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At least 19 records

Machine learning for interpreting coherent X-ray speckle patterns

Speckle patterns produced by coherent X-ray have a close relationship with the internal structure of materials but quantitative inversion of the relationship to determine structure from speckle patterns is challenging. Here, in this work, we investigate the link between coherent X-ray speckle patterns and sample structures using a model 2D disk system and explore the ability of machine learning to learn aspects of the relationship. Specifically, we train a deep neural network to classify the coherent X-ray speckle patterns according to the disk number density in the corresponding structure. It is demonstrated that the classification system is accurate for both non-disperse and disperse size distributions.

36 MATERIALS SCIENCE↗

Interference in astronomical speckle patterns

Astronomical speckle patterns are examined in an atmospheric-optics context in order to determine what kind of image quality is to be expected from several different imaging techniques. The model used to describe the instantaneous complex field distribution across the pupil of a large telescope regards the pupil as a deep phase grating with a periodicity given by the size of the cell of uniform phase or the refractive index structure function. This model is used along with an empirical formula derived purely from the physical appearance of the speckle patterns to discuss the orders of interference in astronomical speckle patterns.

Breckinridge, J. B.↗

SpeckleNN: a unified embedding for real-time speckle pattern classification in X-ray single-particle imaging with limited labeled examples

With X-ray free-electron lasers (XFELs), it is possible to determine the three-dimensional structure of noncrystalline nanoscale particles using X-ray single-particle imaging (SPI) techniques at room temperature. Classifying SPI scattering patterns, or `speckles', to extract single-hits that are needed for real-time vetoing and three-dimensional reconstruction poses a challenge for high-data-rate facilities like the European XFEL and LCLS-II-HE. Here, we introduce SpeckleNN, a unified embedding model for real-time speckle pattern classification with limited labeled examples that can scale linearly with dataset size. Trained with twin neural networks, SpeckleNN maps speckle patterns to a unified embedding vector space, where similarity is measured by Euclidean distance. We highlight its few-shot classification capability on new never-seen samples and its robust performance despite having only tens of labels per classification category even in the presence of substantial missing detector areas. Without the need for excessive manual labeling or even a full detector image, our classification method offers a great solution for real-time high-throughput SPI experiments.

47 OTHER INSTRUMENTATION↗

Laser Speckle Pattern Stability in Hypersonic Regimes for Experimental Mechanics and Metrological Studies

Here, an empirical study assessing the suitability of laser speckle patterns for use in experimental mechanics research conducted at hypersonic conditions is presented. Speckle patterns generated via coherent optical scattering from a gold-coated graphite surface inserted into a Mach 10 air stream were collected and analyzed using Computer-Aided Speckle Interferometry using two methodologies: a typical spanwise approach involving increasing temporal span between image pairs, and a sequential approach that utilizes a combination of temporal re-referencing and spatial resampling. Results were characterized for spatial-temporal stability and variance. Our observations demonstrate that optical methods relying on stable and properly formed speckle patterns can be used in a hypersonic regime at various Reynolds numbers and common camera frame rates, but the technique is sensitive to the conditions of the airflow and the processing methodology chosen.

42 ENGINEERING↗

Speckle Pattern Application to Woven Softgoods

Space habitation is becoming more accessible and commercially available which is driving the development and testing of inflatable softgoods habitats that can be both lighter and more volume-efficient than heritage metallic pressure vessels. Photogrammetry test methods are used on new materials and larger inflatable softgood test articles to measure material displacement and strain during pressurization. A speckle pattern must be applied to the surface of interest for testing when using photogrammetry which is typically a very labor and time intensive process. Two methods were tested as options for a faster and more effective application to hand painting and temporary tattoos, which are the current application methods for the structural/restraint layer. One approach was to mix a plastic additive with a matte clear coat to create a speckle pattern that could be applied to the article. The second method uses a speckle paint gun to speckle the article after a white base coat is applied. Both methods adhered well to the Kevlar test sample materials and showed up well when examined with photogrammetry cameras. On the woven test samples the additive in a clear coat method could be applied evenly as was the paint gun method.

