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At least 271 records · Page 15

Materials Problems in Chemical Liquid-Propellant Rocket Systems

With the advent of the space age, new adjustments in technical thinking and engineering experience are necessary. There is an increasing and extensive interest in the utilization of materials for components to be used at temperatures ranging from -423 to over 3500 deg F. This paper presents a description of the materials problems associated with the various components of chemical liquid rocket systems. These components include cooled and uncooled thrust chambers, injectors, turbine drive systems, propellant tanks, and cryogenic propellant containers. In addition to materials limitations associated with these components, suggested research approaches for improving materials properties are made. Materials such as high-temperature alloys, cermets, carbides, nonferrous alloys, plastics, refractory metals, and porous materials are considered.

Gilbert, L. L.↗

Thermal Performance of Low Layer Density Multilayer Insu1ation Using Liquid Nitrogen

In order to support long duration cryogenic propellant storage, the Cryogenic Fluid Management (CFM) Project of the Exploration Technology Development Program (ETDP) is investigating the long duration storage propertie$ of liquid methane on the lunar surface. The Methane Lunar Surface Thermal Control (MLSTC) testing is using a tank of the approximate dimensions of the Altair ascent tanks inside of a vacuum chamber to simulate the environment in low earth orbit and on the lunar surface. The thermal performance testing of multilayer insulation (MLI) coupons that are fabricated identically to the tank applied insulation is necessary to understand the performance of the blankets and to be able to predict the performance of the insulation prior to testing. This coupon testing was completed in Cryostat-100 at the Cryogenics Test Laboratory. The results showed the properties of the insulation as a function of layer density, number of layers, and warm boundary temperature. These results aid in the understanding of the performance parameters o fMLI and help to complete the body of literature on the topic.

Johnson, Wesley L.↗

A Liquefaction Model for A Cryogenically Refrigerated Ellipsoidal Tank

Over the past few decades NASA has been developing technology to produce cryogenic propellants on the surfaces of the Moon or Mars. In-situ propellant production reduces the amount of propellants needed to be taken to Moon/Mars and ultimately reduces mission cost. Utilizing Lunar/Martian resources, the produced gases are liquefied and stored prior to use on the ascent vehicle. This paper presents a model for the liquefaction process of gaseous propellants in a cryogenically refrigerated tank. The tank is cylindrical with elliptical top and bottom domes. A transient model is developed based on the mass and energy conservation principles and wall-gas and liquid-gas interfacial mass and heat transfer correlations. The model is incorporated into the Generalized Fluid System Simulation Program (GFSSP), an MSFC in-house general-purpose computer program for flow network analysis. Description of the model and comparison of predicted results with available test data is presented.

Liquefaction↗

Principles of Fluid Dynamic Similarity Analysis for Slosh Experiments

Most tank slosh test programs are not conducted with flight hardware in a flight-like environment due to cost and schedule constraints. Instead, subscale tanks are typically tested on the ground. If the “real”, flight liquid in the tank is a cryogenic propellant, sometimes a cryogen is used during testing, but more often a simulant liquid is used. Fluid dynamic similarity analysis, or “scaling analysis” as it is sometimes called, for slosh examines nondimensional numbers to determine which fluid dynamic regime(s) a tank is operating in. If the relevant nondimensional numbers of a scale tank test are similar enough to the real tank’s nondimensional numbers, then it is likely that the scale test data will be similar to what would be obtained with the real tank. This type of analysis is useful for guiding experiment design, test liquid selection, and for understanding the physical relevance of prior test data to a specific application. The authors have performed scaling analyses for many slosh test programs conducted in ground, parabolic flight, suborbital, and in-orbit environments. Basics of how to perform the analysis, along with select examples from ground and microgravity environments, are presented. Suggestions for various assumptions and compromises to make are discussed. Limitations and challenges are also discussed.

slosh↗

Addressing CFM Modeling Gaps for Application into NASA’S Future Cutting Edge Missions

