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At least 235 records · Page 13

A Data-Driven Framework for Direct Local Tensile Property Prediction of Laser Powder Bed Fusion Parts

This article proposes a generalizable, data-driven framework for qualifying laser powder bed fusion additively manufactured parts using part-specific in situ data, including powder bed imaging, machine health sensors, and laser scan paths. To achieve part qualification without relying solely on statistical processes or feedstock control, a sequence of machine learning models was trained on 6299 tensile specimens to locally predict the tensile properties of stainless-steel parts based on fused multi-modal in situ sensor data and a priori information. A cyberphysical infrastructure enabled the robust spatial tracking of individual specimens, and computer vision techniques registered the ground truth tensile measurements to the in situ data. The co-registered 230 GB dataset used in this work has been publicly released and is available as a set of HDF5 files. The extensive training data requirements and wide range of size scales were addressed by combining deep learning, machine learning, and feature engineering algorithms in a relay. The trained models demonstrated a 61% error reduction in ultimate tensile strength predictions relative to estimates made without any in situ information. Lessons learned and potential improvements to the sensors and mechanical testing procedure are discussed.

36 MATERIALS SCIENCE↗

3D Printing of High Viscosity Reinforced Silicone Elastomers

Recent advances in additive manufacturing, specifically direct ink writing (DIW) and ink-jetting, have enabled the production of elastomeric silicone parts with deterministic control over the structure, shape, and mechanical properties. These new technologies offer rapid prototyping advantages and find applications in various fields, including biomedical devices, prosthetics, metamaterials, and soft robotics. Stereolithography (SLA) is a complementary approach with the ability to print with finer features and potentially higher throughput. However, all high-performance silicone elastomers are composites of polysiloxane networks reinforced with particulate filler, and consequently, silicone resins tend to have high viscosities (gel- or paste-like), which complicates or completely inhibits the layer-by-layer recoating process central to most SLA technologies. Herein, the design and build of a digital light projection SLA printer suitable for handling high-viscosity resins is demonstrated. Further, a series of UV-curable silicone resins with thiol-ene crosslinking and reinforced by a combination of fumed silica and MQ resins are also described. The resulting silicone elastomers are shown to have tunable mechanical properties, with 100–350% elongation and ultimate tensile strength from 1 to 2.5 MPa. Three-dimensional printed features of 0.4 mm were achieved, and complexity is demonstrated by octet-truss lattices that display negative stiffness.

36 MATERIALS SCIENCE↗

Application of powder metallurgy to an advanced-temperature nickel-base alloy, NASA-TRW 6-A

Bar stock of the NASA-TRW 6-A alloy was made by prealloyed powder techniques and its properties evaluated over a range of temperatures. Room temperature ultimate tensile strength was 1894 MN/sq m (274 500 psi). The as-extruded powder product showed substantial improvements in strength over the cast alloy up to 649 C (1200 F) and superplasticity at 1093 C (2000 F). Both conventional and autoclave heat treatments were applied to the extruded powder product. The conventional heat treatment was effective in increasing rupture life at 649 and 704 C (1200 and 1300 F); the autoclave heat treatment, at 760 and 816 C (1400 and 1500 F).

Freche, J. C.↗

Evaluation of nondestructive tensile testing

The results of a series of experiments performed in the evaluation of nondestructive tensile testing of chip and wire bonds are presented. Semiconductor devices were subjected to time-temperature excursions, static-load life testing and multiple pre-stressing loads to determine the feasibility of a nondestructive tensile testing approach. The report emphasizes the importance of the breaking angle in determining the ultimate tensile strength of a wire bond, a factor not generally recognized nor implemented in such determinations.

Bowe, J. J.↗

Improvement of chemical vapor deposition process for production of large diameter carbon base monofilaments

Research was conducted to develop large diameter carbon monofilament, containing 25 to 35 mole % element boron, in the 2.0 to 10.0 mil diameter range using the chemical vapor deposition process. The objective of the program was to gain an understanding of the critical process variables and their effect on fiber properties. Synthesis equipment was modified to allow these variables to be studied. Improved control of synthesis variables permitted reduction in scatter of properties of the monofilaments. Monofilaments have been synthesized in the 3.0 to nearly 6.0 mil diameter range having measured values up to 552,000 psi for ultimate tensile strength and up to 30 million psi for elastic modulus.

