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At least 235 records · Page 13

LSP Composite Susbtrate Destructive Evaluation Test Assessment Manual

This document specifies the processes to perform post-strike destructive damage evaluation of tested CFRP panels.It is recognized that many factors besides lightning damage protection are involved in the selection of an appropriate Lightning Strike Protection (LSP) for a particular system (e.g., cost, weight, corrosion resistance, shielding effectiveness, etc.). This document strives primarily to address the standardized generation of damage protection performance data.

Kovach, Daniel J.↗

Single-Event Effect Report for EPC Series eGaN FETs: Comparison of EPC1000 and EPC2000 Series Devices for Destructive SEE

Recent testing of the EPC1000 series eGaN FETs has shown sensitivity to Single Event Effects (SEE) that are destructive. These effects are most likely the failure of the very thin gate structure in HEMT architecture. EPC has recently changed the doping of the substrate to improve the performance and the SEE response. This testing compares the SEE response of both devices.

Scheick, Leif↗

Comprehensive Non-Destructive Conservation Documentation of Lunar Samples Using High-Resolution Image-Based 3D Reconstructions and X-Ray CT Data

Established contemporary conservation methods within the fields of Natural and Cultural Heritage encourage an interdisciplinary approach to preservation of heritage material (both tangible and intangible) that holds "Outstanding Universal Value" for our global community. NASA's lunar samples were acquired from the moon for the primary purpose of intensive scientific investigation. These samples, however, also invoke cultural significance, as evidenced by the millions of people per year that visit lunar displays in museums and heritage centers around the world. Being both scientifically and culturally significant, the lunar samples require a unique conservation approach. Government mandate dictates that NASA's Astromaterials Acquisition and Curation Office develop and maintain protocols for "documentation, preservation, preparation and distribution of samples for research, education and public outreach" for both current and future collections of astromaterials. Documentation, considered the first stage within the conservation methodology, has evolved many new techniques since curation protocols for the lunar samples were first implemented, and the development of new documentation strategies for current and future astromaterials is beneficial to keeping curation protocols up to date. We have developed and tested a comprehensive non-destructive documentation technique using high-resolution image-based 3D reconstruction and X-ray CT (XCT) data in order to create interactive 3D models of lunar samples that would ultimately be served to both researchers and the public. These data enhance preliminary scientific investigations including targeted sample requests, and also provide a new visual platform for the public to experience and interact with the lunar samples. We intend to serve these data as they are acquired on NASA's Astromaterials Acquisistion and Curation website at http://curator.jsc.nasa.gov/. Providing 3D interior and exterior documentation of astromaterial samples addresses the increasing demands for accessability to data and contemporary techniques for documentation, which can be realized for both current collections as well as future sample return missions.

Blumenfeld, E. H.↗

Non-destructive Evaluation of Bonds Between Fiberglass Composite and Metal

To assess the integrity and reliability of an adhesive joint in an automotive composite component, several non-destructive evaluation (NDE) methodologies are correlated to lap shear bond strengths. A glass-fabric-reinforced composite structure was bonded to a metallic structure with a two-part epoxy adhesive. Samples were subsequently cut and tested in shear, and flaws were found in some areas. This study aims to develop a reliable and portable NDE system for service-level adhesive inspection in the automotive industry. The results of the experimental investigation using several NDE methods are presented and discussed. Fiberglass-to-metal bonding is the ideal configuration for NDE via thermography using excitation with induction heating, due to the conductive metal and non-conductive glass-fiber-reinforced composites. Excitation can be either by a research-grade induction heater of highly defined frequency and intensity, or by a service-level heater, such as would be used for sealing windshields in a body shop. The thermographs thus produced can be captured via a high-resolution infrared camera, with principal component analysis and 2D spatial Laplacian processing. Alternatively, the thermographs can be captured by low resolution thermochromic microencapsulated liquid crystal film imaging, which needs no post-processing and can be very inexpensive. These samples were also examined with phased-array ultrasound. The NDE methods are compared to the lap shear values and to each other for approximate cost, accuracy, and time and level of expertise needed.

