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DOE OSTI · 1305869

Integrated Data Collection Analysis (IDCA) Program - SSST Testing Methods

Sandstrom, Mary M.·Brown, Geoffrey W.·Preston, Daniel N.·Pollard, Colin J.·Warner, Kirstin F.·Remmers, Daniel L.·Sorensen, Daniel N.·Whinnery, LeRoy L.·Phillips, Jason J.·Shelley, Timothy J.·Reyes, Jose A.·Hsu, Peter C.·Reynolds, John G.
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Abstract

The Integrated Data Collection Analysis (IDCA) program is conducting a proficiency study for Small- Scale Safety and Thermal (SSST) testing of homemade explosives (HMEs). Described here are the methods used for impact, friction, electrostatic discharge, and differential scanning calorimetry analysis during the IDCA program. These methods changed throughout the Proficiency Test and the reasons for these changes are documented in this report. The most significant modifications in standard testing methods are: 1) including one specified sandpaper in impact testing among all the participants, 2) diversifying liquid test methods for selected participants, and 3) including sealed sample holders for thermal testing by at least one participant. This effort, funded by the Department of Homeland Security (DHS), is putting the issues of safe handling of these materials in perspective with standard military explosives. The study is adding SSST testing results for a broad suite of different HMEs to the literature. Ultimately the study will suggest new guidelines and methods and possibly establish the SSST testing accuracies needed to develop safe handling practices for HMEs. Each participating testing laboratory uses identical test materials and preparation methods wherever possible. The testing performers involved are Lawrence Livermore National Laboratory (LLNL), Los Alamos National Laboratory (LANL), Indian Head Division, Naval Surface Warfare Center, (NSWC IHD), Sandia National Laboratories (SNL), and Air Force Research Laboratory (AFRL/RXQL). These tests are conducted as a proficiency study in order to establish some consistency in test protocols, procedures, and experiments and to compare results when these testing variables cannot be made consistent.

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37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRYcarbondodecanefriction-HMEimpact-PETNpotassium chloratepotassium perchlorateproficiency testproficiency test methodsRDXround-robin testsafety testing protocolssmall-scale safety testingsodium chloratespark discharge-sugarthermal testing

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Sandstrom, Mary M., Brown, Geoffrey W., Preston, Daniel N., Pollard, Colin J., Warner, Kirstin F., Remmers, Daniel L., Sorensen, Daniel N., Whinnery, LeRoy L., Phillips, Jason J., Shelley, Timothy J., Reyes, Jose A., Hsu, Peter C., Reynolds, John G.. 2013-03-25. Integrated Data Collection Analysis (IDCA) Program - SSST Testing Methods. https://doi.org/10.2172/1305869

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