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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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DOE OSTI2020

Reconfigurable structure and tunable transport in synchronized active spinner materials

Ensembles of actuated colloids are excellent model systems to explore emergent out-of-equilibrium structures, complex collective dynamics, and design rules for the next generation materials. Here, we demonstrate that ferromagnetic microparticles suspended at an air-water interface and energized by an external rotating magnetic field spontaneously form dynamic ensembles of synchronized spinners in a certain range of the excitation field parameters. Each spinner generates strong hydrodynamic flows, and collective interactions of the multiple spinners promote a formation of dynamic lattices. On the basis of experiments and simulations, we reveal structural transitions from liquid to nearly crystalline states in this novel active spinner material and demonstrate that dynamic spinner lattices are reconfigurable, capable of self-healing behavior and that the transport of embedded inert cargo particles can be remotely tuned by the parameters of the external excitation field. Our findings provide insights into the behavior of active spinner materials with reconfigurable structural order and tunable functionalities.

36 MATERIALS SCIENCE↗

DOE OSTI2021

Emergence of Lanes and Turbulent-like Motion in Active Spinner Fluid

Assemblies of self-rotating particles are gaining interest as a novel realization of active matter with unique collective behaviors such as edge currents and non-trivial dynamic states. Here, we develop a continuum model for a system of fluid-embedded spinners by coarse-graining the equations of motion of the discrete particles. We apply the model to explore mixtures of clockwise and counterclockwise rotating spinners. We find that the dynamics is sensitive to fluid inertia: in the inertialess system, after transient turbulent-like motion the spinners segregate and form steady traffic lanes. At small but finite Reynolds number instead, the turbulent-like motion persists and the system exhibits a chirality breaking transition leading to a single rotation sense state. Our results shed light on the dynamic behavior of non-equilibrium materials exemplified by active spinners.

36 MATERIALS SCIENCE↗

NASA NTRS1995

HINCOF-1: a Code for Hail Ingestion in Engine Inlets

One of the major concerns during hail ingestion into an engine is the resulting amount and space- and time-wise distribution of hail at the engine face for a given geometry of inlet and set of atmospheric and flight conditions. The appearance of hail in the capture streamtube is invariably random in space and time, with respect to size and momentum. During the motion of a hailstone through an inlet, a hailstone undergoes several processes, namely impact with other hailstones and material surfaces of the inlet and spinner, rolling and rebound following impact; heat and mass transfer; phase change; and shattering, the latter three due to friction and impact. Taking all of these factors into account, a numerical code, designated HINCOF-I, has been developed for determining the motion hailstones from the atmosphere, through an inlet, and up to the engine face. The numerical procedure is based on the Monte-Carlo method. The report presents a description of the code, along with several illustrative cases. The code can be utilized to relate the spinner geometry - conical or, more effective, elliptical - to the possible diversion of hail at the engine face into the bypass stream. The code is also useful for assessing the influence of various hail characteristics on the ingestion and distribution of hailstones over the engine face.

Gopalaswamy, N.↗

DOE OSTI2023

Mechanistic origins of corrosion protection of aluminum alloys by graphene/polyetherimide nanocomposite coatings