Rylee Cardon↗

Speckle Pattern Application to Woven Softgoods

Space habitation is becoming more accessible and commercially available which is driving the development and testing of inflatable softgoods habitats that can be both lighter and more volume-efficient than heritage metallic pressure vessels. Photogrammetry test methods are used on new materials and larger inflatable softgood test articles to measure material displacement and strain during pressurization. A speckle pattern must be applied to the surface of interest for testing when using photogrammetry which is typically a very labor and time intensive process. Two methods were tested as options for a faster and more effective application to hand painting and temporary tattoos, which are the current application methods for the structural/restraint layer. One approach was to mix a plastic additive with a matte clear coat to create a speckle pattern that could be applied to the article. The second method uses a speckle paint gun to speckle the article after a white base coat is applied. Both methods adhered well to the Kevlar test sample materials and showed up well when examined with photogrammetry cameras. On the woven test samples the additive in a clear coat method could be applied evenly as was the paint gun method.

Rylee Cardon↗

Speckle Pattern for Woven Softgood Habitats Photogrammetry Testing

Space habitation is becoming more accessible and commercially available which is driving the development and testing of inflatable softgoods habitats that can be both lighter and more volume-efficient than heritage metallic pressure vessels. Photogrammetry test methods are used on new materials and larger inflatable softgood test articles to measure material displacement and strain during pressurization. A speckle pattern must be applied to the surface of interest for testing when using photogrammetry which is typically a very labor and time intensive process. Two methods were tested as options for a faster and more effective application to hand painting and temporary tattoos, which are the current application methods for the structural/restraint layer. One approach was to mix a plastic additive with a matte clear coat to create a speckle pattern that could be applied to the article. The second method uses a speckle paint gun to speckle the article after a white base coat is applied. Both methods adhered well to the Kevlar test sample materials and showed up well when examined with photogrammetry cameras. On the woven test samples the additive in a clear coat method could be applied evenly as was the paint gun method.

Rylee Cardon↗

Operation Program for the Spatially Phase-Shifted Digital Speckle Pattern Interferometer - SPS-DSPI

SPS-DSPI software has been revised so that Goddard optical engineers can operate the instrument, instead of data programmers. The user interface has been improved to view the data collected by the SPS-DSPI, with a real-time mode and a play-back mode. The SPS-DSPI has been developed by NASA/GSFC to measure the temperature distortions of the primary-mirror backplane structure for the James Webb Space Telescope. It requires a team of computer specialists to run successfully, because, at the time of this reporting, it just finished the prototype stage. This software improvement will transition the instrument to become available for use by many programs that measure distortion

Blake, Peter N.↗

Optical Strain Measurement System Development

Investigations of physical phenomena affecting the durability of SSME components require measurement systems operational in hostile environments. The need for such instrumentation caused the definition and operation of an optical strain measurement system. This optical strain measurement system based on the speckle shift method is being developed. This is a noncontact, automatic method of measuring surface strain in one dimension that corrects for error due to rigid body motion. It provides a gauge length of 1 to 2 mm and allows the region of interest on the test specimen to be mapped point by point. The output is a graphics map of the points inspected on the specimen; data points is stored in quasi-real time. This is the first phase of a multiphase effort in optical strain measurement. The speckle pattern created by the test specimen is interpreted as high order interference fringes resulting from a random diffraction grating, being the natural surface roughness of the specimen. Strain induced on the specimen causes a change in spacing of the surface roughness, which in turn shifts the position of the interference pattern (speckles).

