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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2018

The Effect of 1–10-MeV Neutrons on the JESD89 Test Standard

Here, the JESD89 test standard defines how terrestrial neutron testing is conducted [1] . The test standard covers a number of different types of radiation used for testing, including protons, neutrons, and alphas, and different types of testing, including life testing and accelerated testing. Broad-spectrum neutron testing is the most common type of accelerated radiation testing for the terrestrial radiation environment. Unlike most test standards, the JESD89 defines the minimum energy for determining the cumulative fluence for the deployed and test environment. Currently, the minimum energy is set at 10 MeV. As the test standard is currently being rewritten, changing the minimum energy to 1 MeV is being explored, because it is believed that the onset to neutron-induced single-event effects (SEEs) is less than 10 MeV. There are three separate problems with lowering the minimum energy: determining whether electronics have a sensitivity to neutron-induced SEEs below 10 MeV, determining whether the test spectra match the terrestrial environment in the 1–10-MeV range, and the measurement error caused by not including the fluence from 1 to 10 MeV. In this paper, we present information on these factors and whether the minimum energy should be lowered to 1 MeV.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
DOE OSTI2023

Development of ASTM International D8405—Standard Test Method for Evaluating PM 2.5 Sensors or Sensor Systems Used in Indoor Applications

Sensors and sensor systems for monitoring fine particles with aerodynamic diameters smaller than 2.5 µm can provide real-time feedback on indoor air quality and thus can help guide actions to manage indoor air pollutant concentrations. Standardized verification of the performance and accuracy of sensors and sensor systems is crucial for predicting the efficacy of such monitoring. A new ASTM International standard test method (ASTM D8405) was created for this need and is the most exacting laboratory protocol published to date for evaluating indoor air quality sensors and sensor systems measuring particles smaller than 2.5 µm in diameter. ASTM D8405 subjects sensors and sensor systems to five test phases: (1) an initial particle concentration ramp; (2) exposure to various temperature and humidity conditions; (3) exposure to interfering particles; (4) temperature cycling; and (5) a final particle concentration ramp to assess drift. This paper discusses the development of the standard test method, key aspects of the testing process, example evaluation results, and a comparison of this standard test method against peer evaluation protocols.

47 OTHER INSTRUMENTATION↗
DOE OSTI2019

Guidance on the Use of Existing ASTM Polymer Testing Standards for ABS Parts Fabricated Using FFF

When evaluating the static mechanical performance of fused filament fabrication (FFF) polymers, researchers have conducted tensile testing using American Society for Testing Materials International (ASTM) D3039 rectangular test specimens and ASTM D638 Type I and Type IV dogbone test specimens. The choice of ASTM D638 versus ASTM D3039 test specimen geometry is usually based on the perceived susceptibility of the ASTM D638 test specimens to failure within the fillet radius. ASTM polymer and plastic tensile test standards define criteria for acceptably tested specimens as requiring failure inside the narrow length (i.e., ASTM D638) or outside of the grips (i.e., ASTM D3039) for the results to be considered acceptable. There has been limited published research regarding the selection of an ASTM test specimen geometry for FFF polymer materials. This study provides evidence-based guidance through the comparison of the mechanical performance and failure acceptance rates of ASTM D3039 and ASTM D638 test specimen geometries, fabricated using FFF acrylonitrile butadiene styrene (ABS). Here, the purpose of the study is to provide guidance on the use of existing ASTM polymer testing standards for additively manufactured polymers. Results indicate there is an inherent benefit to using ASTM D3039 over ASTM D638 Type I and Type IV test specimens for tensile testing. ASTM D3039 test specimens provide the most consistent failure within the test specimen’s gage length, which is attributed to the rectangular design of the test specimen. Results also indicated that, like traditionally manufactured polymer composites, there will be differences in the tensile test results (e.g., ultimate tensile strength, elastic modulus) based on the different cross-sectional areas of the test specimen geometries.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Binary pseudorandom array test standard optimized for characterization of large field-of-view optical interferometers