NASA, the US industry, and international partners are crafting frameworks to enable sustaining lunar missions. The ongoing programs, led by the agency, and prominent industry players, encompass plans for the sustained use of cryogenic propellants in lunar landers and in-space propellant refueling depots. NASA’s proactive funding initiatives have fueled the advancement of predictive computational models tailored to enhance the storage and transfer of cryogenic propellant. This paper aims to spotlight the latest advancements in this arena and delve into the collaborative efforts surrounding predictive model development within internal NASA programs as well as current and previous collaborations with industry and international partners. The paper presents an overview of recent advancements in cryogenic fluid management model development, along with their correlation with recent microgravity and large-scale cryogenic ground tests. The tests include key experiments such as the ISS Zero-Boil-Off Tank (ZBOT) series of experiments and the (Robotic Refueling Mission 3) RRM3 test during which liquid methane was stored on-orbit for an extended period of five months. The paper also highlights the anchoring of propellant tank pressurized drain tests involving sloshing that were conducted with liquid methane propellant during the Apollo/Saturn Era. Additionally, the paper discusses model anchoring against more recent sloshing tests carried out with liquid hydrogen propellant. Notable large-scale tests, such as a liquid oxygen propellant transfer test conducted by SpaceX were also used to help correlate a two-phase propellant transfer model using the valuable data measured during the test. The paper further showcases model correlations against a substantial oxygen liquefaction test undertaken by NASA to validate In-Situ-Resource-Utilization (ISRU) technologies that will prove pivotal for a sustained lunar presence.

Low-gravity fluid modeling↗

Liquid hydrogen/oxygen external tank development for the Space Shuttle

The evolution of the Space Shuttle System using an expendable External Tank was discussed. The reasoning for the cryogenic propellant selection for the Space Shuttle Main Engine was addressed. The unique problems, solutions, and design features imposed on the External Tank by the cryogenic propellants was discussed with special emphasis on the use of cryogenic insulation for aerodynamic heating protection. Manufacturing techniques for high production rate cryogenic tankage concluded the report.

Odom, J. B.↗

Damage Tolerance Assessment of Friction Pull Plug Welds

Friction stir welding is a solid state welding process developed and patented by The Welding Institute in Cambridge, England. Friction stir welding has been implemented in the aerospace industry in the fabrication of longitudinal welds in pressurized cryogenic propellant tanks. As the industry looks to implement friction stir welding in circumferential welds in pressurized cryogenic propellant tanks, techniques to close out the termination hole associated with retracting the pin tool are being evaluated. Friction pull plug welding is under development as a one means of closing out the termination hole. A friction pull plug weld placed in a friction stir weld results in a non-homogenous weld joint where the initial weld, plug weld, their respective heat affected zones and the base metal all interact. The welded joint is a composite, plastically deformed material system with a complex residual stress field. In order to address damage tolerance concerns associated with friction plug welds in safety critical structures, such as propellant tanks, nondestructive inspection and proof testing may be required to screen hardware for mission critical defects. The efficacy of the nondestructive evaluation or the proof test is based on an assessment of the critical flaw size in the test or service environments. Test data relating residual strength capability to flaw size in two aluminum alloy friction plug weld configurations is presented.

McGill, Preston↗

Reliable Ignition of LOX Methane Propellants in Thermal Vacuum Environment

The goal of this project is to demonstrate reliable ignition of liquid oxygen-liquid methane at thermal vacuum conditions using a coil-on-plug (COP) sparking exciter. Testing will be performed using EP’s Frost-Mint cryogenic propellant test stand, using an engine updated based on data collected from previous engine testing at Plum Brook Station, to determine conditions under which the cryogenic propellants will consistently and reliably ignite. In FY22 the project successfully completed the following milestones. The cryogenic test stand Frost-Mint was upgraded to include an integrated vacuum tube and liquid nitrogen cooling system enabling cold vacuum ignition testing. The Integrated GN2/LN2 Ultra-Low-temperature Enclosure (IGLUE), a custom-built close-coupled heater exchanger shroud was designed, fabricated, tested and integrated into the test stand. The vacuum tube and IGLUE enabled the thruster body and propellants to be conditioned to temperatures and pressures desired. This work recreated the no-light conditions experienced during vehicle-level thermal vacuum testing and obtained thruster performance data and ignition imagery.

