In-Situ Laser-Based Ultrasonic Measurement of Material Cooling from Supersonic and Hypersonic Flow
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Many industrial processes are inaccessible or inhospitable to characterization by traditional temperature measurement methods, such as thermocouples, especially over prolonged exposure to harsh environments. Ultrasound is an established characterization technology with diverse applications ranging from medical imaging to therapies to flaw detection to nondestructive evaluation. Ultrasound may characterize solid materials and components noninvasively as a nondestructive evaluation modality and obtain internal measurements of material properties. For example, the speed of ultrasound propagation changes with Young’s modulus and Poisson’s ratio, which can be found from its measurements. Traditional ultrasonic characterization assumes all material properties remain constant with the position. When this assumption holds, a property of interest may be measured by relating it to the speed of ultrasound propagation (or a speed of sound, SOS) and measuring the SOS by timing the ultrasound propagation through a known distance. However, when a property of interest is spatially distributed, the propagation time depends on the SOS changing with the position along the ultrasound propagation path. The multiple temperature distributions may lead to an identical time of flight (TOF). Temperature is one property that impacts the speed of ultrasound and often cannot be assumed to remain constant with the position. Previously, in the context of temperature, we addressed the challenge of ultrasonic characterization of spatially distributed properties by developing a method for measuring segmental temperature distributions (MSTD). This method divides the ultrasonic propagation into segments bound by echogenic features. These features provide ultrasonic interfaces where some energy is reflected toward the receiving transducer, and the rest continues through the medium. The time-of-flight between the echoes reflected from echogenic features characterizes the spatial distribution in the properties of interest in the corresponding segment of the ultrasonic propagation path. This project demonstrated the application of the MSTD method in industrial conditions of the coal-fired power plant. We implemented the MSTD using metals and alloys waveguides, which may be the existing structure for which the temperature distribution is characterized or purposefully designed waveguides added to the structure by welding or other means specifically to quantify thermal properties using the MSTD method. Previous iterations of the MSTD method used ceramic and cementitious waveguides, which significantly attenuate ultrasound. On the other hand, low attenuation in metallic waveguides creates interactions between echogenic features which compilates the signal analysis in the segmental TOF measurements. We have established the WG design principles that minimize the interferences between trailing and primary echoes and, in some cases, eliminate them. The waveguides in which echoes do not interfere improve the timing accuracy and the robustness of ultrasonic measurements of the spatial distributions in material properties. Our emphasis remained on the estimation of the temperature distributions. We have developed general recommendations for designing ultrasonically segmented waveguides with the reduced influence of trailing echoes. Two of our waveguide designs were tested in the industry. The first waveguide was designed for insertion into a combustion zone of the utility-scale coal-fired power plant boiler. The second design allows the characterization of temperature distribution in the direction normal to the boiler’s water wall, a large heat exchanger converting the chemical energy released during combustion to the steam driving the electrical power generation turbines. These waveguides were designed to operate within a restrictive space of thermally insulated water wall and incorporate densely located echogenic features while combatting the influence of trailing echoes. The project has successfully demonstrated the feasibility of using the developed method for accurate, continuous, and robust temperature measurements in extreme environments of power generation and other industrial processes. It, therefore, has achieved its overarching goal of advancing the technology readiness level of the novel Ultrasound Measurements of Segmental Temperature Distribution (US-MSTD) method for real-time measurements of the temperature distribution and heat fluxes closer to commercial availability, developing a prototype multipoint measurement system, and validating its performance on coal-fired utility boilers. The success of this project was achieved in collaboration with the power generator, Rocky Mountain Power, and set the stage for the transfer of this technology from the laboratory to the industry.