Recently, a technique for calibrating the modulation transfer function (MTF) of a broad variety of metrology instrumentation has been demonstrated. This technique is based on test samples structured as one-dimensional binary pseudo-random (BPR) sequences and two-dimensional BPR arrays (BPRAs). The inherent power spectral density of BPR gratings (sequences) and arrays has a deterministic white-noise-like character that allows direct determination of the MTF with uniform sensitivity over the entire spatial frequency range and field-of-view of an instrument. As such, the BPR samples satisfy the characteristics of a test standard: functionality, ease of specification and fabrication, reproducibility, and low sensitivity to manufacturing error. Here we discuss our recent developments directed to the optimization of the sample design, fabrication, application, and data processing procedures, suitable for thorough characterization of large aperture optical interferometers. Compared with the previous coded-aperture based design, the improved, 'highly randomized' BPRA pattern of the new test standard provides better accuracy and reliability of instrument MTF and aberration characterization, and enables operation optimization of large aperture optical interferometers. We describe the pattern generation algorithm and tests to verify the compliance to desired BPRA topography. The data acquisition and analysis procedures for different applications of the technique are also discussed.

Yashchuk, Valeriy V.↗
DOE OSTI2019

Test Standards: Displacement Damage [Slides]

This report contains a set of slides intended for the 2019 Los Alamos National Laboratory (LANL) radiation effects summer school. On the topic of testing standards for displacement damage, this presentation discusses the purpose of tests, the test instruments used, pre-exposure and exposure procedures, and documentation requests and reports.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2024

Optimization-Based Model Reduction Scheme for Renewable Energy Power Plants Using Standardized Testing Scenarios

This paper presents an optimization-based model reduction scheme for renewable energy (RE) power plants consisting of inverter-based resources (IBRs) operating in grid-following (GFL) or grid-forming (GFM) modes. More importantly, the datasets feeding the optimization-based model reduction scheme are generated and re-used through the standardized grid-interactive testing scenarios. Particularly, the proposed scheme makes use of the power plant point of common coupling (PCC) measurements of various quantities specified by standardized tests (e.g., voltage and frequency ride through) as per IEEE 2800, to estimate the parameters of the reduced-order model such that its dynamic performance aligns with the original detailed power plant model. The proposed model reduction approach does not require the parameters of individual IBRs and using standardized test data as input to the formulated optimization problem simplifies the reduced-order modelling scheme. Extensive case studies following standardized test scenarios verified the remarkable accuracy of the proposed approach.

Yallamilli, Ram S. [Purdue University]↗
DOE OSTI2018

Characterization and operation optimization of large aperture optical interferometers using binary pseudorandom array test standards

Recently, a technique for calibration of the Modulation Transfer Function (MTF) of a broad variety of metrology instrumentation has been established. The technique is based on test samples structured according to binary pseudorandom (BPR) one-dimensional sequences and two-dimensional arrays. The inherent power spectral density of BPR gratings and arrays, has a deterministic white-noise-like character that allows a direct determination of the MTF with a uniform sensitivity over the entire spatial frequency range and field-of-view of an instrument. As such, the BPR samples satisfy the characteristics of a test standard: Functionality, ease of specification and fabrication, reproducibility, and low sensitivity to manufacturing error. Here we discuss our recent developments working with support of the U.S. Department of Energy on industrialization of the technique. The goal is to develop affordable BPR test samples, application procedures, and data processing software, suitable for thorough characterization of optical interferometers and microscopes, as well as x-ray, electron (scanning and transmission), and atomic force microscopes. We report on the development of BPR array test samples optimized for advanced characterization (including the instrumental MTF and aberrations) and operation optimization of large aperture optical interferometers. We describe the sample fabrication process and tests to verify the compliance to desired surface topography. The data acquisition and analysis procedures for application of the technique for precise focusing of Fizeau interferometer are discussed in detail.

