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Allen, J. L.

Publications and source records attributed to Allen, J. L..

At least 19 records

Laser pyrolysis fabrication of ferromagnetic gamma'-Fe4N and FeC nanoparticles

Using the laser pyrolysis method, single phase gamma'-Fe4N nanoparticles were prepared by a two step method involving preparation of nanoscale iron oxide and a subsequent gas-solid nitridation reaction. Single phase Fe3C and Fe7C3 could be prepared by laser pyrolysis from Fe(CO)5 and 3C2H4 directly. Characterization techniques such as XRD, TEM and vibrating sample magnetometer were used to measure phase structure, particle size and magnetic properties of these nanoscale nitride and carbide particles. c2000 American Journal of Physics.

NASA Discipline Life Sciences Technologies

Point defect formation in optical materials expos ed to the space environment

Point defect formation associated with early stages of optical damage was observed unexpectedly in two, and possibly three, different optical materials subjected to short-duration space exposure. Three calcium fluoride, two lithium fluoride, and three magnesium fluoride samples were flown on Space Shuttle flight STS-46 as part of the Evaluation of Oxygen Interactions with Materials - Third Phase experiment. One each of the calcium and magnesium fluoride samples was held at a fixed temperature of 60 C during the space exposure, while the temperatures of the other samples were allowed to vary with the ambient temperature of the shuttle cargo bay. Pre-flight and post-flight optical absorption measurements were performed on all of the samples. With the possible exception of the magnesium fluoride samples, every sample clearly showed the formation of F-centers in that section of the sample that was exposed to the low earth orbit environment. Solar vacuum ultraviolet radiation is the most probable primary cause of the defect formation; however, the resulting surface metallization may be synergistically altered by the atomic oxygen environment.

Allen, J. L.

A high-efficiency acoustic chamber and the anomalous sample rotation

A high efficiency acoustic chamber for the levitation and manipulation of liquid or molten samples in a microgravity environment has been developed. The chamber uses two acoustic drivers that are mounted at opposite corners of the chamber; by driving these at the same frequency, with 18-deg phase shifts, an increase in force of a factor of 3-4 is obtainable relative to the force of a single-driver system that is operated at the same power level. This enhancement is due to the increased coupling between the sound driver and the chamber. An anomalous rotation is noted to be associated with the chamber; this is found to be eliminated by a physically as-yet inexplicable empirical solution.

Wang, Taylor G.

Laser Pyrometer For Spot Temperature Measurements

Laser pyrometer makes temperature map by scanning measuring spot across target. Scanning laser pyrometer passively measures radiation emitted by scanned spot on target and calibrated by similar passive measurement on blackbody of known temperature. Laser beam turned on for active measurements of reflectances of target spot and reflectance standard. From measurements, temperature of target spot inferred. Pyrometer useful for non-contact measurement of temperature distributions in processing of materials.

Elleman, D. D.

Rotation Control In A Cylindrical Acoustic Levitator

Second driver introduces net circulation around levitated sample. Two transducers produce two sets of equal counterrotating acoustic fields. By appropriate adjustment of amplitudes and phases in two transducers, total acoustic field made to consist of two unequal counterrotating fields, producing net torque on levitated sample.

Barmatz, M. B.

The glass transition, crystallization and melting in Au-Pb-Sb alloys

The glass transition, crystallization and melting of Au(55)Pb(22.5)Sb(22.5) alloys have been studied by differential scanning calorimetry DSC. Crystallization on heating above the glass transition temperature Tg (45 C) begins at 64 C. Further crystallization events are observed at 172 C and 205 C. These events were found to correspond to the formation of the intermetallic compounds AuSb2, Au2Pb, and possibly AuPb2, respectively. Isothermal DSC scans of the glassy alloy above Tg were used to monitor the kinetics of crystallization. The solidification behavior and heat capacity in the glass-forming composition range were determined with droplet samples. An undercooling level of 0.3T(L) below the liquidus temperature T(L) was achieved, resulting in crystallization of different stable and metastable phases. The heat capacity C(P) of the undercooled liquid was measured over an undercooling range of 145 C.

Lee, M. C.

Noncontact temperature pattern measuring device

This invention relates to a noncontact imagine pyrometer system for obtaining the true temperature image of a given substance in a contactless fashion without making assumptions about localized emissivity of the substance or the uniformity of the temperature distribution. Such a contactless temperature imaging system has particular application in the study and production of many materials where the physical contact required to make a conventional temperature measurement drastically effects or contaminates the physical process being observed. Two examples where accurate temperature profiles are of critical interest are: (1) the solid-liquid phase change interface in the production of electronic materials and (2) metastable materials in the undercooling region. The apparent novelty resides in the recognition that an active pyrometer system may be advantageously adapted to perform contactless temperature imaging so that an accurate temperature profile can be obtained.

Elleman, D. D.

Levitation With a Single Acoustic Driver

Pair of reports describes acoustic-levitation systems in which only one acoustic resonance mode excited, and only one driver needed. Systems employ levitation chambers of rectangular and cylindrical geometries. Reports first describe single mode concept and indicate which modes used to levitate sample without rotation. Reports then describe systems in which controlled rotation of sample introduced.

Barmatz, M. B.