liquid oxygen↗

Small rocket research and technology

Small chemical rockets are used on nearly all space missions. The small rocket program provides propulsion technology for civil and government space systems. Small rocket concepts are developed for systems which encompass reaction control for launch and orbit transfer systems, as well as on-board propulsion for large space systems and earth orbit and planetary spacecraft. Major roles for on-board propulsion include apogee kick, delta-V, de-orbit, drag makeup, final insertions, north-south stationkeeping, orbit change/trim, perigee kick, and reboost. The program encompasses efforts on earth-storable, space storable, and cryogenic propellants. The earth-storable propellants include nitrogen tetroxide (NTO) as an oxidizer with monomethylhydrazine (MMH) or anhydrous hydrazine (AH) as fuels. The space storable propellants include liquid oxygen (LOX) as an oxidizer with hydrazine or hydrocarbons such as liquid methane, ethane, and ethanol as fuels. Cryogenic propellants are LOX or gaseous oxygen (GOX) as oxidizers and liquid or gaseous hydrogen as fuels. Improved performance and lifetime for small chemical rockets are sought through the development of new predictive tools to understand the combustion and flow physics, the introduction of high temperature materials to eliminate fuel film cooling and its associated combustion inefficiency, and improved component designs to optimize performance. Improved predictive technology is sought through the comparison of both local and global predictions with experimental data. Results indicate that modeling of the injector and combustion process in small rockets needs improvement. High temperature materials require the development of fabrication processes, a durability data base in both laboratory and rocket environments, and basic engineering property data such as strength, creep, fatigue, and work hardening properties at both room and elevated temperature. Promising materials under development include iridium-coated rhenium and a ceramic composite of mixed hafnium carbide and tantalum carbide reinforced with graphite fibers.

Schneider, Steven↗

Advanced Small Rocket Chambers. Basic Program and Option 2: Fundamental Processes and Material Evaluation

Propellants, chamber materials, and processes for fabrication of small high performance radiation cooled liquid rocket engines were evaluated to determine candidates for eventual demonstration in flight-type thrusters. Both storable and cryogenic propellant systems were considered. The storable propellant systems chosen for further study were nitrogen tetroxide oxidizer with either hydrazine or monomethylhydrazine as fuel. The cryogenic propellants chosen were oxygen with either hydrogen or methane as fuel. Chamber material candidates were chemical vapor deposition (CVD) rhenium protected from oxidation by CVD iridium for the chamber hot section, and film cooled wrought platinum-rhodium or regeneratively cooled stainless steel for the front end section exposed to partially reacted propellants. Laser diagnostics of the combustion products near the hot chamber surface and measurements at the surface layer were performed in a collaborative program at Sandia National Laboratories, Livermore, CA. The Material Sample Test Apparatus, a laboratory system to simulate the combustion environment in terms of gas and material temperature, composition, and pressure up to 6 Atm, was developed for these studies. Rocket engine simulator studies were conducted to evaluate the materials under simulated combustor flow conditions, in the diagnostic test chamber. These tests used the exhaust species measurement system, a device developed to monitor optically species composition and concentration in the chamber and exhaust by emission and absorption measurements.

Jassowski, Donald M.↗

Thermal Desktop Modeling of the 2016 CRYOTE-2 Tank Chill and Fill Tests

The storing and transfer of cryogenic propellants is an enabling technology for NASA as it moves to expand future missions into low Earth orbit (LEO) and beyond. The transfer of cryogenic propellants is of particular interest because it has never been successfully demonstrated in microgravity. Several ground tests have been conducted in past decades examining various tank chilldown and fill methods. Creating accurate models using these historical datasets is a vital step toward developing appropriate modeling tools to form pre-test predictions for eventual flight and ground tests of various novel injector concepts. The goal of this work was to create a working model in Thermal Desktop using data from the CRYOTE-2 experiments whose purpose was to demonstrate the chill and fill process in a spherical receiver tank parametrically examining the effect of injection method, receiver tank initial wall temperature and initial state, supply pressure, and mass flow rate on the NVF process. These tests were conducting using liquid nitrogen with different injectors with different injection patterns. The focus of the current work is on one particular spray nozzle. The pressure rise inside the tank, the fill level, and the change in the outside wall temperature were all tracked and compared with test data. The Thermal Desktop model was able to accurately predict each of these metrics for this nozzle within 11.0%, 22.0%, and 7.0%, respectively.