Yashchuk, VV↗
DOE OSTI2023

A review of regulatory standard test methods for residential wood heaters and recommendations for their advancement

In many regions, residential wood heaters are a leading source of harmful air pollution but only satisfy a small portion of local heating demands. In response, standardized laboratory test methods have been developed to characterize and limit wood heater emissions. While these test methods are a key tool for advancing both wood heater technology and environmental regulations, many of the experimental procedures are outdated and provide few actionable insights for improving heater performance. Furthermore, these test methods vary widely around the world and may not adequately capture the performance of wood heaters operating in residences. This study presents a comprehensive review of standardized wood heater test methods to identify fundamental experimental objectives and regulated performance metrics. Using the results of this review, recommendations are provided to make the test methods more accessible and representative of residential performance, while generating actionable data to motivate heater design improvements. This study elucidates the current state of standard test methods, and the developments needed to advance clean wood heater technologies and public policies.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗
DOE OSTI2021

Antimicrobial properties of nanostructured surfaces – demonstrating the need for a standard testing methodology

Bioinspired nanostructured materials that exhibit antimicrobial properties are being synthesized and tested at increasing rates for use in healthcare, manufacturing processes, and diagnostics. Although progress has been made in improving and understanding their bactericidal activity, arguably, the biggest problem currently in the field is the lack of a standard testing methodology that allows for optimal characterization and better comparison of emerging nanostructures. In this work, we examine two forms of nanostructured silicon that vary in their ability to kill certain bacterial species due to different physical mechanisms and derive guidelines for the comparative testing. We perform a comprehensive evaluation of methodologies used extensively in the field (e.g., colony counting and live dead analysis) and the novel application of high-throughput flow cytometry. The data reveal how the techniques are complementary but not always directly equivalent or correlative. Therefore, comparison of results obtained using different methodologies on different materials can be grossly misleading. We report significant variations in bactericidal efficiencies depending on experimental environments (medium type, etc.) and methodologies employed. In addition, we demonstrate how cytometry is yet another powerful complementary tool that can aid the mechanistic understanding of antimicrobial activities of rough surfaces. Besides standardization for comparison, ultimately, evaluation methods need to consider anticipated applications. Then and only then can the true potential (or limitation) of a novel material be determined for its suitability for advancement in a particular field of use.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2019

JESD89 Test Standard [Slides]

This report contains a set of slides discussing JESD89A, specifically the revision of JESD89 from August 2001, intended for a presentation at a summer school at Los Alamos National Laboratory (LANL). It discusses how tests are designed and the different types of tests implemented, including real time testing, alpha testing, fast neutron testing, and thermal neutron testing.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
DOE OSTI2019

Development of a Standard Test Method for Reducing the Uncertainties in Measuring the Capture Efficiency of Range Hoods

Cooking activities are a major source of indoor air pollutants. To control pollutants generated from cooking activities, a range hood is commonly used in residential kitchens. Several building codes require that a range hood be installed in new homes to control pollutants from cooking, and the required airflow rates for range hoods are specified by indoor air quality (IAQ) standards. However, air flow alone does not tell us how much of the cooking pollutants are exhausted by the range hood. A better metric to evaluate range hood IAQ performance is capture efficiency (CE)—the fraction of contaminants emitted during cooking that are exhausted directly to the outside via the range hood. This paper summarizes the development of a range hood CE test method for use in laboratory testing and equipment rating.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗
DOE OSTI2018

Towards the development of a standardized testing protocol for overhead island kitchen exhaust devices: Procedures, measurements and paths forward

