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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 343 records · Page 19
All sourcesNASA NTRSDOE OSTI
NASA NTRSDate not supplied

The Material Response of PICA-NuSil to a Hypersonic Flow Environment

Phenolic Impregnated Carbon Ablator (PICA) is NASA’s baseline thermal protection system for missions to Mars. PICA is friable; therefore, NuSil ® CV-1144-0 is applied to the surface of flight hardware to mitigate the contamination of spacecraft sensors. NuSil is composed of a polysiloxane resin system that can transform into an oxidation-resistant coating upon heating. Therefore, a pathfinder campaign was conducted at the Hypersonic Materials Environmental Test System (HyMETS) at the NASA Langley Research Center to investigate the material response of instrumented sphere-cone models made from PICA coated with NuSil ® . Analysis of the post-test data is presented and suggests that NuSil ® impacts the material response of test articles subjected to oxidizing atmospheres, as evidenced by a reduction of the measured surface temperature and in-depth temperature response. Finally, a four-step ablation mechanism is proposed based on observations from high-speed video, optical emission spectroscopy, thermal analysis, and post-test surface characterization.

PICA PICA-NuSil Siloxane Silicone↗
NASA NTRSDate not supplied

Development of Langmuir and Spatially Resolved OES Diagnostics for Arc Jet Shock and Boundary Layer Measurements Relevant to Atmospheric Re-Entry Environments

The second-generation miniature Arc Jet Research Chamber (mARC) ground testing facility at NASA Ames requires physical characterization of its supersonic plasma flow to verify numerical models and material sample testing. Two types of plasma diagnostics will be utilized: Langmuir probes and optical emission spectroscopy (OES). Several single and triple Langmuir probes have been constructed and will be inserted parallel to the flow via a sweep arm to measure post-shock electron temperature and number density along radial profiles at different axial distances. Due to the high heat flux (200-3000 W/cm2) sweep durations are necessarily short (< 0.1 s). Measuring these properties near the probe surface provide characterization of the post-shock environment. This is an important metric for validating coupled CFD-material codes, and will provide insight into longstanding thermocouple anomalies attributed to charging of heatshield surfaces. An OES system has also been assembled to obtain spatially resolved density and temperature for various flow species. The system consists of a convex lens that forms an image of the plasma onto a 16-channel linear fiber array, which will simultaneously capture the spectra from sixteen different locations. The light emission from the plasma is then focused by a spherical mirror into a spectrometer and recorded with a camera. These measurements non-intrusively provide a new spatially resolved flow characterization capability. This will initially be used to resolve issues with shock radiation interference in pyrometer measurements of material surface temperature. The design of each diagnostic and any initial results will be discussed.

Ethan Main-Loam Leong↗
NASA NTRSDate not supplied

The Characterization of a DC Glow Discharge in a Tripped Hypersonic Boundary Layer

A direct current glow discharge plasma was generated on a canonical 2.75° half-angle wedge test article. Experiments were conducted in the Texas A&M University Actively Controlled Expansion tunnel at 𝑀 = 5.7 and 𝑅𝑒 = 6 × 10 6 /m. The effect of Reynolds number, polarity, and upstream perturbation were all independently studied via imaging, power measurements, and optical emission spectroscopy (OES). These measurements are the first to be conducted in a tripped hypersonic boundary layer and allow a deeper understanding of the electrohydrodynamics. The plasma, formally characterized as a normal glow discharge, had negligible Joule and cathode heating effects on the boundary layer. Analogously, the installation of trips upstream of the electrodes changed only the appearance of the plasma, creating periodic streaks corresponding to the wakes and vortices produced by each trip but not altering the power across the electrodes. The plasma power peaked at 47 W, which OES revealed was sufficient to generate NO in the positive column and negative glow.

Casey J. Broslawski↗
NASA NTRSDate not supplied

The Characterization of a DC Glow Discharge in a Tripped Hypersonic Boundary Layer

A direct current glow discharge plasma was generated on a canonical 2.75° half-angle wedge test article. Experiments were conducted in the Texas A&M University Actively Controlled Expansion tunnel at 𝑀 = 5.7 and 𝑅𝑒 = 6 × 10 6 /m. The effect of Reynolds number, polarity, and upstream perturbation were all independently studied via imaging, power measurements, and optical emission spectroscopy (OES). These measurements are the first to be conducted in a tripped hypersonic boundary layer and allow a deeper understanding of the electrohydrodynamics. The plasma, formally characterized as a normal glow discharge, had negligible Joule and cathode heating effects on the boundary layer. Analogously, the installation of trips upstream of the electrodes changed only the appearance of the plasma, creating periodic streaks corresponding to the wakes and vortices produced by each trip but not altering the power across the electrodes. The plasma power peaked at 47 W, which OES revealed was sufficient to generate NO in the positive column and negative glow.

