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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 271 records · Page 15
All sourcesNASA NTRSDOE OSTI
NASA NTRS1993

Hot Hydrogen Testing of Refractory Metals and Ceramics

The objective of this investigation is to develop a technique with which refractory metal carbide samples can be exposed to hydrogen containing gases at high temperatures, and to use various microstructural and analytical techniques to determine the chemical and rate processes involved in hydrogen degradation in these materials. Five types of carbides were examined including WC, NbC, HfC, ZrC, and TaC. The ceramics were purchased and were all monolithic in nature. The temperature range investigated was from 850 to 1600 C with a hydrogen pressure of one atmosphere. Control experiments, in vacuum, were also conducted for comparison so that the net effects due to hydrogen could be isolated. The samples were analyzed prior to and after exposure. Gas samples were collected in selected experiments and analyzed using gas chromography. Characterization of the resulting microstructure after exposure to hydrogen was conducted using optical microscopy, x-ray diffraction, scanning electron microscopy, and weight change. The ceramics were purchased and were all monolithic in nature. It was found that all samples lost weight after exposure, both in hydrogen and vacuum. Results from the microstructure analyses show that the degradation processes are different among the five types of ceramics involved. In addition, the apparent activation energy for the degradation process is a function of temperature even within the same material. This indicates that there are more than one mechanism involved in each material, and that the mechanisms are temperature dependent.

Zee, Ralph↗
NASA NTRS2012

Surface, Water, and Air Biocharacterization (SWAB) Flight Experiment

The determination of risk from infectious disease during spaceflight missions is composed of several factors including both the concentration and characteristics of the microorganisms to which the crew are exposed. Thus, having a good understanding of the microbial ecology aboard spacecraft provides the necessary information to mitigate health risks to the crew. While preventive measures are taken to minimize the presence of pathogens on spacecraft, medically significant organisms have been isolated from both the Mir and International Space Station (ISS). Historically, the method for isolation and identification of microorganisms from spacecraft environmental samples depended upon their growth on culture media. Unfortunately, only a fraction of the organisms may grow on a specific culture medium, potentially omitting those microorganisms whose nutritional and physical requirements for growth are not met. To address this bias in our understanding of the ISS environment, the Surface, Water, and Air Biocharacterization (SWAB) Flight Experiment was designed to investigate and develop monitoring technology to provide better microbial characterization. For the SWAB flight experiment, we hypothesized that environmental analysis using non-culture-based technologies would reveal microorganisms, allergens, and microbial toxins not previously reported in spacecraft, allowing for a more complete health assessment. Key findings during this experiment included: a) Generally, advanced molecular techniques were able to reveal a few organisms not recovered using culture-based methods; however, there is no indication that current monitoring is "missing" any medically significant bacteria or fungi. b) Molecular techniques have tremendous potential for microbial monitoring, however, sample preparation and data analysis present challenges for spaceflight hardware. c) Analytical results indicate that some molecular techniques, such as denaturing gradient gel electrophoresis (DGGE), can be much less sensitive than culture-based methods. d) More sensitive molecular techniques, such as quantitative polymerase chain reaction (QPCR), were able to identify viral DNA from ISS environments, suggesting potential transfer of the organism between crewmembers. In addition, the hardware selected for this experiment represented advances for next-generation sample collection. The advanced nature of this collection hardware was noted, when the Sartorius MD8 Air Port air sampler from the SWAB experiment remained on board ISS at the request of JAXA investigators, who intend to use it in completion of their microbial ecology experiment.

Castro, V. A.↗
NASA NTRS1988

Some instrumentation requirement issues for the Space Station structural characterization experiment

The Space Station will provide unique opportunities to the research and technology community as a national in-space research facility. Opportunities will exist for technology experiments in a variety of disciplines, including dynamics and control of large space structures (LSS). The Space Station Structural Characterization Experiment (SSSCE) is an early space station technology experiment now under development. The objective of the experiment is to instrument and use the Space Station as a generic research test article, in support of research and technology activities in the areas of structural dynamics and control/structure interaction (CSI). Tests will be conducted, potentially, on each assembly flight configuration, as well as on the phase 1 configuration. Structural dynamic response data will be measured and transferred to the ground for analysis. These measurements will support the development and in-space verification of system identification and analytical modeling techniques for future LSS, including the evolutionary Space Station. The paper begins by restating the principal objective of SSSCE, along with the basic approach that will be used. The body of the paper deals with instrumentation requirement issues. The paper closes with several questions concerning modal-testing objectives and limitations, a brief review of a previous on-orbit experiment, the Solar Array Flight Experiment, and concluding remarks.

