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At least 307 records · Page 17

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NASA NTRS1985

Investigation of superlattice device structures

This report describes the investigation of growth properties, and the structure of epitaxial multilayer Si(Si(1x)Ge(x)) films grown on bulk Silicon Substrates. It also describes the fabrication and characterization of MOSFET and MESFET devices made on these epitaxial films. Films were grown in a CVD reactor using hydrides of Si and Ge with H2 and He as carrier gases. Growth temperatures were between 900 C and 1050 C with most films grown at 1000 C. Layer thickness was between 300A and 2000A and total film thickness was between 0.25 micro m and 7 micro m. The Ge content (X) in the alloy layers was between .05 and 0.2. N-type multilayer films grown on (100) p-type Si showed Hall mobility in the range 1000 to 1500 sq cm/v for an average carrier concentration of approx. 10 to the 16th power/cu cm. This is up to 50% higher than the Hall mobility observed in epitaxial Si films grown under the same conditions and with the same average carrier concentration. The mobility enhancement occurred in films with average carrier concentration (n) from 0.7 x 10 to the 16th power to 2 x 10 to the 17th power/cu cm, and total film thickness greater than 1.0 micro m. No mobility enhancement was seen in n-type multilayer films grown on (111) Si or in p-type multilayer films. The structure of the films was investigated was using SEM, TEM, AES, SIMS, and X-ray double crystal diffraction techniques. The film composition profile (AES, SIMS) showed that the transition region between layers is of the order of about 100A. The TEM examination revealed a well defined layered structure with fairly sharp interfaces and good crystalline quality. It also showed that the first few layers of the film (closest to the substrate) are uneven, most probably due to the initial growth pattern of the epitaxial film where growth occurs first in isolated islands that eventually growth and coalesce. The X-ray diffraction measurement determined the elastic strain and strain relief in the alloy layers of the film and the elastic strain in the intervening Si layers.

Gergis, I. S.↗

NASA NTRS1985

Ephemeral regions versus pseudo ephemeral regions

New studies of the quiet Sun reveal that ephemeral active regions constitute minority rather than a majority of all the short lived, small scale bipolar features on the Sun. In contrast to the recognized patterns of growth and decay of ephemeral regions, various examples of the creation of other temporary bipoles nicknamed pseudo ephemeral regions are illustrated. The pseudo ephemeral regions are the consequence of combinations of small scale dynamic processes of the quiet Sun including: (1) fragmentation of network magnetic fields, (2) the separation of opposite polarity halves of ephemeral regions as they grow and evolve, and (3) the coalescence of weak network or intranetwork magnetic fields. New observations offer the possibility of resolving the discrepancies that have arisen in the association of ephemeral regions with X-ray bright points. Many X-ray bright points may be related to those pseudo ephemeral regions which have begun to exhibit magnetic flux loss.

Martin, S. F.↗

NASA NTRS1984

On the nature of the material surrounding Vega

Observations of Vega at 193 microns indicate that the far-infrared emission from the circumstellar material discovered by IRAS (Aumann et al. 1984) may decline more rapidly than a Planck spectrum at wavelengths greater than 100 microns. This suggests that the emitting particles may be smaller than the millimeter-sized objects proposed by Aumann et al. (1984). Small grains would be driven from the stellar system by radiation pressure, or their orbits would decay as a result of Poynting -Robertson drag. In order to maintain a state of dynamic equilibrium, a continuous supply of new particles would be required. It is hypothesized that the small grains are ejected by sublimation of volatile material from larger comet-like bodies in a partially coalesced preplanetary disk. A reservoir containing less than a few hundred earth masses could sustain the source over the lifetime of the star.

Harper, D. A.↗

NASA NTRS1985

STS 8 Orbiter mission window pitting and the possible association with the El Chichon eruption of March and April 1982

The possibility that the pitting that occurred in the STS-8 Orbiter windows was caused by dust from the El Chichon volcano eruption in March-April 1982 is considered. The pit density was more than 30/sq cm, most being 2.5-5 microns deep, and showed no evidence of impact melting. An 'alley' of higher incidence of pits in one window coincided with the line of a seam between TPS tiles. The particles causing the sandblasting were concluded to have arrived in parallel and could not be attributed to the ET, SRBs or a dust storm. The sulfuric gas-rich El Chichon plume injected sufficient material into the atmosphere so that the globe was soon encircled. Most of the resulting particulates (480-8400 tons) stayed in the Northern Hemisphere, and H2SO4 and ash concentrations were high during the STS-8 mission. The Orbiter cut through the debris layer at 19.8 km altitude at a 10 deg angle of attack, which matches the particle crater impact angle in the Orbiter windows. Since the passage was at night, larger H2SO4 droplets may have coalesced and formed larger particles on available solid nuclei, thus producing the 20-40 microns cratering observed in the windows.