Light-weighting vehicular components through adoption of light-metal structural alloys holds promise for reducing the fuel consumption of internal combustion engine vehicles and increasing the range of battery electric vehicles. However, the alloyed microstructure and surface precipitates of aluminum alloys render these materials susceptible to corrosion under modest excursions from neutral pH. Traditional chromium-based anodic passivation layers are subject to increasingly stringent environmental regulations, whereas options for sacrificial cathodic films are sparse for electropositive metals. While hybrid nanocomposite coatings have shown initial promise, mechanistic underpinnings remain poorly understood. Here, a fully imidized polyetherimide (PEI) resin is utilized as the continuous phase with inclusion of unfunctionalized exfoliated graphite (UFG). A comprehensive investigation of the mechanisms of corrosion protection reveals key fundamental design principles underpinning corrosion inhibition. First, strong interfacial adhesion, which for PEI is facilitated by binding of imide carbonyl moieties to Lewis acidic sites on Al surfaces. Second, the miscibility of ion-impervious nanoscopic UFG fillers and stabilization of a substantial interphase region at UFG/PEI boundaries that result in minimizing the free volume at the filler/polymer interface. Finally, extended tortuosity of ion diffusion pathways imbued by the below-percolation-threshold 2D fillers. These three design principles help govern and modulate ion transport from electrolyte/coating interfaces to the coating/metal interface and are crucial for the extended preservation of barrier properties. The results suggest an approach to systematically activate multiple modes of corrosion inhibition through rational design of hybrid nanocomposite coatings across hard-to-abate sectors where light metal alloys are likely to play an increasingly prominent role.

36 MATERIALS SCIENCE↗

NASA NTRS2001

Effect of convection on osteoblastic cell growth and function in biodegradable polymer foam scaffolds

Culture of seeded osteoblastic cells in three-dimensional osteoconductive scaffolds in vitro is a promising approach to produce an osteoinductive material for repair of bone defects. However, culture of cells in scaffolds sufficiently large to bridge critical-sized defects is a challenge for tissue engineers. Diffusion may not be sufficient to supply nutrients into large scaffolds and consequently cells may grow preferentially at the periphery under static culture conditions. Three alternative culturing schemes that convect media were considered: a spinner flask, a rotary vessel, and a perfusion flow system. Poly(DL-lactic-co-glycolic acid) (PLGA) foam discs (12.7 mm diameter, 6.0 mm thick, 78.8% porous) were seeded with osteoblastic marrow stromal cells and cultured in the presence of dexamethasone and L-ascorbic acid for 7 and 14 days. Cell numbers per foam were found to be similar with all culturing schemes indicating that cell growth could not be enhanced by convection, but histological analysis indicated that the rotary vessel and flow system produced a more uniform distribution of cells throughout the foams. Alkaline phosphatase (ALP) activity per cell was higher with culture in the flow system and spinner flask after 7 days, while no differences in osteocalcin (OC) activity per cell were observed among culturing methods after 14 days in culture. Based on the higher ALP activity and better cell uniformity throughout the cultured foams, the flow system appears to be the superior culturing method, although equally important is the fact that in none of the tests did any of the alternative culturing techniques underperform the static controls. Thus, this study demonstrates that culturing techniques that utilize fluid flow, and in particular the flow perfusion system, improve the properties of the seeded cells over those maintained in static culture.

NASA Discipline Cell Biology↗

NASA NTRS1986

Large-scale Advanced Prop-fan (LAP) hub/blade retention design report

The Large-scale Advanced Prop-fan (LAP) hub assembly forms a semi-rigid link between the blades, which provide the thrust, and the engine shaft, which provides the torque. The hub and tailshaft is a one piece partially forged part which is carburized, heat treated and machined. A single row ball bearing restrains each of the eight blades in the hub, while the tailshaft secures the propeller to the engine shaft with two cone seats that are preloaded against each other by the Prop-fan retaining nut. The hub also forms the support for the pitch change actuator system, the control and the spinner. The retention transmits the loads from the blades to the hub while allowing the changes in blade pitch. The single row ball bearing retention provides ease of maintenance by allowing individual blade replacement without dissassembly of the hub. It has a through hardened inner race which seats against the aluminum blade shank and an outer race which is integral with the barrel. The outer race area is carburized to achieve the hardness necessary to support the ball loads. The balls are kept from contact with each other by a separator. The rotational speed of the propeller keeps the retention submerged in the oil which is contained in the hub by a seal. Stress and strain analysis, material hardness requirements, weight predictions, and stiffness characteristics are discussed.