Pappa, Richard S.↗
NASA NTRS2004

Computational Simulation of Acoustic Modes in Rocket Combustors

A combination of computational fluid dynamic analysis and analytical solutions is being used to characterize the dominant modes in liquid rocket engines in conjunction with laboratory experiments. The analytical solutions are based on simplified geometries and flow conditions and are used for careful validation of the numerical formulation. The validated computational model is then extended to realistic geometries and flow conditions to test the effects of various parameters on chamber modes, to guide and interpret companion laboratory experiments in simplified combustors, and to scale the measurements to engine operating conditions. In turn, the experiments are used to validate and improve the model. The present paper gives an overview of the numerical and analytical techniques along with comparisons illustrating the accuracy of the computations as a function of grid resolution. A representative parametric study of the effect of combustor mean flow Mach number and combustor aspect ratio on the chamber modes is then presented for both transverse and longitudinal modes. The results show that higher mean flow Mach numbers drive the modes to lower frequencies. Estimates of transverse wave mechanics in a high aspect ratio combustor are then contrasted with longitudinal modes in a long and narrow combustor to provide understanding of potential experimental simulations.

Harper, Brent↗
NASA NTRS2012

Comparative Mineralogy, Microstructure and Compositional Trends in the Sub-Micron Size Fractions of Mare and Highland Lunar Soils

The morphology, mineralogy, chemical composition and optical properties of lunar soils show distinct correlations as a function of grain size and origin [1,2,3]. In the <20 m size fraction, there is an increased correlation between lunar surface properties observed through remote sensing techniques and those attributed to space weathering phenomenae [1,2]. Despite the establishment of recognizable trends in lunar grains <20 in size [1,2,3], the size fraction < 10 m is characterized as a collective population of grains without subdivision. This investigation focuses specifically on grains in the <1 m diameter size fraction for both highland and mare derived soils. The properties of these materials provide the focus for many aspects of lunar research including the nature of space weathering on surface properties, electrostatic grain transport [4,5] and dusty plasmas [5]. In this study, we have used analytical transmission and scanning transmission electron microscopy (S/TEM) to characterize the mineralogy type, microstructure and major element compositions of grains in this important size range in lunar soils.

Thompson, M. S.↗
NASA NTRS2016

Vibroacoustic Characterization of Corrugated-Core and Honeycomb-Core Sandwich Panels

The vibroacoustic characteristics of two candidate launch vehicle fairing structures, corrugated- core and honeycomb-core sandwich designs, were studied. The study of these structures has been motivated by recent risk reduction efforts focused on mitigating high noise levels within the payload bays of large launch vehicles during launch. The corrugated-core sandwich concept is of particular interest as a dual purpose structure due to its ability to harbor resonant noise control systems without appreciably adding mass or taking up additional volume. Specifically, modal information, wavelength dispersion, and damping were determined from a series of vibrometer measurements and subsequent analysis procedures carried out on two test panels. Numerical and analytical modeling techniques were also used to assess assumed material properties and to further illuminate underlying structural dynamic aspects. Results from the tests and analyses described herein may serve as a reference for additional vibroacoustic studies involving these or similar structures.

Allen, Albert↗
NASA NTRS1980

Argon/UF6 plasma experiments: UF6 regeneration and product analysis

An experimental and analytical investigation was conducted to aid in developing some of the technology necessary for designing a self-critical fissioning uranium plasma core reactors (PCR). This technology is applicable to gaseous uranium hexafluoride nuclear-pumped laser systems. The principal equipment used included 1.2 MW RF induction heater, a d.c. plasma torch, a uranium tetrafluoride feeder system, and batch-type fluorine/UF6 regeneration systems. Overall objectives were to continue to develop and test materials and handling techniques suitable for use with high-temperature, high-pressure, gaseous UF6; and to continue development of complementary diagnostic instrumentation and measurement techniques to characterize the effluent exhaust gases and residue deposited on the test chamber and exhaust system components. Specific objectives include: a development of a batch-type UF6 regeneration system employing pure high-temperature fluorine; development of a ruggedized time-of-flight mass spectrometer and associated data acquisition system capable of making on-line concentration measurements of the volatile effluent exhaust gas species in a high RF environment and corrosive environment of UF6 and related halide compounds.