Casey Broslawski↗
NASA NTRSDate not supplied

Evaluating Diurnal Ozone Emissions: A Comparative Analysis of DSCOVR EPIC, PANDORA, and TOLNet Data for Space-Based Monitoring Assessment: A Case Study by ASDC

Stratospheric ozone occurs naturally in the upper atmosphere, forming a protective layer that shields us from the sun's harmful ultraviolet rays. Tropospheric ozone is not emitted directly into the air but is created by chemical reactions between nitrogen oxides (NOx) and volatile organic compounds (VOC). This reaction happens when pollutants emitted by cars, power plants, industrial boilers, refineries, chemical plants, and other sources chemically react in sunlight [1]. Therefore, increased levels of tropospheric ozone indicate the presence of pollutants in the air. While daily anthropogenic activity causes an increase of ground-level ozone, variation of stratospheric ozone changes happens much slower, so that variation of the total ozone column reflects the variation of the tropospheric column due to natural, e.g., wildfires and anthropogenic air pollution. Both total and tropospheric ozone column products are used in this study. The reflectance spectra measured by the Earth Polychromatic Imaging Camera (EPIC) instrument aboard the Deep Space Climate Observatory (DSCOVR) spacecraft are compared with a set of radiative transfer-derived lookup tables for the EPIC filter transmission functions and a wide range of ozone values to retrieve ozone with a maximum resolution of 18 km at the sub-satellite point [2]. EPIC provides total column ozone in level 2 and level 4 products and tropospheric column ozone in level 4 products. Both EPIC Ozone products [2] are available at the Atmospheric Science Data Center (ASDC) at NASA Langley Research Center [3, 4]. Pandora spectrometer instrument measures columnar amounts of trace gases in the atmosphere. These gases (O3, NO2, CH2O) absorb light from the sun at specific wavelengths in the ultraviolet-visible spectrum [5]. Using the theoretical solar spectrum as a reference, Pandora determines trace gas amounts using differential optical absorption spectroscopy (DOAS). Pandora ozone retrievals are available from the Pandonia Global Network [6]. Pandora data from North American major metropolitan areas, New York, NY, Washington DC, Los Angeles, CA, and Mexico City. Tropospheric Ozone Lidar Network (TOLNet) was established in 2012 to provide high spatiotemporal observations of tropospheric ozone to (1) better understand physical processes driving the ozone budget in various meteorological and environmental conditions and (2) validate the tropospheric ozone measurements of space-borne missions [7]. TOLNet data are available at ASDC [8]. While EPIC provides global coverage of ozone retrievals several times daily, temporal resolution may miss some features in daily ozone variations. Ground-based sensors such as Pandora spectrometers and TOLNet lidars provide better temporal resolution while missing continuous spatial coverage. The forthcoming ozone retrieval from the TEMPO mission [9] will provide better spatial and temporal coverage of air quality (including ozone) over North America. This study investigates whether EPIC ozone products can detect diurnal air quality variations and compare ozone temporal development with retrieval by ground-based instruments.

diurnal ozone emissions, DSCOVR EPIC, PANDORA, spa↗
NASA NTRSDate not supplied

Characterization of Titan Entry Radiative Heating in the Low Density Electric Arc Shock Tube

Prediction of aftbody radiative heating for Dragonfly’s entry at Titan requires accurate models to inform the design of its thermal protection systems. Previously reported investigations of shock layer aftbody radiation in the Electric Arc Shock Tube (EAST) at NASA Ames Research Center focused on the lower altitude/higher density part of the trajectory. This paper presents the first optical emission spectroscopy measurements of an ongoing test series in the new aluminum Low Density Shock Tube (LDST), recently installed at EAST, focusing on the radiative heating characterization through the higher altitude portion of Dragonfly’s entry path. Experimental data collected at a fill pressure of 0.1 Torr and shock velocities between 5.2 and 6.2 km/s show favorable agreement to similar conditions previously tested in the 4" High-Velocity Shock Tube, as well as improvements in the signal to noise ratio and available test time. Simulations employing DPLR and NEQAIR underpredict the experimental radiance, with increasing discrepancy from the NIR towards the UV wavelength range, thus motivating further efforts in improving the current non-Boltzmann model for the CN molecule.