Acoustic Translation of an Acoustically Levitated Sample

Acoustic-levitation apparatus uses only one acoustic mode to move sample from one region of chamber to another. Sample heated and cooled quickly by translation between hot and cold regions of levitation chamber. Levitated sample is raised into furnace region by raising plunger. Frequency of sound produced by transducers adjusted by feedback system to maintain (102) resonant mode, which levitates sample midway between transducers and plunger regardless of plunger position.

Barmatz, M. B.

Gravity enhanced acoustic levitation method and apparatus

An acoustic levitation system is provided for acoustically levitating an object by applying a single frequency from a transducer into a resonant chamber surrounding the object. The chamber includes a stabilizer location along its height, where the side walls of the chamber are angled so they converge in an upward direction. When an acoustic standing wave pattern is applied between the top and bottom of the chamber, a levitation surface within the stabilizer does not lie on a horizontal plane, but instead is curved with a lowermost portion near the vertical axis of the chamber. As a result, an acoustically levitated object is urged by gravity towards the lowermost location on the levitation surface, so the object is kept away from the side walls of the chamber.

Barmatz, M. B.

Off-Resonance Acoustic Levitation Without Rotation

Orthogonal acoustic-levitation modes excited at slightly different frequencies to control rotation. Rotation of object in square cross-section acoustic-levitation chamber stopped by detuning two orthogonal (x and y) excitation drivers in plane of square cross section. Detuning done using fundamental degenerate modes or odd harmonic modes.

Barmatz, M. B.

MAST space research flight experiment

The MAST flight experiments comprise a research program focusing on major LSS issues for which it is deemed necessary to test, measure, and validate techniques and concepts in the space environment. The MAST Shuttle attached test articles are transported to space by the STEP experiment carrier and are compatible with STEP interfaces in all configurations. As the experiments require no particular orbit and the operational timeliness needed for mission performance are not extensive, it is forseen that the STEP/MAST combination could provide an attractive repetitive element within the Shuttle mixed cargo manifesting process. Using the STEP experiment carrier and a retractable reusable test article allows repetitive flight research to the extent that the STEP is able to be manifested on a regular basis. Since this research program examines generic phenomena, maximum emphasis is placed upon information quality and the fidelity with which the phenomena model emulates the LSS issue.

Allen, J. L.

Experimental investigation of the scattering effects of a sphere in a cylindrical resonant chamber

Resonance frequency, acoustic pressure, and quality factor measurements for transverse and longitudinal modes of a cylindrical chamber are presented as a function of the position of a sphere along the chamber axis. The tests were performed over a wide range of sample-to-chamber ratios, and formulations were devised of the resonance frequency shift as a function of the components of the volume ratios. Departures from linearity were explored for intermediate ratios. The results are considered significant for acoustic levitation operations in space, where the acoustic radiation may alter the acoustic properties of the chamber.

Barmatz, M.

Preliminary study of VTO thrust requirements for a V/STOL aircraft with lift plus lift/cruise propulsion

A preliminary assessment was made of the VTO thrust requirements for a supersonic (Type B) aircraft with a Lift plus Lift/Cruise propulsion system. A baseline aircraft with a takeoff gross weight (TOGW) of 13 608 kg (30,000 lb) was assumed. Pitch, roll, and yaw control thrusts (i.e., the thrusts needed for aircraft attitude control in the flight hover mode) were estimated based on a specified set of maneuver acceleration requirements for V/STOL aircraft. Other effects (such as installation losses, suckdown, reingestion, etc.), which add to the thrust requirements for VTO were also estimated. For the baseline aircraft, the excess thrust required for attitude control of the aircraft during VTO and flight hover was estimated to range from 36.9 to 50.9 percent of the TOGW. It was concluded that the total thrust requirements for the aircraft/propulsion system are large and significant. In order to achieve the performance expected of this aircraft/propulsion system, reductions must be made in the excess thrust requirements.

Turney, G. E.

Preliminary study of propulsion systems and airplane wing parameters for a US Navy subsonic V/STOL aircraft

Two V/STOL propulsion concepts were evaluated in a common aircraft configuration. One propulsion system consists of cross coupled turboshaft engines driving variable pitch fans. The other system is a gas coupled combination of turbojet gas generators and tip turbine fixed pitch fans. Evaluations were made of endurance at low altitude, low speed loiter with equal takeoff fuel loads. Effects of propulsion system sizing, bypass ratio, and aircraft wing planform parameters were investigated and compared. Shaft driven propulsion systems appear to result in better overall performance, although at higher installed weight, than gas systems.

Zola, C. L.

Upper-stage space shuttle propulsion by means of separate scramjet and rocket engines

A preliminary mission study of a reusable vehicle from staging to orbit indicates payload advantages for a dual-propulsion system consisting of separate scramjet and rocket engines. In the analysis the scramjet operated continuously and the initiation of rocket operation was varied. For a stage weight of 500,000 lb the payload was 10.4 percent of stage weight or 70 percent greater than that of a comparable all-rocket-powered stage. When compared with a reusable two-state rocket vehicle having 50,000 lb payload, the use of the dual propulsion system for the second stage resulted in significant decreases in lift-off weight and empty weight, indicating possible lower hardware costs.

Franciscus, L. C.