Integrated Data Collection Analysis (IDCA) Program - NaClO 3 /Icing Sugar

Sandstrom, Mary M.; Brown, Geoffrey W.; Preston, Daniel N.; Pollard, Colin J.; Warner, Kirstin F.; Sorensen, Daniel N.; Remmers, Daniel L.; Shelley, Timothy J.; Reyes, Jose A.; Hsu, Peter C.; Reynolds, John G.

doi:10.2172/1305885

DOE OSTI · 1305885

Integrated Data Collection Analysis (IDCA) Program - NaClO 3 /Icing Sugar

Sandstrom, Mary M.·Brown, Geoffrey W.·Preston, Daniel N.·Pollard, Colin J.·Warner, Kirstin F.·Sorensen, Daniel N.·Remmers, Daniel L.·Shelley, Timothy J.·Reyes, Jose A.·Hsu, Peter C.·Reynolds, John G.

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Abstract

The Integrated Data Collection Analysis (IDCA) program is conducting a proficiency study for Small- Scale Safety and Thermal (SSST) testing of homemade explosives (HMEs). Described here are the results for impact, friction, electrostatic discharge, and differential scanning calorimetry analysis of a mixture of NaClO 3 and icing sugar—NaClO 3 /icing sugar mixture. The mixture was found to: be more sensitive than RDX but less sensitive than PETN in impact testing (180-grit sandpaper); be more sensitive than RDX and about the same sensitivity as PETN in BAM fiction testing; be less sensitive than RDX and PETN except for one participant found the mixture more sensitive than PETN in ABL ESD testing; and to have one to three exothermic features with the lowest temperature event occurring at ~ 160°C always observed in thermal testing. Variations in testing parameters also affected the sensitivity.

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37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY carbon dodecane friction HME impact-PETN potassium chlorate potassium perchlorate proficiency test RDX round-robin test safety testing protocols small-scale safety testing sodium chlorate spark discharge-sugar thermal testing

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Sandstrom, Mary M., Brown, Geoffrey W., Preston, Daniel N., Pollard, Colin J., Warner, Kirstin F., Sorensen, Daniel N., Remmers, Daniel L., Shelley, Timothy J., Reyes, Jose A., Hsu, Peter C., Reynolds, John G.. 2013-02-11. Integrated Data Collection Analysis (IDCA) Program - NaClO 3 /Icing Sugar. https://doi.org/10.2172/1305885

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