Roman, W. C.↗
NASA NTRS1988

Surface temperature determination in surface analytic systems by infrared optical pyrometry

An IR pyrometric technique for measuring the surface temperatures of metal specimens in an ultrahigh-vacuum analytic chamber is described and demonstrated. The experimental setup comprises a commercial IR microscope with a long-working-distance right-angle objective (focal spot diameter 1 mm at 53 cm), a metal-coated glass vacuum chamber with a Ta-mesh-covered quartz viewport, an Mo specimen stub with an internal heating element, and a Ta disk test specimen with a flat side coated with a high-emissivity graphite film. The results of an initial calibration test are presented graphically and briefly characterized. The measurement error at 450 C is found to be less than 10 C.

Wheeler, Donald R.↗
NASA NTRS1994

Estimation of Vegetation Aerodynamic Roughness of Natural Regions Using Frontal Area Density Determined from Satellite Imagery

Parameterizations of the frontal area index and canopy area index of natural or randomly distributed plants are developed, and applied to the estimation of local aerodynamic roughness using satellite imagery. The formulas are expressed in terms of the subpixel fractional vegetation cover and one non-dimensional geometric parameter that characterizes the plant's shape. Geometrically similar plants and Poisson distributed plant centers are assumed. An appropriate averaging technique to extend satellite pixel-scale estimates to larger scales is provided. ne parameterization is applied to the estimation of aerodynamic roughness using satellite imagery for a 2.3 sq km coniferous portion of the Landes Forest near Lubbon, France, during the 1986 HAPEX-Mobilhy Experiment. The canopy area index is estimated first for each pixel in the scene based on previous estimates of fractional cover obtained using Landsat Thematic Mapper imagery. Next, the results are incorporated into Raupach's (1992, 1994) analytical formulas for momentum roughness and zero-plane displacement height. The estimates compare reasonably well to reference values determined from measurements taken during the experiment and to published literature values. The approach offers the potential for estimating regionally variable, vegetation aerodynamic roughness lengths over natural regions using satellite imagery when there exists only limited knowledge of the vegetated surface.

Jasinski, Michael F.↗
NASA NTRS1998

Parameterization of Vegetation Aerodynamic Roughness of Natural Regions Satellite Imagery

Parameterizations of the frontal area index and canopy area index of natural or randomly distributed plants are developed, and applied to the estimation of local aerodynamic roughness using satellite imagery. The formulas are expressed in terms of the subpixel fractional vegetation cover and one non-dimensional geometric parameter that characterizes the plant's shape. Geometrically similar plants and Poisson distributed plant centers are assumed. An appropriate averaging technique to extend satellite pixel-scale estimates to larger scales is provided. The parameterization is applied to the estimation of aerodynamic roughness using satellite imagery for a 2.3 sq km coniferous portion of the Landes Forest near Lubbon, France, during the 1986 HAPEX-Mobilhy Experiment. The canopy area index is estimated first for each pixel in the scene based on previous estimates of fractional cover obtained using Landsat Thematic Mapper imagery. Next, the results are incorporated into Raupach's (1992, 1994) analytical formulas for momentum roughness and zero-plane displacement height. The estimates compare reasonably well to reference values determined from measurements taken during the experiment and to published literature values. The approach offers the potential for estimating regionally variable, vegetation aerodynamic roughness lengths over natural regions using satellite imagery when there exists only limited knowledge of the vegetated surface.