Most ultrasonic measurements of materials involve the generation of an acoustic wave and the propagation of that wave from a transducer through a coupling medium to a specimen under test. After interacting with the specimen, the wave propagates through the coupling medium to a receiving transducer and is converted to an electrical signal. The information presented to the observer by the electrical signal depends on each element of the system. In this paper, the role that the receiving transducer plays in ultrasonic measurements is examined. The phase-sensitive nature of conventional receiving transducers has, for the most part, been neglected in nondestructive evaluations. This is shown to lead to significant data misinterpretation. A new acoustoelectric transducer (AET) has been developed which is phase insensitive. Comparative data obtained with both conventional and AET transducers are presented and discussed. The AET is shown to produce more accurate measurements for the cases investigated.
Standing wave ultrasonic techniques for the measurement of very small changes in acoustic attenuation and phase velocity are discussed. Enhanced sensitivity to these small changes was achieved by making the specimen part of a composite ultrasonic resonator. It was found that a point of maximum sensitivity on the response of such an ultrasonic resonator need not coincide with a point of maximum signal-to-error ratio. A model is presented and analyzed which takes into account error due to long term (low frequency) noise effects such as gain drifts and dc level shifts. This model yields a quantitative value for the signal-to-error ratio in which the signal is defined as the ideal change in the monitored response and the error as the difference between the experimentally measured change and the signal. The specific frequency dependent forms for the ultrasonic response and the sensitivity enhancement factor were used to predict the operating point on a mechanical resonance corresponding to maximum signal-to-error ratio.
Pulse echo ultrasonic measurement of thin film layer between thick media, using real time computation
Ultrasonic measurement of core material temperature in nuclear rocket engines
Ultrasonic techniques to measure residual stress in surface of aluminum structures
Ultrasonic testing system yields data on elastic constants of matrix/fiber laminated composite material. Related to one described in "Ultrasonic System Measures Elastic Properties of Composites" (NPO-18729). Tests performed nondestructive, and involve access by ultrasonic probes to only one side of material specimen. In comparison with other available ultrasonic testing systems, this system relatively inexpensive, and based on testing technique that is simpler and rapidly yields more-accurate results.
Two ultrasonic methods for nondestructive measurements of the depth of a case-hardened layer in steel are described. One method involves analysis of ultrasonic waves diffused back from the bulk of the workpiece. The other method involves finding the speed of propagation of ultrasonic waves launched on the surface of the work. Procedures followed in the two methods for measuring case depth are described.
Ultrasonic measurements of density and elastic constants at high pressure
Extreme environmental conditions are common in energy conversion applications, in which the most hardened insertion sensors often do not perform reliably for long. On the other hand, ultrasonic measurements can be acquired noninvasively, with sensitive components kept away from the damaging environment. We have previously developed the ultrasonic method for measuring the spatial distribution of temperatures in solid materials applicable when large thermal gradients are present. In the developed approach, we use the echogenically segmented ultrasound propagation path, structured to contain engineered or naturally occurring echogenic features, to produce a train of echoes in response to an external pulse of ultrasonic excitation. This paper outlines the testing results of this approach applied to the temperature distribution measurements to a waterwall of a 500 MW power-plant utility boiler. The validation results obtained over the prolonged power plant test show that the estimated temperature profile is correctly captured, and the measurement accuracy can be comparable with traditional insertion sensors, such as thermocouples. Overall, the testing has confirmed that the developed approach has matured to become an attractive alternative to conventional sensing in solving challenging problems of long-term temperature measurements in extreme environments. Heat fluxes and thermal stresses in the structure can then be characterized noninvasively using the measured temperature distribution as the basis.
New technique improves accuracy of measurements of ultrasonic shearwave velocity. Technique eliminates need to measure incident sound angle. Technique contains groove in which steel sphere is placed. Sphere act as reference point for measuring path lengths and propagation times. Velocity measurements are within 1 percent of published data.