Cooking is one of the most important sources of airborne pollutants in the indoor environments of residential buildings. Elevated concentrations of NO 2 due to cooking have been reported widely (Garret et al. 1998; Garrett et al. 1999; Mullen et al. 2016; Ryan et al. 1988; Schwab et al. 1994; J. Spengler et al. 1994; J. D. Spengler et al. 1983; Wilson et al. 1995). Many researchers have attributed elevated particulate concentrations to cooking, and some have attributed extremely high short-term concentrations of fine particles (>300 μg/m3) and ultrafine particles (>105 μg/m3) to cooking events (Abdullahi et al. 2013; Abt et al. 2000; Afshari et al. 2005; Buonanno et al. 2009; He et al. 2004; Kearney et al. 2011; Lance A. Wallace et al. 2004; See and Balasubramanian 2008; Stieb et al. 2008; Wallace and Ott 2011; Wheeler et al. 2011; Zhang et al. 2010). Cooking is also a source of other gas-phase pollutants including carbon monoxide, formaldehyde, acrolein, and other volatile organic compounds (Garret et al. 1998; Garrett et al. 1999; Logue et al. 2013; Mullen et al. 2016; Ryan et al. 1988; Schwab et al. 1994; J. Spengler et al. 1994; J. D. Spengler et al. 1983; V. Seaman et al. 2007; Wilson et al. 1995). Lastly, cooking can be a significant source of water vapor, and the water vapor produced from cooking can eventually lead to moisture-related problems (Parrott and Emmel 2003)

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗
DOE OSTI2024

Status memorandum on ORNL support of vendor irradiation capsule design and ASME irradiation code development and new ASTM test standard development activities

This report is in submission of completion of the Level 4 milestone number M4TG-24OR0501111 within the larger Advanced Reactor Technologies Gas Cooled Reactor program at Oak Ridge National Laboratory (ORNL). The focus of this year’s efforts is to continue support of industry needs related to the development of future industry-funded irradiation programs. At ORNL these efforts included the development of a generalized three-dimensional CAD model of an irradiation creep capsules for graphite, cost estimates of the expansion of the Materials Irradiation Facility (MIF), involvement with ASTM D02.F0 “Manufactured Carbon and Graphite Products” and the ASME Boiler and Pressure Vessel Code, and publication of papers supporting these efforts. This report will document the status of these activities.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗
DOE OSTI2024

Effect of Sample Thickness on the Tensile Strength of Small Graphite Discs

This report formally documents the completion of the Advanced Reactor Technologies (ART) Level 3 Milestone (M3TG-24OR0501054), “Continue activities related to Split Disc-DIC - complete analysis of effect of sample thickness on one fine grain graphite,” due May 31, 2024. Details within this report outline the status of activities aimed at elucidating the effect of sample thickness on the tensile strength measurement using the small-disc, split-disc testing standard in support of the US Department of Energy’s ART Graphite R&D Program. The ASTM D8289, Standard Test Method for Tensile Strength Estimate by Disc Compression of Manufactured Graphite, was developed to provide an alternative means for testing tensile strength on smaller specimens, which are compatible with available irradiation capsule volumes, and other compatibility measurements. ASTM D8289 specifies that acceptable specimen diameter can range from 6 to 12.7 mm and that the maximum allowed sample thickness should be half of the diameter. However, information is limited with respect to the effect of thickness on the measured splitting tensile strength. This report documents efforts to understand the effect of sample thickness on splitting tensile strength. The work involved testing Ø12.7 mm samples of fine-grain graphites 2114 and IG-110 of different thicknesses (6.35, 5, 4, and 3 mm). The digital image correlation (DIC) method was applied to the samples, along with the ASTM D8289 Standard, to help interpret the measured results.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Interlaboratory Round Robin Study on Axial Tensile Properties of Tubular SiC/SiC Specimens

Extensive research and development work is being conducted at different governmental, university and industrial laboratories for developing accident tolerant fuel-cladding systems for light water reactors. Continuous SiC fiber-reinforced SiC matrix (SiC/SiC) composites is one of the candidate materials for replacing the traditional zirconium alloy cladding due to its high temperature stability, chemical inertness and stability under neutron irradiation. A comprehensive database on the statistics of the mechanical properties of SiC/SiC composite is much needed to estimate the failure probability in evolving thermo-mechanical conditions as well as rigorous analysis of the material’s behavior under normal and off-normal reactor conditions. In addition to the properties database, test standards, which ensure the unbiased characterization of the material, are needed. The mechanical properties database, particularly for tubular SiC/SiC specimens, is limited and standardized test methods are still under development.

36 MATERIALS SCIENCE↗