Cour-Palais, B. G.↗

NASA NTRS1983

Radial gradients of galactic cosmic rays measured by Pioneer 10 from 1-29 AU through the period of solar maximum

During the approach to maximum solar modulation in 1982, the radial gradient of high energy galactic cosmic rays gradually increased to about 2.5 percent/AU from the solar minimum value of about 1.5 percent/AU. In the same period, at energies lower than 70 MeV/n, the radial gradients for protons decreased from about 8 percent/AU to about 1 percent/AU. It is found that at solar maximum, in contrast to solar minimum, essentially all of the modulation of low energy cosmic rays occurs outside R = 29 AU. The combined effects of solar flare shocks coalescing in the far outer heliosphere may account for this dramatic change in the radial dependence of modulation.

Mckibben, R. B.↗

NASA NTRS1985

Optical studies of a binary miscibility gap system

Model transparent fluids are being studied to develop a better understanding of phase separation processes in binary miscibility-gap metal alloys. The model selected for the reported work is diethylene glycol-ethyl salicylate. This system is well characterized with respect to its phase diagram, density, surface and interfacial tensions, viscosity, and other pertinent physical properties. Minority phase growth, coalescence, and droplet motions are observed using holographic microscopy which is capable of recording particle densities up to 10 to the 7th particles/cu cm and is able to resolve particles as small as 2 to 3 microns in diameter throughout the entire volume of the test cell. Sequential holograms allow determination of droplet size distribution changes throughout the total volume with respect to time and temperature. This allows a direct method for testing various theories of droplet growth and ripening phenomena.

Witherow, W. K.↗

NASA NTRS1984

Transient processes in combustion of single submillimeter metal droplets

A laser was used to ignite Al, Zr, Ti and Hf droplets in separate trials to study metal droplet combustion in air. The burning was recorded with high speed film at high magnification. Al was found to flash vaporize, melt, surface oxidize, revaporize, then combust. All species burned with a vapor diffusion flame surrounded by an oxide condensation front. The Zr, Ti and Hf droplets grew by condensation, coalesced, then convected toward the perimeter of the condensation zone. It is expected that the data will serve as bases for a theoretical vapor diffusion model. Finally, the introduction of a transverse acoustic field was observed to have no effect on either the luminosity or combustion zone geometry.

Pellett, G. L.↗

NASA NTRS1985

Multiple Raman up-conversion of radiation from pre-existing Langmuir turbulence

Little is known regarding the mechanisms involved in the production of radiation at frequencies which are much higher than the maximum plasma frequency in nonmagnetic plasmas. It is pointed out that radiation at high multiples of the plasma frequency has been observed in laser-pellet experiments, in relativistic beam-plasma interactions, and in low-energy beam-plasma interactions. Radiation at twice the plasma frequency can be produced by coalescence of two Langmuir waves. Another approach is based on radiation near the plasma frequency or its second harmonic, produced by instability or by external sources. Raman scatter from preexisting Langmuir turbulence is permitted repeatedly. At each step such scattering will produce frequency upshifts (anti-Stokes process) and downshifts (Stokes process). The present paper is concerned with this process. Attention is given to equilibrium spectra, analytic approximations, laser-plasma interaction and coherent radiation from relativistic electron beams.

Russell, D.↗

NASA NTRS1985

Stream dynamics between 1 AU and 2 AU - A comparison of observations and theory

A radial alignment of three solar wind stream structures observed by IMP-7 and -8 (at 1.0 AU) and Voyager 1 and 2 (in the range 1.4 to 1.8 AU) in late 1977 is presented. It is demonstrated that several important aspects of the observed dynamical evolution can be both qualitatively and quantitatively described with a single-fluid 2-D MHD numerical model of quasi-steady corotating flow, including accurate prediction of: (1) the formation of a corotating shock pair at 1.75 AU in the case of a simple, quasi-steady stream; (2) the coalescence of the thermodynamic and magnetic structures associated with the compression regions of two neighboring, interacting, corotating streams; and (3) the dynamical destruction of a small (i.e., low velocity-amplitude, short spatial-scale) stream by its overtaking of a slower moving, high-density region associated with a preceding transient flow. The evolution of these flow systems is discussed in terms of the concepts of filtering and entrainment.

