data collected from three-electrode cells confirm the results from the differential potential approach, which suggests a voltage slippage to a higher voltage at the blended anode side. Additionally, the voltage slippage causes a reduced utilization of the Gr component and exacerbates side reactions between the Si-Gr anode and carbonate electrolytes. Furthermore, based on these failure mechanisms, we adopted a mitigation strategy to tune the open circuit voltage of the prelithiated anode while stabilizing the surface. As a result, the full cells with the modified Si-Gr anodes (mass loading, 2.5 mAh/cm 2 ) offer a highly reversible full-cell energy density of 390 Wh/kg (based on the mass of both anode and cathode materials in a full cell) with a cycling CE of 99.9% over 200 cycles.

25 ENERGY STORAGE↗
DOE OSTI2022

Super-resonant four-photon collinear laser frequency multiplication in plasma

Resonant four-photon scattering could nearly double frequencies of intense laser pulses in plasma. However, transverse slippage between pulses presents a technological challenge, while collinear four-photon scattering is forbidden for classical light dispersion in plasma. Nonlinear renormalization of intense laser pulses can enable collinear four-photon resonance. However, such a very intensity-sensitive resonance is difficult to maintain for evolving pulses. Remarkably, there is a lower-dimensionality submanifold of the resonant four-photon manifold where the evolving pulses stay in resonance. Furthermore this could enable an all-optical frequency doubling of mildly relativistic-intense laser pulses in collinear geometry, advantageously free of the transverse slippage challenges.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2025

Improving high temperature resilience of fiber sensor embedded smart components through laser shock peening

This study explores the use of laser shock peening (LSP) to enhance material properties and high-temperature performance of fiber-sensor-fused smart parts fabricated by additive manufacturing (AM) methods. Using embedded fiber sensors as distributed strain gauges, the study demonstrates that LSP can induce compressive strains of up to 130 µε on fiber embedded 1-mm below metal surfaces. The electron backscatter diffraction (EBSD) analysis shows that, with optimized LSP parameters, the metallic matrix undergoes substantial microstructural refinement, resulting in denser structures. Thermal cycling tests showed that the LSP process can increase fiber slippage temperatures by more than 50 °C. This work shows that the LSP process is an effective room-temperature process for enhancing both surface quality and increasing fiber slippage threshold under both thermal and mechanical stress.

Zhong, Shuda [University of Pittsburgh, PA (United↗
DOE OSTI2024

H2 Materials Compatibility of Low Cost, High Pressure, Polymer H2 Dispensing Hoses

NanoSonic was recently awarded a DOE Phase IIB SBIR program for the commercialization of an innovative metal-free polymer based H2 dispensing hose to make H2 an economically viable fuel alternative to gasoline. During the Phase I and Phase II base programs, NanoSonic's H2 hose demonstrated ultra-high hydrostatic burst strength values > 31,000 psi where failure occurred due to fitting slippage, rather than hose burst. Additionally, our hoses survived > 51,000 pressure impulse cycles at 12,000 psi over a thermal cycle of -40 °C to 85 °C. These hoses also failed due to fitting slippage. Thus, our Phase IIB program is centralized on the addition of a new fitting, polymer hose refinement, and validation of a complete hose and fitting system certified for use with H2. While NanoSonic has partnered with the National Renewable Energy Laboratory (NREL) to test our hose on their robotic H2 dispensing system, we are also seeking durability with the H2 environment at the molecular level. Here, NanoSonic proposes a CRADA with Pacific Northwest National Laboratory (PNNL), who has expertise in H2 polymer materials compatibility. Together, we will determine the lifetime of our H2 hose polymer and composite constituents via: 1) time-temperature superposition (TTS) studies via dynamic mechanical analysis (DMA) under H2, 2) friction and wear resistance under in situ H2 tribometry, and 3) multi-axis strain testing under cryogenic conditions. PNNL has the unique test equipment essential to gain this type of insight and lifetime prediction data. Importantly, the work conducted under the proposed CRADA will increase the safety and reliability of our H2 hoses while expanding the market for use of our low H2 permeation polymers and durable cryogenic composites to realize the H2@Scale objectives to reduce the cost of H2.

08 HYDROGEN↗