A Fagnani↗
NASA NTRS1992

Multilayer and grazing incidence X-ray/EUV optics; Proceedings of the Meeting, San Diego, CA, July 22-24, 1991

The present conference discusses the Advanced X-ray Astrophysics Facility (AXAF) calibration by means of synchrotron radiation and its X-ray reflectivity, X-ray scattering measurements from thin-foil X-ray mirrors, lobster-eye X-ray optics using microchannel plates, space-based interferometry at EUV and soft X-ray wavelengths, a water-window imaging X-ray telescope, a graded d-spacing multilayer telescope for high energy X-ray astronomy, photographic films for the multispectral solar telescope array, a soft X-ray ion chamber, and the development of hard X-ray optics. Also discussed are X-ray spectroscopy with multilayered optics, a slit aperture for monitoring X-ray experiments, an objective double-crystal spectrometer, a Ly-alpha coronagraph/polarimeter, tungsten/boron nitride multilayers for XUV optical applications, the evaluation of reflectors for soft X-ray optics, the manufacture of elastically bent crystals and multilayer mirrors, and selective photodevices for the VUV.

Hoover, Richard B.↗
NASA NTRS1998

Characterization of Semi-Insulating CdTe Crystals Grown by Horizontal Seeded Physical Vapor Transport

CdTe crystals were grown by horizontal seeded physical vapor transport technique in uncoated and boron nitride coated fused silica ampoules with the source materials near the congruent sublimation condition. The grown crystals were characterized by current-voltage measurements, low temperature photoluminescence spectroscopy, near IR transmission optical microscopy, spark source mass spectroscopy and chemical etching. The measured resistivities of the crystals were in the high-10(exp 8) ohm-cm range. Although the crystal grown in the boron nitride coating was contaminated with boron from the photoluminescence measurements, the coating yielded a single crystal with no inclusions or precipitates.

Chattopadhyay, K.↗
NASA NTRS2011

Galex and Optical Observations of GW Librae during the Long Decline from Superoutburst

The prototype of accreting, pulsating white dwarfs (GW Lib) underwent a large amplitude dwarf nova outburst in 2007. We used ultraviolet data from Galaxy Evolution Explorer and ground-based optical photometry and spectroscopy to follow GW Lib for three years following this outburst. Several variations are apparent during this interval. The optical shows a superhump modulation in the months following outburst, while a 19 minute quasi-periodic modulation lasting for several months is apparent in the year after outburst. A long timescale (about 4 hr) modulation first appears in the UV a year after outburst and increases in amplitude in the following years. This variation also appears in the optical two years after outburst but is not in phase with the UV. The pre-outburst pulsations are not yet visible after three years, likely indicating the white dwarf has not returned to its quiescent state.

NOVAE↗
NASA NTRS2004

Optical Metrology for the Segmented Optics on the Constellation-X Spectroscopy X-Ray Telescope

We present the metrology requirements and metrology implementation necessary to prove out the reflector technology for the Constellation X(C-X) spectroscopy X-ray telescope (SXT). This segmented, 1.6m diameter highly nested Wolter-1 telescope presents many metrology and alignment challenges. In particular, these mirrors have a stringent imaging error budget as compared to their intrinsic stiffness; This is required for Constellation-X to have sufficient effective area with the weight requirement. This has implications for the metrology that can be used. A variety of contract and noncontact optical profiling and interferometric methods are combined to test the formed glass substrates before replication and the replicated reflector segments.The reflectors are tested both stand-alone and in-situ in an alignment tower.Some of these methods have not been used on prior X-ray telescopes and some are feasible only because of the segmented approach used on the SXT. Methods discussed include high precision coordinate measurement machines using very low force or optical probe axial interferometric profiling azimuthal circularity profiling and use of advanced null optics such as conical computer generated hologram (CGHs).

Content, David↗
NASA NTRS1988

The use of four-photon Raman spectroscopy for the remote sensing of natural objects

The results of the laboratory simulation of optical Kerr effect/Raman spectroscopy for the purpose of remote sensing are presented. The experimental setup is described, and measurements of the vibrational spectra of various liquids obtained. Attention is paid to the possibility of using the proposed method to detect trace hydrocarbons in water, and the spectrum of petroleum is obtained. Full-scale measurements using a laser spectrometer were made on the Black Sea.