Zhao, Selina↗

Nitrous Oxides Ozone Destructiveness Under Different Climate Scenarios

Nitrous oxide (N2O) is an important greenhouse gas and ozone depleting substance as well as a key component of the nitrogen cascade. While emissions scenarios indicating the range of N2O's potential future contributions to radiative forcing are widely available, the impact of these emissions scenarios on future stratospheric ozone depletion is less clear. This is because N2O's ozone destructiveness is partially dependent on tropospheric warming, which affects ozone depletion rates in the stratosphere. Consequently, in order to understand the possible range of stratospheric ozone depletion that N2O could cause over the 21st century, it is important to decouple the greenhouse gas emissions scenarios and compare different emissions trajectories for individual substances (e.g. business-as-usual carbon dioxide (CO2) emissions versus low emissions of N2O). This study is the first to follow such an approach, running a series of experiments using the NASA Goddard Institute for Space Sciences ModelE2 atmospheric sub-model. We anticipate our results to show that stratospheric ozone depletion will be highest in a scenario where CO2 emissions reductions are prioritized over N2O reductions, as this would constrain ozone recovery while doing little to limit stratospheric NOx levels (the breakdown product of N2O that destroys stratospheric ozone). This could not only delay the recovery of the stratospheric ozone layer, but might also prevent a return to pre-1980 global average ozone concentrations, a key goal of the international ozone regime. Accordingly, we think this will highlight the importance of reducing emissions of all major greenhouse gas emissions, including N2O, and not just a singular policy focus on CO2.

stratospheric ozone depletion↗

Structure from Motion Photogrammetry and Micro X-Ray Computed Tomography 3-D Reconstruction Data Fusion for Non-Destructive Conservation Documentation of Lunar Samples

Our team is developing a modern, cross-disciplinary approach to documentation and preservation of astromaterials, specifically lunar and meteorite samples stored at the Johnson Space Center (JSC) Lunar Sample Laboratory Facility. Apollo Lunar Sample 60639, collected as part of rake sample 60610 during the 3rd Extra-Vehicular Activity of the Apollo 16 mission in 1972, served as the first NASA-preserved lunar sample to be examined by our team in the development of a novel approach to internal and external sample visualization. Apollo Sample 60639 is classified as a breccia with a glass-coated side and pristine mare basalt and anorthosite clasts. The aim was to accurately register a 3-dimensional Micro X-Ray Computed Tomography (XCT)-derived internal composition data set and a Structure-From-Motion (SFM) Photogrammetry-derived high-fidelity, textured external polygonal model of Apollo Sample 60639. The developed process provided the means for accurate, comprehensive, non-destructive visualization of NASA's heritage lunar samples. The data products, to be ultimately served via an end-user web interface, will allow researchers and the public to interact with the unique heritage samples, providing a platform to "slice through" a photo-realistic rendering of a sample to analyze both its external visual and internal composition simultaneously.

Beaulieu, K. R.↗

Computational Non-Destructive Evaluation Improving Ultrasonic Interrogation of Complex Geometry Composite Parts

Finite element simulation was employed in modeling the ultrasound (UT) pressure pulse propagation through a coupled liquid-composite medium to reproduce experimental data. From the simulation point of view, the proposed approach is challenging when there is a large simulation domain. For example, it is shown that a sub-micron wavelength of an ultrasonic wave requires a mesh size of several microns and this in turn requires significant computational resources, as well as special care in modeling. Some of the simulation results are presented considering that such modeling should reproduce experimental data for a healthy and faulty composite structure with complex geometry. Many possible experimental setups are simulated to demonstrate the non-destructive testing technique. This setup includes the generation of pressure pulse propagating through the tested composite plate and possible scattering by discontinuities (area of different impedance) that may be present in the panel. This scattered pulse together with the baseline pressure pulse generates a signature on the probe element which can be used to locate the position of defects in the structures.

modeling↗

Documentation of Destructive Analyses on Thin Sections in the US Antarctic Meteorite Collection