Jasinski, Michael F.↗
NASA NTRS2015

NASA Work Experience

I have had the opportunity to support the analytical laboratories in chemical analysis of unknown samples, using Optical Microscopy (OM), Polarizing Light Microscopy (PLM), Fourier-Transform Infrared Spectroscopy (FT-IR), Scanning Electron Microscopy with Energy Dispersive Spectroscopy (SEMEDS), and X-ray Powder Diffraction (XPD). I have assisted in characterizing fibers pulled from a spacecraft, a white fibrous residue discovered in a jet refueler truck, brown residue from a plant habitat slated for delivery to the ISS (International Space Station), corrosion on a pipe from a sprinkler, and air filtration material brought back from the ISS. I also conducted my own fiber study in order to practice techniques and further my understanding of background concepts. Furthermore, I had the opportunity to participate in diverse work assignments, where I was assigned to work with other branches of the engineering department for 1-2 days each. The first was in the Materials Science branch where I participated in the construction of the plant habitat intended for use in research aboard the ISS. The second was in the Testing Design branch where I assisted with tensile and hardness testing of over 40 samples. In addition, I have had the privilege to attend multiple tours of the NASA KSC campus, including to the Astronaut Crew Quarters, the VAB (the main area, the Columbia room, and the catwalk), the Visitor Center housing the shuttle Atlantis, the Saturn-V exhibit, the Prototype laboratory, SWAMP WORKS, the Shuttle Landing Facility, the Crawler, and the Booster Fabrication Facility (BFF). Lastly, much of my coursework prepared me for this experience, including numerous laboratory courses with topics diverse as chemistry, physics, and biology.

Florida Tech↗
NASA NTRS2004

Microscale Distribution of Hydrogen Isotopes in Two Carbonaceous Chondrites

Hydrogen isotopes are highly variable among primitive meteorites and interplanetary dust particles (IDPs) [1, 2]. In particular, many primitive objects exhibit D (and N-15) enrichments, relative to terrestrial values, thought to represent partial preservation of presolar material fractionated in molecular clouds. However, the diversity of D/H ratios among IDPs and chondrites indicates a complex history of processing in the solar nebula and on meteorite parent bodies. Deconvolving this record requires identification and characterization of the carriers of D enrichments in different objects. Isotopic imaging has proven to be a powerful method to quantitatively explore the distribution of D/H ratios on a one to several m scale in IDPs [2-4] and the CR chondrite Renazzo [5, 6]. In this study, we have used ion imaging to explore the microscale D/H distribution of two carbonaceous chondrites, Tagish Lake (unique) and Al Rais (CR2). Previous D/H measurements (on a ~tens of microns scale) of Tagish Lake matrix fragments by Messenger [7] and Engrand et al. [8] have found different results, most likely related to the analytical techniques used. Previous work has also shown a large range of D/H ratios in CR chondrites, including very large variations on a scale of a few microns [5, 6, 9].

Young, A. F.↗
NASA NTRS2018

Characterization and Analysis of Phoca Vitulina, Zalophus Californianus and Mirounga Angustirostris Vibrissae

Vibrissae of Phoca Vitulina (harbor seal) and Mirounga Angustirostris (elephant seal) possess undulations along their length. Harbor seal vibrissae have shown potential to reduce vortex induced vibrations and reduce drag compared to cylinders and ellipses. The exact geometry of the whiskers has not been well documented and the parameters that are responsible for the reduction in drag and vortex induced vibrations have not been characterized. Samples of six harbor seal vibrissae, six elephant seal vibrissae and six California sea lion (Zalophus californianus) vibrissae were collected from the Marine Mammal Center in California. The objectives of this study were to (1) Compare measurement techniques for digitizing and extracting parameters of the seal whiskers for the PeTaL (Periodic Table of Life) database. CT scanning, microscopy and 3D scanning techniques were compared. (2) Compare aerodynamic characteristics of a representative harbor seal whisker, elephant seal whisker, California sea lion whisker and ellipse at Re = 12000 and Re = 23000 based on major axis and free stream velocity. The data (in appendices) is available to compare CFD models or for further experimental validation, (3) Show close up images of whiskers and look for surface roughness effects. Variations in the seven parameters of the seal whisker were observed that may either be a feature of the vibration reduction mechanism or a result of natural variation. It is hypothesized that six parameters are sufficient to characterize seal whiskers based on analytic fitting. The drag coefficient of harbor seal whiskers examined in this study were found to be 25 percent lower than that of an ellipse with comparable major and minor axis lengths at Reynolds number of 12000. The dissipation length scale was found to be larger for seal whiskers. Potential applications of seal whisker morphology for aerospace are discussed. Roughness is not thought to play a factor in seal hydrodynamics.

Shyam, Vikram↗
NASA NTRS1986

Analytical ultrasonics for evaluation of composite materials response. Part 2: Generation and detection

To evaluate the response of composite materials, it is imperative that the input excitation as well as the observed output be well characterized. This characterization ideally should be in terms of displacements as a function of time with high spatial resolution. Additionally, the ability to prescribe these features for the excitation is highly desirable. Various methods for generating and detecting ultrasound in advanced composite materials are examined. Characterization and tailoring of input excitation is considered for contact and noncontact, mechanical, and electromechanical devices. Type of response as well as temporal and spatial resolution of detection methods are discussed as well. Results of investigations at Virginia Tech in application of these techniques to characterizing the response of advanced composites are presented.