Cryogenic Tank Chilldown↗

Reduced Boil-Off System Sizing

NASA is currently developing cryogenic propellant storage and transfer systems for future space exploration and scientific discovery missions by addressing the need to raise the technology readiness level of cryogenic fluid management technologies. Cryogenic propellants are baselined in many propulsion systems due to their inherently high specific impulse; however, their low boiling points can cause substantial boil-off losses over time. Recent efforts such as the Reduced Boil-off Testing and the Active Thermal Control Scaling Study provide important information on the benefit of an active cooling system applied to LH2 propellant storage. Findings show that zero-boil off technologies can reduce overall mass in LH2 storage systems when low Earth orbit loiter periods extend beyond two months. A significant part of this mass reduction is realized by integrating two stages of cooling: a 20 K stage to intercept heat at the tank surface, and a 90 K stage to reduce the heat entering the less efficient 20 K stage. A missing element in previous studies, which is addressed in this paper, is the development of a direct method for sizing the 90 K cooling stage. Such a method requires calculation of the heat entering both the 90 K and 20 K stages as compared to the overall system masses, and is reliant upon the temperature distribution, performance, and unique design characteristics of the system in question. By utilizing the known conductance of a system without active thermal control, the heat being intercepted by a 90 K stage can be calculated to find the resultant lift and mass of each active thermal control stage. Integral to this is the thermal conductance of the cooling straps and the broad area cooling shield, key parts of the 90 K stage. Additionally, a trade study is performed to show the ability of the 90 K cooling stage to reduce the lift on the 20 K cryocooler stage, which is considerably less developed and efficient than 90 K cryocoolers.

Cryogenic fluid management↗

Liquid Oxygen Propellant Densification Unit Ground Tested With a Large-Scale Flight-Weight Tank for the X-33 Reusable Launch Vehicle

Propellant densification has been identified as a critical technology in the development of single-stage-to-orbit reusable launch vehicles. Technology to create supercooled high-density liquid oxygen (LO2) and liquid hydrogen (LH2) is a key means to lowering launch vehicle costs. The densification of cryogenic propellants through subcooling allows 8 to 10 percent more propellant mass to be stored in a given unit volume, thereby improving the launch vehicle's overall performance. This allows for higher propellant mass fractions than would be possible with conventional normal boiling point cryogenic propellants, considering the normal boiling point of LO2 and LH2.

Tomsik, Thomas M.↗

Validation of CFD Model Prediction of Flow Boiling Regime Transitions during LN2 Line Chilldown

Propellant storage and transfer during future long-duration missions will involve fuel depot operations in which a donor depot tank is used to fill a receiver spacecraft tank with a cryogenic propellant. Prior to the on-Orbit filling operation both the receiver tank and the transfer line must be cooled. The line chilldown process involves transition between boiling regimes in microgravity that will be quite different from their 1g ground-based counterparts. Since the cryogenic propellant itself will be used to perform the chilldown process, the time constants to cool the wall and the amount of fuel that will be used become important design considerations. In this light, the focus of the present work is to understand the flow boiling characteristics of a cryogenic fluid, namely, liquid nitrogen, during the chill-down of a transfer line using CFD modelling and simulations. The cryogenic chill-down process involves different flow boiling regimes: film boiling, transition boiling and nucleate boiling. The prediction of transition between these regimes in a CFD framework is new and challenging. The present work addresses this challenge by employing a volume-of-fluid (VOF) based methodology with Lee phase change model to predict the film boiling regime of the chill-down process in ANSYS Fluent®. The transition and nucleate boiling regimes are predicted by incorporating a sub-grid model developed by Craft Tech that accounts for bubble nucleation, growth, shedding frequency, and departure diameter. The sub-grid model is implemented into Fluent via a user-defined function for wall-fluid heat flux calculations. The sub-grid model is similar in formulation to the well-known Rensselaer Polytechnic Institute (RPI) boiling model. The model constants are tested for different operating conditions and designated values are reported. The CFD model is validated against published experimental data for liquid nitrogen chill-down of a heated stainless-steel pipe in 1g. Predicted results showing good agreement of wall temperature, rewetting temperature, and transition between film and nucleate boiling with the experimental measurements are presented and discussed.

Boiling regimes↗

Predictions of Line Chilldown Boiling Regime Transitions by a Coupled CFD-Sub-Grid Boiling Model Validated against 1G LN2 Experiments

Propellant storage and transfer during future long-duration missions will involve fuel depot operations in which a donor depot tank is used to fill a receiver spacecraft tank with a cryogenic propellant. Prior to the on-Orbit filling operation both the receiver tank and the transfer line must be cooled. The line chilldown process involves transition between boiling regimes in microgravity that will be quite different from their 1g ground-based counterparts. Since the cryogenic propellant itself will be used to perform the chilldown process, the time constants to cool the wall and the amount of fuel that will be used become important design considerations. In this light, the focus of the present work is to capture the flow boiling characteristics of a cryogenic fluid, namely, liquid nitrogen, during the chill-down of a transfer line using CFD modelling and simulations. The cryogenic chill-down process involves different flow boiling regimes: film boiling, transition boiling and nucleate boiling. The prediction of transition between these regimes in a CFD framework is new and challenging. The present work addresses this challenge by employing a volume-of-fluid (VOF) based methodology with Lee phase change model to predict the film boiling regime of the chill-down process in ANSYS Fluent®. The transition and nucleate boiling regimes are predicted by incorporating a sub-grid model that accounts for bubble nucleation, growth, shedding frequency, and departure diameter. The sub-grid model is implemented into Fluent via a user-defined function for wall-fluid heat flux calculations. The sub-grid model is similar in formulation to the well-known Rensselaer Polytechnic Institute (RPI) boiling model. The CFD model is validated against published experimental data for liquid nitrogen chill-down of a heated stainless-steel pipe in 1g. Predicted results shows good agreement of wall temperature, rewetting temperature, and transition between film and nucleate boiling with the experimental measurements for several different LN2 flowrates in the vertical orientation. The strengths and weaknesses of this modeling approach are presented and discussed.