Detailed studies and analytical measurements are commonly made using thin sections of rocks affixed with epoxy to a slide. Thin sections [1,2] are a convenient medium in which to study rocks and meteorites, and fit into sample holders compatible with many instruments. Thin sections can also be used multiple times by different researchers, and many meteorite thin sections from the US Antarctic meteorite collection, have been utilized by 5 to 6 researchers over their 40 year lifetime. Thin sections are thus a scientifically valuable resource that must be preserved, documented and conserved over time. Analytical capabilities for meteorite and other sample studies have progressed extensively in the last 20 years, including many different kinds of analysis of high spatial resolution on thin sections. The progression to analysis on small samples has provided new and efficient ways to characterize samples while also preserving more material for future generations to study. While the development of analytical tools has expanded, many of these analyses are destructive in the sense that small pits or holes or other effects of the analysis are created on the thin sections. Preserving material for future generations thus requires recording the effects of multiple analyses on thin sections. Here we describe the process used for documenting the effects of various analyses on thin sections in the US Antarctic meteorite collection.

thin section↗

Functionalized surfaces for the destruction of pathogens and organics

The disclosure is directed to a surface having a binding component applied thereto for the adsorption or capture of pathogens and organic molecules or materials. The surface may be a component of a porous or nonporous substrate. The binding component may also bind a photocatalyst to the surface for photocatalytic destruction of the captured pathogens and organic molecules or materials.

36 MATERIALS SCIENCE↗

Utility Energy Service Contract Boosts Chemical Weapons Destruction Mission at Army Pueblo Chemical Depot

For six decades, the U.S. Army has safely and securely stored chemical munitions at the Pueblo Chemical Depot in Colorado. To help fulfill international treaty obligations and to meet a congressional deadline of 2023 for the elimination of these aging weapons, initial destruction of the Pueblo chemical weapons stockpile began in 2015. A utility energy service contract (UESC) executed in 2016 between the U.S. Army Corps of Engineers and the Depot’s serving utility, Black Hills Energy (BHE), directly supported this mission with the installation of a new electrical substation that was essential to the Depot’s need for uninterrupted power.

Army Pueblo Chemical Depot↗

Fabrication of thin-film electronic devices with non-destructive wafer reuse

Thin-film electronic devices such as LED devices and field effect transistor devices are fabricated using a non-destructive epitaxial lift-off technique that allows indefinite reuse of a growth substrate. The method includes providing an epitaxial protective layer on the growth substrate and a sacrificial release layer between the protective layer and an active device layer. After the device layer is released from the growth substrate, the protective layer is selectively etched to provide a newly exposed surface suitable for epitaxial growth of another device layer. The entire thickness of the growth substrate is preserved, enabling continued reuse. Inorganic thin-film device layers can be transferred to a flexible secondary substrate, enabling formation of curved inorganic optoelectronic devices.

Forrest, Stephen R.↗

Prioritizing Countries by Concern Regarding Access to Weapons of Mass Destruction Materials

This article presents a global prioritization methodology that evaluates the relative risks of non-state actor acquisition of materials that could be used in chemical, biological, radiological, nuclear and high explosive Weapons of Mass Destruction (WMD) from the country’s relevant infrastructure. Prioritization is based on three domains: 1. Assessing relative scale of materials in each country, 2. The country’s corresponding security posture, and 3. The presence of threat actors. The output is a list of countries prioritized from greatest risk to least. Rather than providing an overall 1 to N ranking, however, the results are placed into tiers based upon their natural groupings within the three domains. The countries in the highest tiers are flagged as potential US national security concern; those scoring in the middle and at the bottom are flagged as posing lower US national security concern. A systematic approach assesses each country by leveraging many disciplines, such as risk and decision analysis, as well as expert judgement. A quantitative value model based on Multi-Attribute Value Theory (MAVT) organizes the objectives scoring criteria into a value tree using lessons learned from previous studies, published literature, and expert judgement. The article presents the prioritization categories and corresponding value model scoring criteria to include measurement type, weight, range, and value preference. Country names and data are notional in order to share the details on the underlying methodology and model without identification of actual security risks. A deliberative process addresses factors external to the model and scrutinizes inputs, methodology, model, and results.

98 NUCLEAR DISARMAMENT, SAFEGUARDS, AND PHYSICAL P↗

In-process, layer-by-layer non-destructive testing of additive manufactured components using linear and nonlinear vibrational resonance

Provided is an additive manufacturing system capable of performing in-process, layer-by-layer non-destructive testing, the additive manufacturing system including: a plate for producing a part thereon; a transducer attached to the plate and configured to induce vibrations in the part; and a laser vibrometer configured to detect a vibrational response of the part to determine whether defect and/or anisotropy exists within the part.