Hough, R. L.↗

Directional solidification of eutectic composites in space environment

The Ni-Ni3Ta eutectic and a nickel-base alloy containing 30 wt pct Ta were solidified unidirectionally in an electron beam floating zone melting apparatus. It was found that the volume fraction of the Ni3Ta phase in the Ni-Ni3Ta eutectic mixture was increased from 7.6 to 36 volume pct in agreement with the theory as predicted. Tensile properties of the randomly solidified and unidirectionally solidified Ni-Ni3Ta eutectic were determined as function of solidification rate and temperature. It was found that the ultimate tensile strength decreased as both the test temperature and solidification rate increased. An elongation of 40 pct was obtained for a nickelbase alloy containing 30 wt at room temperature. This unusually large elongation was attributed to the superplastic behavior of the alloy. The critical currents versus the external fields at 2.5, 3.0, 3.5 and 4.2 deg for the unidirectionally solidified Pb-Sn eutectic were measured. The values of critical fields at zero critical currents were obtained by extrapolation.

Yue, A. S.↗

Tensile and fatigue data for irradiated and unirradiated AISI 310 stainless steel and titanium - 5 percent aluminum - 2.5 percent tin: Application of the method of universal slopes

Irradiated and unirradiated tensile and fatigue specimens of AISI 310 stainless steel and Ti-5Al-2.5Sn were tested in the range of 100 to 10,000 cycles to failure to determine the applicability of the method of universal slopes to irradiated materials. Tensile data for both materials showed a decrease in ductility and increase in ultimate tensile strength due to irradiation. Irradiation caused a maximum change in fatigue life of only 15 to 20 percent for both materials. The method of universal slopes predicted all the fatigue data for the 310 SS (irradiated as well as unirradiated) within a life factor of 2. For the titanium alloy, 95 percent of the data was predicted within a life factor of 3.

Debogdan, C. E.↗

Properties criteria for components and materials used in lightweight solar arrays

The present work describes the characteristics and design criteria for components and materials used in lightweight substrate solar arrays. This includes descriptions of wraparound-electrode solar cells, cell covers, and cell interconnects. Cell cover systems briefly discussed are fused silica, cerium stabilized glass, microsheet, FEP (tape, heat laminated, and spray on), and ESB 7070 glass integral covers. The majority of solar arrays orbited have used either silver, Kovar, copper, or molybdenum as interconnect metals. Data are presented comparing the Young's modulus E, ultimate tensile strength, coefficient of expansion, thermal conductivity, and percent elongation of these and other interconnect candidate materials. Guidelines for the use of end tab wraparound cells are listed.

Lott, D. R.↗

Hot hardness of nickel-rich nickel-chromium-aluminum alloys

Rockwell A hardness of cast nickel-chromium-aluminum (NiCrAl) alloys was examined from ambient to 1150 K and compared to cast NiAl and IN-100. Alloy constitution was either gamma, gamma prime + gamma or gamma + beta + alpha + gamma prime. Below 1000 K beta containing NiCrAl alloys have hardnesses comparable to IN-100; above 1000 K they soften faster than IN-100. At 1150 K the hardness of beta-containing NiCrAl alloys decreases with increasing beta-content. The beta-containing NiCrAl alloys were harder than beta-NiAl. The ultimate tensile strengths of the NiCrAl alloys were estimated. The effects of NiCrAl coatings on strength and fatigue life of cooled turbine components were deduced.

Levine, S. R.↗

A Directionally Solidified Iron-chromium-aluminum-tantalum Carbide Eutectic Alloy

A eutectic alloy, Fe-13.6CR-3.7Al+9TaC, was directionally solidified in a high gradient furnace, producing a microstructure of alined TaC fibers in an oxidation resistant alpha-iron matrix. Tensile and stress rupture properties, thermal cycling resistance, and microstructures were evaluated. The alloy displays at 1000 C an ultimate tensile strength of 58 MPa and a 100-hour rupture life at a stress of 21 MPa. Thermal cycling to 1100 C induces faceting in the TaC fibers.

Harf, F. H.↗

A study of the mechanisms of hydrogen embrittlement in molybdenum

The mechanical properties of polycrystalline molybdenum samples in both the 'as annealed' and hydrogenized conditions were studied. The results indicate that hydrogen does not alter the yield stress of samples significantly although it reduces both the ultimate tensile strength and the ductility considerably. Fractographic study of samples shows a tendency to intercrystalline cracking of the hydrogenised molybdenum at low temperatures. In the light of the results, a mechanism involving grain boundary weakening is suggested.