Bunkin, A. F.↗
NASA NTRS1992

Non-mechanical optical path switching and its application to dual beam spectroscopy including gas filter correlation radiometry

A non-mechanical optical switch is developed for alternately switching a monochromatic or quasi-monochromatic light beam along two optical paths. A polarizer polarizes light into a single, e.g., vertical component which is then rapidly modulated into vertical and horizontal components by a polarization modulator. A polarization beam splitter then reflects one of these components along one path and transmits the other along the second path. In the specific application of gas filter correlation radiometry, one path is directed through a vacuum cell and one path is directed through a gas correlation cell containing a desired gas. Reflecting mirrors cause these two paths to intersect at a second polarization beam splitter which reflects one component and transmits the other to recombine them into a polarization modulated beam which can be detected by an appropriate single sensor.

Sachse, Glen W.↗
NASA NTRS1972

Development of techniques for advanced optical contamination measurement with internal reflection spectroscopy, phase 2, volume 2

Attenuated total reflectance spectra of individual contaminants in space simulation chambers are presented as well as spectra of mixtures and figures exhibiting the effects of film thickness on reflectance spectra. Detailed calibration spectra were made for three selected concentrations (film thickness) for two contaminants and for one concentration for all contaminants.

Hayes, J. D.↗
NASA NTRS1972

Development of techniques for advanced optical contamination measurement with internal reflection spectroscopy, phase 1, volume 1

The feasibility of monitoring volatile contaminants in a large space simulation chamber using techniques of internal reflection spectroscopy was demonstrated analytically and experimentally. The infrared spectral region was selected as the operational spectral range in order to provide unique identification of the contaminants along with sufficient sensitivity to detect trace contaminant concentrations. It was determined theoretically that a monolayer of the contaminants could be detected and identified using optimized experimental procedures. This ability was verified experimentally. Procedures were developed to correct the attenuated total reflectance spectra for thick sample distortion. However, by using two different element designs the need for such correction can be avoided.

Hayes, J. D.↗
NASA NTRS2006

White-Light Whispering-Gallery-Mode Optical Resonators

Whispering-gallery-mode (WGM) optical resonators can be designed to exhibit continuous spectra over wide wavelength bands (in effect, white-light spectra), with ultrahigh values of the resonance quality factor (Q) that are nearly independent of frequency. White-light WGM resonators have potential as superior alternatives to (1) larger, conventional optical resonators in ring-down spectroscopy, and (2) optical-resonator/electro-optical-modulator structures used in coupling of microwave and optical signals in atomic clocks. In these and other potential applications, the use of white-light WGM resonators makes it possible to relax the requirement of high-frequency stability of lasers, thereby enabling the use of cheaper lasers. In designing a white-light WGM resonator, one exploits the fact that the density of the mode spectrum increases predictably with the thickness of the resonator disk. By making the resonator disk sufficiently thick, one can make the frequency differences between adjacent modes significantly less than the spectral width of a single mode, so that the spectral peaks of adjacent modes overlap, making the resonator spectrum essentially continuous. Moreover, inasmuch as the Q values of the various modes are determined primarily by surface Rayleigh scattering that does not depend on mode numbers, all the modes have nearly equal Q. By use of a proper coupling technique, one can ensure excitation of a majority of the modes. For an experimental demonstration of a white-light WGM resonator, a resonator disk 0.5-mm thick and 5 mm in diameter was made from CaF2. The shape of the resonator and the fiberoptic coupling arrangement were as shown in Figure 1. The resonator was excited with laser light having a wavelength of 1,320 nm and a spectral width of 4 kHz. The coupling efficiency exceeded 80 percent at any frequency to which the laser could be set in its tuning range, which was >100-GHz wide. The resonator response was characterized by means of ring-down tests in which the excitation was interrupted by a shutter having a rise and a fall time of 5 ns. The ring-down time of photodiodes and associated circuitry used to measure the interrupted excitation and the resonator output was <1 ns. Figure 2 shows the shapes of representative input and output light pulses. The average ring-down time was found to be 120 ns, corresponding to Q=2x10(exp 8). The variations of Q with the laser carrier frequency were found to be <5 percent. Hence, the resonator was shown to have the desired white light properties.

Matsko, Andrey↗