Remillieux, Marcel↗

Improvement of Quantification in Non-Destructive Characterization of Radioactive Waste Packages -Introduction to the Ideas of a Currently Started Project - 20197

For the characterization of radioactive waste packages (e.g. 200-L drums) with inhomogeneous activity and density distributions preferably non-destructive methods like segmented gamma scanning and transmission measurements are applied. While the first is used for identification of the radioactive inventory, both are necessary for a reliable activity quantification. Although at nuclear facilities, segmented gamma scanner are state-of-the-art and are mostly equipped with a vertically moveable transmission source the combining of this data and further a-priori information improving accuracy in data estimation giving realistic, reliable and traceable uncertainty estimations are improvable. This challenge is tackled by a R and D project funded by the German Federal Ministry of Education and Research (BMBF). The boundary conditions for this project are (i) taking into account the typical instrumentation available at nuclear facilities, (ii) minimize the overall measurement time and (iii) combining data from emission and transmission measurements by Bayesian methods. For the R and D project, being still in its initial stage, the basic ideas, the data used for evaluation and the result of a preliminary investigation demonstrating the proof of principle are presented. Additionally, some first aspects on spatial resolution in emission and transmission measurements are addressed. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Implementation of the Glycolate Destruction Process with Sodium Permanganate in the Defense Waste Processing Facility (DWPF) - 20141

The Savannah River Site (SRS) seeks to replace formic acid with glycolic acid as a chemical reductant in the Defense Waste Processing Facility (DWPF), where borosilicate glass is mixed with high-level radioactive waste, melted at high temperatures, then poured into stainless steel canisters for safe storage. Prior research and development have demonstrated the feasibility and advantages of the new nitric-glycolic acid flowsheet over the current nitric-formic acid flowsheet to chemically adjust the radioactive sludge slurry waste in the Sludge Receipt and Adjustment Tank (SRAT) prior to vitrification. Use of glycolic acid reduces hydrogen and ammonia generation during the reduction process, thus reducing flammability hazards and purge requirements in the DWPF processing vessels. In addition, glycolic acid will support the new Salt Waste Processing Facility (SWPF) by allowing for receipt of higher volumes of waste due to reduction of flammable gases, increased boil-up rates in the vessels, and easing the processing of future sludge batches containing high levels of mercury. However, during DWPF operations, trace amounts of glycolate are anticipated to be entrained in the recycle stream and sent to the Concentration, Storage, and Transfer Facilities (CSTF) via the Recycle Collection Tank (RCT). The RCT receives condensate from the Slurry Mix Evaporator Condensate Tank (SMECT) and Off-gas Condensate Tank (OGCT) that may contain unreacted glycolate. A literature review found the potential for hydrogen generation due to thermolysis of glycolate in caustic CSTF conditions. Savannah River National Laboratory (SRNL) conducted several tests on simulant and radioactive waste from various tanks at SRS and confirmed that glycolate added to waste at concentrations of approximately 1000 mg/L and higher generates hydrogen through thermolysis. There are potential operating scenarios in the future where glycolate concentration could exceed 1000 mg/L in the 2H Evaporator Drop Tank, the highest accumulation point for DWPF organics received via recycle. These findings presented a need to develop another process to mitigate the impact of glycolic acid to the CSTF. Several DWPF compatible options were evaluated for their ability to destroy glycolate in the DWPF recycle stream under various processing conditions, thereby mitigating its introduction to the CSTF. Downselection testing identified sodium permanganate as the most promising and simplest option to oxidize glycolate. It has been demonstrated to be effective in various RCT simulant compositions, operating temperatures, oxidant addition rates, solution pH, and initial glycolate concentrations. A feasibility study identified existing tanks within the facility that could be used for receiving and storing the commercially available sodium permanganate, as well as feeding it to the RCT for processing. The use of existing equipment as well as the ability to purchase the pre-mixed chemical reduces implementation and operational complexity. The downstream impacts of the sodium permanganate reaction were also evaluated and demonstrated to have minimal impact on other chemical species present in the RCT and CSTF, as well as on the materials of construction of the RCT and CSTF vessels and associated piping and instrumentation. Future work is in progress to validate the glycolate destruction process with testing in actual radioactive RCT waste before implementation in DWPF. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