Lant, C. T.↗

Focusing a round coherent beam by spatial filtering the horizontal source

This paper illustrates the use of spatial filtering with a horizontal slit near the source to enlarge the horizontal coherence in an experimental station and produce a diffraction-limited round focus at an insertion device beamline for X-ray photon correlation spectroscopy experiments. Simple expressions are provided to guide the optical layout, and wave propagation simulations confirm their applicability. The two-dimensional focusing performance of Be compound refractive lenses to produce a round diffraction-limited focus at 11 keV capable of generating a high-contrast speckle pattern of an aerogel sample is demonstrated. The coherent scattering patterns have comparable speckle sizes in both horizontal and vertical directions. The focal spot sizes are consistent with hybrid ray-tracing calculations. Producing a two-dimensional focus on the sample can be helpful to resolve speckle patterns with modern pixel array detectors with high visibility. This scheme has now been in use since 2019 for the 8-ID beamline at the Advanced Photon Source, sharing the undulator beam with two separate beamlines, 8-ID-E and 8-ID-I at 7.35 keV, with increased partially coherent flux, reduced horizontal spot sizes on samples, and good speckle contrast.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

Reference-Free, Projection Background-Oriented Schlieren

A projection background-oriented schlieren (P-BOS) system is developed and demonstrated. Instead of a background that has a speckle pattern printed, painted, or otherwise deposited onto its surface, and can thus not be altered, the pattern here is projected onto the background. This allows for changes to the speckle pattern without replacement of the background material, which can be time-consuming and expensive. Reference images are acquired simultaneously with flow images. A pre-test transformation between the reference and flow images allows for on-the-fly changes to the speckle pattern during a test without requiring a stoppage of the flow, allowing for optimization of the BOS signal. Using a programmable LCD screen as the speckled optic allows for remote control of the speckle pattern. Because the background is not speckled, the system can be easily transformed to acquired shadowgraph images by removing the speckled optic and closing the aperture of the light source, which is useful for achieving measurements with higher spatial resolution. The system can be nearly as compact as a conventional BOS system, and can be assembled with polarized optics to reduce or eliminate window reflections and glare, making this system particularly well-suited for wind tunnel testing.

Joshua M Weisberger↗

Nondestructive Strain Measurement System Used to Determine Surface Strain on Fibers

Small-diameter structural fibers are being considered as reinforcements for high temperature ceramic matrix composite materials, and thus they require characterization. At the NASA Lewis Research Center, a nondestructive optical technique was used to determine surface strain on a structural fiber, in real time, as it was pulled in a tensile test machine. With this technique, interference or speckle patterns from the laser illuminated fiber test specimen are recorded. As the fiber is pulled, its speckle pattern shifts in proportion to the strain, translation, and rotation components of the sample deformation. Shifting speckle patterns are detected in real time by two linear charge-coupled discharge (CCD) camera arrays, and the images are processed by a hardware correlator. Surface strain is selectively detected on fibers with diameters on the order of 100 mm and can be resolved to 19 microstrain. This system was designed to be robust and compact and generally does not require surface preparation of the structural fibers. For strain detection, two laser beams are positioned incident on the structural fiber being tested, as shown in the photograph, where the test specimen is mounted in a tensile test machine via two coupons. As the fiber is pulled, the speckle pattern produced from each laser beam is detected by one of two CCD arrays located inside the tube on the right side of the photograph.

Tuma, Margaret L.↗

Laboratory Testbed Verification of Data Post-Processing Strategies for the WFIRST Coronagraph Instrument

One of the objectives of the WFIRST Coronagraph Instrument is to demonstrate post-processing algorithms for space-based exoplanet imaging data in the regime of very high contrast ratios (< 1E-8). We analyzed two 15-hour time series of laboratory images acquired with prototype coronagraph designs on a vacuum chamber testbed at JPL. These data sets enabled us to test the performance of reference differential imaging (RDI) PSF subtraction as a function of time and Euclidean (L2) speckle pattern distance. Starting from an analytical relationship between speckle pattern stability and classical subtraction gain, we compared the classical subtraction result to those of the KLIP RDI algorithm. In both data sets, KLIP RDI contrast gains are typically 3-4× greater than those of classical subtraction. These results suggest that a diverse reference PSF library will enable a significant gain in sensitivity beyond that suggested by the raw, frame-to-frame speckle pattern stability.

