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DOE OSTI2016

FY16 ISCP Nuclear Counting Facility Hardware Expansion Summary

Hardware expansion and detector calibrations were the focus of FY 16 ISCP efforts in the Nuclear Counting Facility. Work focused on four main objectives: 1) Installation, calibration, and validation of 4 additional HPGe gamma spectrometry systems; including two Low Energy Photon Spectrometers (LEPS). 2) Re-Calibration and validation of 3 previously installed gamma-ray detectors, 3) Integration of the new systems into the NCF IT infrastructure, and 4) QA/QC and maintenance of current detector systems.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2011

Integrated Data Collection Analysis (IDCA) Program - Mixing Procedures and Materials Compatibility

Three mixing procedures have been standardized for the IDCA proficiency test—solid-solid, solid-liquid, and liquid-liquid. Due to the variety of precursors used in formulating the materials for the test, these three mixing methods have been designed to address all combinations of materials. Hand mixing is recommended for quantities less than 10 grams and Jar Mill mixing is recommended for quantities over 10 grams. Consideration must also be given to the type of container used for the mixing due to the wide range of chemical reactivity of the precursors and mixtures. Eight web site sources from container and chemical manufacturers have been consulted. Compatible materials have been compiled as a resource for selecting containers made of materials stable to the mixtures. In addition, container materials used in practice by the participating laboratories are discussed. Consulting chemical compatibility tables is highly recommended for each operation by each individual engaged in testing the materials in this proficiency test.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