Soule, Matthew↗

NASA NTRS2006

Status of Solar Sail Propulsion: Moving Toward an Interstellar Probe

NASA's In-Space Propulsion Technology Program has developed the first-generation of solar sail propulsion systems sufficient to accomplish inner solar system science and exploration missions. These first-generation solar sails, when operational, will range in size from 40 meters to well over 100 meters in diameter and have an areal density of less than 13 grams-per-square meter. A rigorous, multiyear technology development effort culminated last year in the testing of two different 20-meter solar sail systems under thermal vacuum conditions. This effort provided a number of significant insights into the optimal design and expected performance of solar sails as well as an understanding of the methods and costs of building and using them. In a separate effort, solar sail orbital analysis tools for mission design were developed and tested. Laboratory simulations of the effects of long-term space radiation exposure were also conducted on two candidate solar sail materials. Detailed radiation and charging environments were defined for mission trajectories outside the protection of the earth's magnetosphere, in the solar wind environment. These were used in other analytical tools to prove the adequacy of sail design features for accommodating the harsh space environment. Preceding, and in conjunction with these technology efforts, NASA sponsored several mission application studies for solar sails, including one that would use an evolved sail capability to support humanity's first mission into nearby interstellar space. The proposed mission is called the Interstellar Probe. The Interstellar Probe might be accomplished in several ways. A 200-meter sail, with an areal density approaching 1 gram-per-square meter, could accelerate a robotic probe to the very edge of the solar system in just under 20 years from launch. A sail using the technology just demonstrated could make the same mission, but take significantly longer. Conventional chemical propulsion systems would require even longer flight times. Spinner sails of the type being explored by the Japanese may also be a good option, but the level of maturity in that technology is not clear. While the technology to support a 200-meter, ultralightweight sail mission is not yet in hand, the recent NASA investments in solar sail technology are an essential first step toward making it a reality. This paper will describe the status of solar sail propulsion within NASA, near-term solar sail mission applications, and the plan to advance the technology to the point where the Interstellar Probe mission can be flown.

Johnson, Les↗

DOE OSTI2024

Oxidation Temperature-Dependent Electrochemical Doping of WO 3 Deposited via Atomic Layer Deposition

Silicon-based photoelectrochemical devices show promise for the performance of light-driven CO 2 reduction but suffer from instability under photoelectrochemical conditions relevant to CO 2 reduction. Coating silicon electrodes with thin layers of metal oxides has shown promise to passivate unstable silicon surfaces, and many different metal oxides can be deposited on silicon using various techniques. In this study, we investigate the fundamental photoelectrochemical performance of WO 3 -coated silicon photoelectrodes, which were generated by oxidation of W-metal films deposited via atomic layer deposition on both degenerately doped (nSi + ) and low-doped (pSi) silicon. Two different oxidation temperatures were investigated (400 and 600 °C), and it was found that the monoclinic phase of WO 3 predominates at both temperatures but that more grain boundaries are present in the 600 °C film. From X-ray photoelectron spectroscopy, the stoichiometry of both films was found to be 1:3 W:O, and low electron energy loss experiments indicate band gaps of 3.0 and 3.1 eV for 400 and 600 °C films, respectively. Cyclic voltammetry experiments showed that the electron transfer kinetics increased after continued redox cycling, particularly for the material produced at 400 °C. X-ray photoelectron spectra suggest that the observed increase in electrode conductivity is due to the formation of oxygen vacancies in the film. Electrochemical impedance spectroscopy indicated that charge transport through the films was impacted by the grain boundaries that formed during oxidation of the film. Photoelectrochemical studies on pSi/WO 3 electrodes were highly variable, only producing a photocurrent and photovoltage with some samples. Our best sample, formed at 400 °C, produced a photovoltage of 180 mV, which is lower than what has previously been reported for WO 3 -coated silicon (500 mV). We hypothesize that the variability in photoelectrochemical experiments arose from a roughened WSiO x interface that is generated during film preparation. WO 3 shows promise as a metal oxide coating for silicon, but our results suggest that formation of a high-quality interface between Si and WO 3 is vital for best performance.

Charge transfer↗