Cryogenic Fluid Management↗

Solar White Thermal Coating for Cryogenic Propulsion Systems

NASA is currently conducting research into the potential of storing cryogenic fluid in low Earth orbit (LEO). Having cryogenic propellant readily available for high-performance propulsion systems can be very beneficial for deep space missions in the near future. One of the key challenges to storing cryogenic fluid in LEO is minimizing boil-off. To address the challenge, NASA is evaluating new concepts in thermal insulation. One recent experimental study evaluated the feasibility of using Yttrium Oxide (Y2O3), formed into tiles or spray coating that can potentially be used as a thermal coating for cryogenic propellant storage applications in deep space. Due to its temperature and wavelength dependent optical properties, this “solar white” material can reflect a vast majority of the Sun’s radiative energy while having a very high infrared emissivity for rejecting heat to deep space. As a part of the material development and proof of concept testing, multiple tests have been run at KSC and GRC to demonstrate the performance of the material. At GRC, the tests were run using the Deep Space Solar Simulator (DS3) which contains a thermal vacuum chamber in which the solar white sample was exposed to a deep space environment (< 10 K, optically dense walls) while under full illumination via solar lamp. In order to improve the use of the test results and apply them to spacecraft, there is a need to be able to model the material properties within NASA’s standard thermal modeling tools. As such, it was set out to verify a thermal model of one of the experiments using Thermal Desktop with Sinda. The thermal model of the DS3 test setup includes the solar white sample along with a solar lamp simulator capable of outputting heat at varying wavelengths. The model was developed in order to validate the test results and also to help predict results that will be obtained in future tests. This paper will review the modeling methods and thermal analysis results for various test cases that were run within the DS3 facility.

Cryogenic↗

Radiation Shielding for Nuclear Thermal Propulsion

Design and analysis of radiation shielding for nuclear thermal propulsion has continued at Marshall Space Flight Center. A set of optimization tools are in development, and strategies for shielding optimization will be discussed. Considerations for the concurrent design of internal and external shielding are likely required for a mass optimal shield design. The task of reducing radiation dose to crew from a nuclear engine is considered to be less challenging than the task of thermal mitigation for cryogenic propellant, especially considering the likely implementation of additional crew shielding for protection from solar particles and cosmic rays. Further consideration is thus made for the thermal effects of radiation absorption in cryogenic propellant. Materials challenges and possible methods of manufacturing are also discussed.

Caffrey, Jarvis A.↗

Analytical Study of a Cryogenic Thermal Control Coating

This study focuses on the analysis of a cryogenic thermal control coating designed to reflect most of the Sun’s irradiance while emitting long wavelength radiation, thus enabling propulsion systems to maintain cryogenic temperatures while in deep space. This “solar white” coating is composed of yttrium oxide (Y2O3) which has properties that are well-suited for cryogenic propellant storage applications. To conduct proof of concept and material development, many tests have been run at both NASA Kennedy Space Center (KSC) and Glenn Research Center (GRC) to demonstrate the performance of the coating in the cryogenic regime in both powder and ceramic forms. At GRC, the Deep Space Solar Simulator (DS3) was used to run thermal vacuum tests where the coating was exposed to a deep space environment (~10 K) with some tests conducted under the illumination of a solar lamp. Using the test data, a thermal model of the DS3 test setup was developed to correlate the test results to predict the optical properties of the coating. Once the optical properties were determined, an additional thermal model, based on previous work by R.C. Young quist et al., was developed to verify the performance of a theoretical lunar, cryogenic propellant depot. The latter thermal model also demonstrates the usage of the HLS-UG-001 Human Landing System Lunar Thermal Analysis Guidebook published to baseline Artemis-related lunar studies.

Cryogenic↗