Burlaga, L. F.↗

NASA NTRS1985

Improved aqueous scrubber for collection of soluble atmospheric trace gases

A new concentration technique for the extraction and enrichment of water-soluble atmospheric trace gases has been developed. The gas scrubbing technique efficiently extracts soluble gases from a large volume flow rate of air sample into a small volume of refluxed trapping solution. The gas scrubber utilizes a small nebulizing nozzle that mixes the incoming air with an aqueous extracting solution to form an air/droplet mist. The mist provides excellent interfacial surface areas for mass transfer. The resulting mist sprays upward through the reaction chamber until it impinges upon a hydrophobic membrane that virtually blocks the passage of droplets but offers little resistance to the existing gas flow. Droplets containing the scrubbed gases coalesce on the membrane and drip back into the reservoir for further refluxing. After a suitable concentration period, the extracting solution containing the analyte can be withdrawn for analysis. The nebulization-reflex concentration technique is more efficient (maximum flow of gas through the minimum volume of extractant) than conventional bubbler/impinger gas extraction techniques and is offered as an alternative method.

Cofer, W. R., III↗

NASA NTRS1985

Current sheets in solar flares

Numerical simulations of current sheets in solar flares are described, including new features such as the presence of a shock in Petschek's mechanism and impulsive burst-like reconnection due to secondary tearing and coalescence. The general properties of magnetic reconnection are discussed in connection with the basic requirements of numerical current sheet models. Emphasis is given to the need for realistic criteria for energy balance, the Lundquist number, and line tying in calculations of tearing and reconnection modes. The need for analytical models of current sheet processes to compare with the numerical simulations is also stressed.

Priest, E. R.↗

NASA NTRS1985

Studies of Model Immiscible Systems

The objectives are to use model transparent monotectics to obtain fundamental information applicable to two-phase systems in general, to apply this understanding to materials of interest in the Microgravity Science and Applications program, and to interpret results of flight experimental involving monotectic alloys. A number of model immiscible systems are in use to study various aspects of two-phase behavior within the miscibility gap and during solidification. Particle growth, coalescence and particle motions are under investigation using a holographic microscopy system. The system is capable of working with particle densities up to 10 to the 7th power particles/cubic centimeters through a 100 micron depth and can resolve particles of the order of 2 to 3 micron in diameter throughout the entire cell volume. Particle size, distribution changes with respect to time and temperature are observable from sequential holograms. Initial experiments using diethylene glycol/ethyl salicylate (DEG/ES) have demonstrated the usefulness of the technique. The thermal system controls temperature to at least plus or minus 0.001 K over the course of an experiment. A time-lapse film, made from holograms, of a succinonitrile/water solution shows particle size and number distribution changes with time under isothermal conditions. The observations are consistent with Ostwald ripening theory.

Frazier, D. O.↗

NASA NTRS1984

Space shuttle experiments on Al-In liquid phase miscibility gap (LPMG) alloys

Massive phase separation observed at low-g was studied during the phase separation process while cooling through the miscibility gap under a controlled thermal gradient was investigated. The molten drops which form during the phase separation process appear to move in a direction opposite to that predicted by the theory of thermocapillary droplet motion. A second experiment utilized a plunger arrangement designed to eliminate the surface tension driven convection currents originating at a free surface. This experiment suggests that the free surface does contribute to the coalescence process but that there are other mechanisms which are more important.

Gelles, S. H.↗

NASA NTRS1985

The interaction of small metal particles with refractory oxide supports

Islands and continuous layers of Pd were grown in UHV on Mo and MoO subtrates. As-deposited Pd islands and layers exhibited bulk Pd adsorption properties for CO when the Pd had been deposited at RT and at thicknesses exceeding 3 ML. However, CO adsorption was drastically reduced upon annealing. This deactivation was interpreted in terms of substrate/support interaction involving the diffusion of substrate species toward the Pd surface, using AES, TPD, and work function measurement techniques. A study of the growth and annealing behavior of Pd on Mo(110) was made for thicknesses up to 12 monolayers and substrate temperatures up to 1300K, using AES, XPS, LEED, and work function measurements. At low tempertures Pd formed a monolayer without alloying. In thick layers (12 ML) annealed about 700 K, Mo diffusion into the Pd layer and alloying were noted. Such layers remained continuous up to 1100 K. Thinner Pd layers were less stable and started coalescing upon annealing to as little as 550 K. Significant changes in Pd Auger peak shape, as well as shifts of Pd core levels, were observed during layer growth and annealing.