Ygouf, Marie↗

Porosity and Variations in Microgravity Aerogel Nano-Structures: New Laser Speckle Characterization Methods - 2

The transition from sol to gel is a process that is critical to the properties of engineered nanomaterials, but one with few available techniques for observing the dynamic processes occurring during the evolution of the gel network. Specifically, the observation of various cluster aggregation models, such as diffusion-limited and reaction-limited cluster growth can be quite difficult. This can be rather important as the actual aggregation model can dramatically influence the mechanical properties of gels, and is significantly affected by the presence of convective flows, or their absence in microgravity. We have developed two new non-intrusive optical methods for observing the aggregation processes within gels in real time. These make use of the dynamic behavior of laser speckle patterns produced when an intense laser source is passed through a gelling sol. The first method is a simplified time-correlation measurement, where the speckle pattern is observed using a CCD camera and information on the movement of the scattering objects is readily apparent. This approach is extremely sensitive to minute variations in the flow field as the observed speckle pattern is a diffraction-based image, and is therefore sensitive to motions within the sol on the order of the wavelength of the probing light. Additionally, this method has proven useful in determining a precise time for the gel-point, an event often difficult to measure. Monitoring the evolution of contrast within the speckle field is another method that has proven useful for studying aeration. In this case, speckle contrast is dependent upon the size (correlation length) and number of scattering centers, increasing with increasing size, and decreasing with increasing numbers. The dynamic behavior of cluster growth in gels causes both of these to change simultaneously with time, the exact rate of which is determined by the specific aggregation model involved. Actual growth processes can now be observed, and the effects of varying gravity fields on the growth processes qualitatively described. Results on preliminary ground-based measurements have been obtained.

Hunt, A. J.↗

An Internal Digital Image Correlation Technique for High-Strain Rate Dynamic Experiments

Full-field, quantitative visualization techniques, such as digital image correlation (DIC), have unlocked vast opportunities for experimental mechanics. However, DIC has traditionally been a surface measurement technique, and has not been extended to perform measurements on the interior of specimens for dynamic, full-scale laboratory experiments. This limitation restricts the scope of physics which can be investigated through DIC measurements, especially in the context of heterogeneous materials. The focus of this study is to develop a method for performing internal DIC measurements in dynamic experiments. The aim is to demonstrate its feasibility and accuracy across a range of stresses (up to 650 MPa), strain rates (10 3 - 10 6 s -1 ), and high-strain rate loading conditions (e.g., ramped and shock wave loading). Internal DIC is developed based on the concept of applying a speckle pattern at an inner-plane of a transparent specimen. The high-speed imaging configuration is coupled to the traditional dynamic experimental setups, and is focused on the internal speckle pattern. During the experiment, while the sample deforms dynamically, in-plane, two-dimensional deformations are measured via correlation of the internal speckle pattern. In this study, the viability and accuracy of the internal DIC technique is demonstrated for split-Hopkinson (Kolsky) pressure bar (SHPB) and plate impact experiments. The internal DIC experimental technique is successfully demonstrated in both the SHPB and plate impact experiments. In the SHPB setting, the accuracy of the technique is excellent throughout the deformation regime, with measurement noise of approximately 0.2% strain. In the case of plate impact experiments, the technique performs well, with error and measurement noise of 1% strain. The internal DIC technique has been developed and demonstrated to work well for full-scale dynamic high-strain rate and shock laboratory experiments, and the accuracy is quantified. Here, the technique can aid in investigating the physics and mechanics of the dynamic behavior of materials, including local deformation fields around dynamically loaded material heterogeneities.

36 MATERIALS SCIENCE↗

A two-dimensional white-light amplitude interferometer

A review of the applications of a point-symmetric, 180-degree, rotational shearing interferometer is given. Material includes, photographs of the Michelson stellar interferometer fringes from Alpha-Lyr, measures of amplitude of phase excursions in the atmosphere, and a measure of the order of interference of speckle patterns. New material includes unpublished double star speckle patterns to illustrate the isoplanatic patch, a measure of the time fluctuations in the earth's atmosphere, and measurements of the properties of a 256 channel linear reticon.

Breckinridge, J. B.↗