DOE OSTI · 3385031
Influence of microstructure and temperature on impact toughness of H13 steel produced by binder jet additive manufacturing
Abstract
Binder Jet Additive Manufacturing (BJAM) is a promising manufacturing pathway to produce H13 steel dies and tooling with complex geometries for applications in high pressure aluminum die casting, hot stamping, and injection molding. While fully dense H13 coupons produced using BJAM have been subjected to detailed microstructure characterization, properties which are critical and relevant to the aforementioned applications, such as impact toughness, have not been reported. Here, this work evaluated the influence of microstructural characteristics and test temperature on the impact toughness of H13 produced by BJAM. Coupons were produced from three different powder size distributions (PSDs), with nominal powder size ranges of −22 μm, 10-32 μm, and 15-53 μm. Coupons were printed, sintered, hot isostatically pressed (HIPed), and heat treated by quenching and tempering. After HIPing, the measured porosities of the different PSDs were all less than 0.015 vol%. The −22 μm PSD BJAM material exhibited the best impact toughness of all three PSDs across the entire test temperature range from 25 to 400 °C, and also exhibited an ambient temperature impact toughness of 10.9 J at a hardness of 46 HRC, equivalent to minimum threshold requirements for premium grade H13. However, all three BJAM PSDs exhibited moderately lower impact toughness than premium grade wrought H13 from RT to 400 °C. We attribute this in part due to the very large prior-austenite grain (PAG) sizes near 400 μm and segregation from former liquid channels leading to greater amounts of carbide precipitation on PAG boundaries. Technical pathways for optimizing processing and chemistry of BJAM H13 to further improve impact toughness are discussed.
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Pierce, Dean T. [Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)] (ORCID:0000000304223423), Nayir, Selda [Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)] (ORCID:0000000324578467), Sebeck, Katherine [US Army Combat Capabilities Development Command Ground Vehicle Systems Center, Warren, MI (United States)], Guajardo, Anthony [Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)], Poplawsky, Jonathan D. [US Army Combat Capabilities Development Command Ground Vehicle Systems Center, Warren, MI (United States)] (ORCID:0000000242727043), Cakmak, Ercan [Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)] (ORCID:0000000172724815), Kannan, Rangasayee [Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)] (ORCID:0000000257925739), Haynes, James A. [Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)] (ORCID:0000000242367383), Boebinger, Matthew [Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States). Center for Nanophase Materials Sciences (CNMS)] (ORCID:0000000196222043), Ludkey, Matt [US Army Combat Capabilities Development Command Ground Vehicle Systems Center, Warren, MI (United States)], Nandwana, Peeyush [Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)] (ORCID:0000000251471668). 2026-10-01. Influence of microstructure and temperature on impact toughness of H13 steel produced by binder jet additive manufacturing. https://doi.org/10.1016/j.msea.2026.150598
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