Duke, J. C., Jr.↗
NASA NTRS1989

Multiple boundary condition testing error analysis

Techniques for interpreting data from multiple-boundary-condition (MBC) ground tests of large space structures are developed analytically and demonstrated. The use of MBC testing to validate structures too large to stand alone on the ground is explained; the generalized least-squares mass and stiffness curve-fitting methods typically applied to MBC test data are reviewed; and a detailed error analysis is performed. Consideration is given to sensitivity coefficients, covariance-matrix theory, the correspondence between test and analysis modes, constraints and step sizes, convergence criteria, and factor-analysis theory. Numerical results for a simple beam problem are presented in tables and briefly characterized. The improved error-updating capabilities of MBC testing are confirmed, and it is concluded that reasonably accurate results can be obtained using a diagonal covariance matrix.

Glaser, R. J.↗
NASA NTRS2003

Understanding Organics in Meteorites and the Pre-Biotic Environment

(1) Refinement of the analytic capabilities of our experiment via characterization of molecule-specific response and the effects upon analysis of the type of sample under investigation; (2) Measurement of polycyclic aromatic hydrocarbons (PAHs) with high sensitivity and spatial resolution within extraterrestrial samples; (3) Investigation of the interstellar reactions of PAHs via the analysis of species formed in systems modeling dust grains and ices; (4) Investigations into the potential role of PAHs in prebiotic and early biotic chemistry via photoreactions of PAHs under simulated prebiotic Earth conditions. To meet these objectives, we use microprobe laser-desorption, laser-ionization mass spectrometry (MuL(exp 2)MS), which is a sensitive, selective, and spatially resolved technique for detection of aromatic compounds. Appendix A presents a description of the MuL(exp 2)MS technique. The initial grant proposal was for a three-year funding period, while the award was given for a one-year interim period. Because of this change in time period, emphasis was shifted from the first research goal, which was more development-oriented, in order to focus more on the other analysis-oriented goals. The progress made on each of the four research areas is given below.

Zare, Richard N.↗
NASA NTRS1998

Effects of Aging-Time Reference on the Long Term Behavior of the IM7/K3B Composite

An analytical study was undertaken to investigate the effects of the time-based shift reference on the long term behavior of the graphite reinforced thermoplastic polyimide composite IM7/K3B at elevated temperature. Creep compliance and the effects of physical aging on the time dependent response was measured for uniaxial loading at several isothermal conditions below the glass transition temperature (T(sub g). Two matrix dominated loading modes, shear and transverse, were investigated in tension and compression. The momentary sequenced creep/aging curves were collapsed through a horizontal (time) shift using the shortest, middle and longest aging time curve as the reference curve. Linear viscoelasticity was used to characterize the creep/recovery behavior and superposition techniques were used to establish the physical aging related material constants. The use of effective time expressions in a laminated plate model allowed for the prediction of long term creep compliance. The effect of using different reference curves with time/aging-time superposition was most sensitive to the physical aging shift rate at lower test temperatures. Depending on the loading mode, the reference curve used can result in a more accurate long term prediction, especially at lower test temperatures.

Veazie, David R.↗
NASA NTRS2014

Mechanical Behavior of Microelectromechanical Microshutters

A custom micro-mechanical test system was constructed using off-the-shelf components to characterize the mechanical properties of microshutters. Microshutters are rectangular microelectromechanical apertures which open and close about a narrow torsion bar hinge. Displacement measurements were verified using both capacitive and digital image correlation techniques. Repeatable experiments on Si3N4 cantilever beams verified that the test system operates consistently. Using beam theory, the modulus of elasticity of the low stress Si3N4 was approximately 150 GPa, though significant uncertainty exists for this measurement due primarily to imprecise knowledge of the cantilever thickness. Tests conducted on microshutter arrays concluded that reducing the Si3N4 thickness from 250 nm to 500 nm reduces the torsional stiffness by a factor of approximately four. This is in good agreement with analytical and finite element models of the microshutters.

silicon nitride↗