Park, C.↗

NASA NTRS1986

Soliton turbulence

Theoretical and numerical works in atmospheric turbulence have used the Navier-Stokes fluid equations exclusively for describing large-scale motions. Controversy over the existence of an average temperature gradient for the very large eddies in the atmosphere suggested that a new theoretical basis for describing large-scale turbulence was necessary. A new soliton formalism as a fluid analogue that generalizes the Schrodinger equation and the Zakharov equations has been developed. This formalism, processing all the nonlinearities including those from modulation provided by the density fluctuations and from convection due to the emission of finite sound waves by velocity fluctuations, treats large-scale turbulence as coalescing and colliding solitons. The new soliton system describes large-scale instabilities more explicitly than the Navier-Stokes system because it has a nonlinearity of the gradient type, while the Navier-Stokes has a nonlinearity of the non-gradient type. The forced Schrodinger equation for strong fluctuations describes the micro-hydrodynamical state of soliton turbulence and is valid for large-scale turbulence in fluids and plasmas where internal waves can interact with velocity fluctuations.

Tchen, C. M.↗

NASA NTRS1986

Ultrasonic characterization of microstructure in powder metal alloy

The ultrasonic wave propagation characteristics were measured for IN-100, a powder metallurgy alloy used for aircraft engine components. This material was as a model system for testing the feasibility of characterizing the microstructure of a variety of inhomogeneous media including powder metals, ceramics, castings and components. The data were obtained for a frequency range from about 2 to 20 MHz and were statistically averaged over numerous volume elements of the samples. Micrographical examination provided size and number distributions for grain and pore structure. The results showed that the predominant source for the ultrasonic attenuation and backscatter was a dense (approx. 100/cubic mm) distribution of small micropores (approx. 10 micron radius). Two samples with different micropore densities were studied in detail to test the feasibility of calculating from observed microstructural parameters the frequency dependence of the microstructural backscatter in the regime for which the wavelength is much larger than the size of the individual scattering centers. Excellent agreement was found between predicted and observed values so as to demonstrate the feasibility of solving the forward problem. The results suggest a way towards the nondestructive detection and characterization of anomalous distributions of micropores when conventional ultrasonic imaging is difficult. The findings are potentially significant toward the application of the early detection of porosity during the materials fabrication process and after manufacturing of potential sites for stress induced void coalescence leading to crack initiation and subsequent failure.

Tittmann, B. R.↗

NASA NTRS1986

Silicon production in a fluidized bed reactor

Part of the development effort of the JPL in-house technology involved in the Flat-Plate Solar Array (FSA) Project was the investigation of a low-cost process to produce semiconductor-grade silicon for terrestrial photovoltaic cell applications. The process selected was based on pyrolysis of silane in a fluidized-bed reactor (FBR). Following initial investigations involving 1- and 2-in. diameter reactors, a 6-in. diameter, engineering-scale FBR was constructed to establish reactor performance, mechanism of silicon deposition, product morphology, and product purity. The overall mass balance for all experiments indicates that more than 90% of the total silicon fed into the reactor is deposited on silicon seed particles and the remaining 10% becomes elutriated fines. Silicon production rates were demonstrated of 1.5 kg/h at 30% silane concentration and 3.5 kg/h at 80% silane concentration. The mechanism of silicon deposition is described by a six-path process: heterogeneous deposition, homogeneous decomposition, coalescence, coagulation, scavenging, and heterogeneous growth on fines. The bulk of the growth silicon layer appears to be made up of small diameter particles. This product morphology lends support to the concept of the scavenging of homogeneously nucleated silicon.

Rohatgi, N. K.↗

NASA NTRS1986

Fluidized-bed development at JPL

Silicon deposition on silicon seed particles by silane pyrolysis in a fluidized bed reactor (FBR) was investigated as a low cost, high throughput method to produce high purity polysilicon for solar cell applications. The emphasis of the research is fundamental understanding of fluidized bed silicon deposition. The mechanisms involved were modeled as a six-path process: heterogeneous deposition; homogeneous decomposition; coalescence; coagulation; scavenging; and chemical vapor deposition growth on fines.

Hsu, G.↗