High temperature ultrasonic temperature measurements in nuclear rocket engine to determine feasibility of rhenium sensor as high temperature sensor
A 6-segment subscale motor was developed to generate a range of internal environments from which multiple propellants could be characterized for erosive burning. The motor test bed was designed to provide a high Mach number, high mass flux environment. Propellant regression rates were monitored for each segment utilizing ultrasonic measurement techniques. These data were obtained for three propellants RSRM, ETM- 03, and Castor@ IVA, which span two propellant types, PBAN (polybutadiene acrylonitrile) and HTPB (hydroxyl terminated polybutadiene). The characterization of these propellants indicates a remarkably similar erosive burning response to the induced flow environment. Propellant burnrates for each type had a conventional response with respect to pressure up to a bulk flow velocity threshold. Each propellant, however, had a unique threshold at which it would experience an increase in observed propellant burn rate. Above the observed threshold each propellant again demonstrated a similar enhanced burn rate response corresponding to the local flow environment.
The development of a quantitative nondestructive method which involves ultrasonic attenuation measurements in frequency domain to determine volume fraction of porosity in aluminum cast is discussed. The aluminum alloy A357 casting samples were produced at the Ohio State University Foundry with controlled porosity contents ranging from 0% to 6%. A computer controlled system was used to direct ultrasonic beam to a test sample to different places to conduct ultrasonic attenuation measurements. The plot of attenuation coefficients as a function of frequency was then evaluated based on existing theories to determine volume fraction of porosity and pore size.
In this paper we report a data analysis protocol for ultrasonic velocity measurements carried out in a synchrotron x-ray facility based multi-anvil high-pressure apparatus. Synthetic ultrasonic signals for the time period between echoes from the two ends of the sample assembly are created with a few simple parameters as the echo waveform is modeled by the first echo from the anvil-assembly boundary. Each echo is modeled as a delta function with an amplitude and arrival time and convolved with this waveform. The final waveform, fit to the data, enables analysis of signals with overlapped echoes as they are common in small cell assemblies and high pressure.
Resonant ultrasonic spectroscopy is an effective methodology capable of measuring a change in modal resonant frequencies of material structures. It encompasses techniques based on ultrasonic frequencies employed to estimate elastic coefficients in solids. It is these frequencies that are uniquely characterized by the material shape, coefficients, symmetry and density that are used to improve and detect changes especially during the additive manufacturing (AM) process. In this report a variety of techniques to extract and validate material resonances are developed starting first with the background theory required to comprehend the approaches. Once the theory is established, various signal processing methodologies are applied to estimate the underlying resonances leading to the extraction of the critical elastic coefficients characterizing the specimen under test. A detailed case study based on wire arc additive manufacturing is discussed demonstrating the applicability of the various approaches.
The purpose of this dissertation was the following: (1) to characterize the effect of pore fraction on a comprehensive set of electrical and magnetic properties for the yttrium-barium-copper-oxide (YBCO) high temperature ceramic superconductor; and (2) to determine the viability of using a room-temperature, nondestructive characterization method to aid in the prediction of superconducting (cryogenic) properties. The latter involved correlating ultrasonic velocity measurements at room temperature with property-affecting pore fraction and oxygen content variations. The use of ultrasonic velocity for estimating pore fraction in YBCO is presented, and other polycrystalline materials are reviewed, modeled, and statistically analyzed. This provides the basis for using ultrasonic velocity to interrogate microstructure. The effect of pore fraction (0.10-0.25) on superconductor properties of YBCO samples was characterized. Spatial (within-sample) variations in microstructure and superconductor properties were investigated, and the effect of oxygen content on elastic behavior was examined. Experimental methods used included a.c. susceptibility, electrical, and ultrasonic velocity measurements. Superconductor properties measured included transition temperature, magnetic transition width, transport and magnetic critical current density, magnetic shielding, a.c. loss, and sharpness of the voltage-current characteristics. An ultrasonic velocity image constructed from measurements at 1mm increments across a YBCO sample revealed microstructural variations that correlated with variations in magnetic shielding and a.c. loss behavior. Destructive examination using quantitative image analysis revealed pore fraction to be the varying microstructural feature.