Integrated Data Collection Analysis (IDCA) Program - Mixing Procedures and Materials Compatibility

Olinger, Becky D.; Sandstrom, Mary M.; Warner, Kirstin F.; Sorensen, Daniel N.; Remmers, Daniel L.; Moran, Jesse S.; Shelley, Timothy J.; Whinnery, LeRoy L.; Hsu, Peter C.; Whipple, Richard E.; Kashgarian, Michaele; Reynolds, John G.

doi:10.2172/1305877

DOE OSTI · 1305877

Integrated Data Collection Analysis (IDCA) Program - Mixing Procedures and Materials Compatibility

Olinger, Becky D.·Sandstrom, Mary M.·Warner, Kirstin F.·Sorensen, Daniel N.·Remmers, Daniel L.·Moran, Jesse S.·Shelley, Timothy J.·Whinnery, LeRoy L.·Hsu, Peter C.·Whipple, Richard E.·Kashgarian, Michaele·Reynolds, John G.

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Abstract

Three mixing procedures have been standardized for the IDCA proficiency test—solid-solid, solid-liquid, and liquid-liquid. Due to the variety of precursors used in formulating the materials for the test, these three mixing methods have been designed to address all combinations of materials. Hand mixing is recommended for quantities less than 10 grams and Jar Mill mixing is recommended for quantities over 10 grams. Consideration must also be given to the type of container used for the mixing due to the wide range of chemical reactivity of the precursors and mixtures. Eight web site sources from container and chemical manufacturers have been consulted. Compatible materials have been compiled as a resource for selecting containers made of materials stable to the mixtures. In addition, container materials used in practice by the participating laboratories are discussed. Consulting chemical compatibility tables is highly recommended for each operation by each individual engaged in testing the materials in this proficiency test.

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37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY HME materials compatibility mixing methods proficiency test round-robin test safety-testing protocols small-scale safety testing

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Olinger, Becky D., Sandstrom, Mary M., Warner, Kirstin F., Sorensen, Daniel N., Remmers, Daniel L., Moran, Jesse S., Shelley, Timothy J., Whinnery, LeRoy L., Hsu, Peter C., Whipple, Richard E., Kashgarian, Michaele, Reynolds, John G.. 2011-01-14. Integrated Data Collection Analysis (IDCA) Program - Mixing Procedures and Materials Compatibility. https://doi.org/10.2172/1305877

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