Taheri, M.↗

Evaluation of urethane for feasibility of use in wind turbine blade design

A preliminary evaluation was conducted of the use of cast urethane as a possible material for low-cost blades for wind turbines. Specimen test data are presented for ultimate tensile strength, elastic modulus, flexural strain, creep, and fatigue properties of a number of urethane formulations. Data are also included for a large-scale urethane blade section composed of cast symmetrical half-profiles tested as a cantilever beam. Based on these results, an analysis was conducted of a full-scale blade design of cast urethane that meets the design specifications of the rotor blades for the NASA/DOE experimental 100-kW MOD-0 wind turbine. Because of the low value of elastic modulus for urethane (around 457 000 psi), the design loads would have to be carried by metal reinforcement. Considerations for further evaluation are noted.

Lieblein, S.↗

Cryogenic container compound suspension strap

A support strap for use in a cryogenic storage vessel for supporting the inner shell from the outer shell with a minimum heat leak is presented. The compound suspension strap is made from a unidirectional fiberglass epoxy composite material with an ultimate tensile strength and fatigue strength which are approximately doubled when the material is cooled to a cryogenic temperature.

Vorreiter, J. W.↗

Room temperature mechanical properties of shuttle thermal protection system materials

Tests were conducted at room temperature to determine the mechanical properties and behavior of materials used for the thermal protection system of the space shuttle. The materials investigated include the LI-900 RSI tiles, the RTV-560 adhesive and the .41 cm (.16 thick) strain isolator pad (SIP). Tensile and compression cyclic loading tests were conducted on the SIP material and stress-strain curves obtained for various proof loads and load cyclic conditioning. Ultimate tensile and shear tests were conducted on the RSI, RTV, and SIP materials. The SIP material exhibits highly nonlinear stress-strain behavior, increased tangent modulus and ultimate tensile strength with increased loading rate, and large short time load relaxation and moderate creep behavior. Proof and cyclic load conditioning of the SIP results in permanent deformation of the material, hysteresis effects, and much higher tensile tangent modulus values at large strains.

Sawyer, J. W.↗

Interfacial reactions in borsic/Ti-3Al-2-1/2V composite

The paper provides a detailed X-ray characterization of a borsic/Ti-3Al-2-1/2V composite, and to correlate the relative intensities of the reaction products with the mechanical properties. Based on X-ray integrated intensity data two stages of interface reactions were identified: during the first stage there is a simultaneous interdiffusion of Si, C, and Ti atoms at the filament/matrix interface resulting in the formation of Ti5Si3, TiSi and small amounts of TiSi2 and TiC. The second stage is associated with considerable TiSi2 and boride formation. It appears that the alpha-phase of Ti is more reactive in forming silicides and borides than the beta-phase. The silicide intensities and the reaction zone thicknesses are shown to be directly related to the reduction of the ultimate tensile strength by thermal degradation, and the results indicate that silicide reaction products are as detrimental to strength as the borides.

Rao, V. B.↗

Degradation of tensile and shear properties of composites exposed to fire or high temperature

The decrease in ultimate tensile strength, shear strength, tensile modulus, and shear modulus of fiber reinforced composites exposed to fire or to high temperature was investigated. A simple model was developed for calculating the mass loss of the material and the thickness of the char layer. The mass loss as well as the degradation in tensile and shear properties of Fiberite T300/1034 and Hercules AS/3501-6 graphite epoxy composites exposed to fire were measured. A correlation between the degradation in properties and the calculated mass loss and the char layer thickness was developed. A technique was proposed for predicting material damage through the use of such correlations.

Pering, G. A.↗

Physical aging in graphite epoxy composites

The matrix dominated mechanical behavior of a graphite epoxy composite was found to be affected by sub Tg annealing. Postcured + or - 45 deg 4S specimens of Thornel 300 graphite/Narmco 5208 epoxy were quenched from above Tg and given a sub Tg annealing at 140 C for times up to 10 to the 5th power min. The ultimate tensile strength, strain to break, and toughness of the composite material were found to decrease as functions of sub Tg annealing time. No weight loss was observed during the sub Tg annealing. The time dependent change in mechanical behavior is explained on the basis of free volume changes that are related to the physical aging of the nonequilibrium glassy network epoxy. The results imply possible changes in composite properties with service time.

Kong, E. S. W.↗