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Battery Grade Graphite Production from Biomass, US DOE SBIR Phase I Final Report, DOE_DE-SC0024994_I_Final_OSTI
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Enhanced Biochar for Soil Reclamation Co-Produced by a Drop-In Biofuels Process, US DOE SBIR Phase II Final Report, DOE_DE-SC0022445_II_Final_OSTI
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Coal to Carbon Fiber (C2CF) Continuous Processing for High Value Composites (Final Report)
Coal tar is a condensed and recovered by-product of the coking of metallurgical coal for steel production. The heaviest fraction of distilled coal tar is an isotropic pitch largely used as a binder in the manufacturing of carbonaceous electrodes for primary aluminum smelting and in electric arc furnaces. Coal tar pitch offers high carbon yield upon carbonization. In this project, a process to convert the domestically sourced isotropic coal tar pitch, containing very low particulates (QI = 0.32 wt.%), to form flow-domain mesophase pitch amenable for melt spinning into precursor (green) fibers for carbon fiber, was developed and optimized. The final reproducible processing developed is reviewed in this report, along with several characterizations of the mesophase pitch. A final definition of the characteristics of a ‘spinnable’ mesophase pitch is presented. With this mesophase pitch, reproducible and stable multifilament melt spinning was developed, producing green fiber tows with filament diameters of approximately 20 m. The multifilament melt spinning was the most challenging aspect of the project and required the most effort. The best practices learned from this project for melt spinning are reviewed in this report. Once spun, the green fibers were oxidatively stabilized, carbonized and graphitized under inert gas atmosphere to form the final carbon fibers. Given the relatively high softening point of the mesophase pitch, no issues of interfilament fusion were observed during batch oxidation, and subsequent batch carbonization and graphitization went smoothly in all cases. An ~ 80 wt.% conversion of the green fiber mass to final carbon fiber was achieved. After graphitization, the carbon fibers showed high tensile moduli (most were ~ 600 GPa, or 87 Msi) consistent with commercially-available high-performance pitch-based carbon fiber. However, tensile strength and strain to failure were comparatively low. Further work to reduce defects in and on the fiber surfaces would increase these properties. SEM imaging of the graphitic fiber textures is presented herein. Rudimentary composites were fabricated from the carbon fibers and characterized showing similar modulus to baseline composites fabricated with commercial carbon fiber. Finally, a basic economic analysis was done showing the potential to increase the value of the isotropic coal tar pitch by up to 13.6 to 136 times based on a carbon fiber value of $\$$5/lb to $\$$50/lb, respectively. Moreover, the site case study suggests that the coal tar from the single integrated steel mill could supply production of up to 16 kt/yr of carbon fiber. Finally, a technological gap analysis was done which shed light on remaining technical challenges. These challenges included: recovery and utilization of condensates from the mesophase pitch processing, further advancing and increasing stability of the multifilament melt spinning processing, optimization of the oxidation processing, defect reduction for increased carbon fiber strength, and the development of a weaving process towards carbon fiber fabrics. To maximize the coal value chain, the primary objectives of this project were to (a) develop and scale efficient processing technology for producing melt-spinnable mesophase pitch from isotropic coal tar pitch, (b) clarify and simplify tedious continuous fiber processing technologies (particularly multifilament melt spinning of mesophase pitch) towards the efficient production of high performance carbon fiber, and (c) demonstrate and characterize representative composite parts derived from the final carbon fiber. Immense progress was made on all 3 objectives and is detailed in this report.
X-43A Final Flight Observations
The presentation will provide an overview of the final flight of the NASA X-43A project. The project consisted of three flights, two planned for Mach 7 and one for Mach 10. The first flight, conducted on June 2, 2001, was unsuccessful and resulted in a nine-month mishap investigation. A two-year return to flight effort ensued and concluded when the second Mach 7 flight was successfully conducted on March 27, 2004. The third and final flight, which occurred on November 16, 2004, was the first Mach 10 flight demonstration of an airframe-integrated, scramjet-powered, hypersonic vehicle. As such, the final flight presented first time technical challenges in addition to final flight project closeout concerns. The goals and objectives for the third flight as well as those for the project will be presented. The configuration of the Hyper-X stack including the X-43A, Hyper-X launch vehicle, and Hyper-X research vehicle adapter wil also be presented. Mission differences, vehicle modifications and lessons learned from the first and second flights as they applied to the third flight will also be discussed. Although X-43A flight 3 was always planned to be the final flight of the X-43A project, the X-43 program had two other vehicles and corresponding flight phases in X-43C and X-43B. Those other projects never manifested under the X-43 banner and X-43A flight 3 also became the final flight of X-43 program.
Orbit Determination Adaptations for the Cassini Grand Finale
satellite encounters. Over this period, there have been several papers describing the orbit determination process and performance up through 2016 [1-5]. In April of 2017, Cassini will enter its Grand Finale mission phase when it will traverse the gap between the D-ring and the Saturn atmosphere twenty-two times before plunging deep into the atmosphere to end the mission. The lack of targeted satellite encounters during this period necessitates updates to the nominal Cassini Orbit Determination (OD) process. This paper describes these planned adaptations for the operation of the Grand Finale. During the Equinox and Solstice Mission Phase (2008-2016), navigation analysis has been divided into segments focused on two particular targeted satellite encounters, called an “arc”. Maneuvers in an arc were usually targeted to encounter B-plane position and time, so the OD state and covariance were mapped forward to the B-plane of the encounter within the arc. Trajectory dispersions during the Grand Finale need instead to be mapped to equator crossings and targeted Cartesian positions. In addition, trajectory arcs have typically covered a few orbital revolutions (~2-8 weeks), in order to span the time between two encounters. However, the Grand Finale will encompass five months of time without an encounter which necessitates an adjusted arc strategy. A modified arc strategy was developed based on OD behavior during long multi-rev periods between encounters in the year leading up to the Grand Finale. The OD covariance study conducted for the Grand Finale mission phase will also be examined.
Final state radiation from high and ultrahigh energy neutrino interactions
Charged leptons produced by high-energy and ultrahigh-energy neutrinos have a substantial probability of emitting prompt internal bremsstrahlung ν ℓ + N → ℓ + X + γ . This can have important consequences for neutrino detection. We discuss observable consequences at high- and ultrahigh-energy neutrino telescopes and the Large Hadron Collider’s (LHC’s) Forward Physics Facility. Logarithmic enhancements can be substantial (e.g., ∼ 20 % ) when either the charged lepton’s energy or the rest of the cascade is measured. We comment on final state radiation’s impacts on measuring the inelasticity distribution, ν / ν ¯ flux ratio, throughgoing muons, and double-bang signatures for high-energy neutrino observation. Furthermore, for ultrahigh-energy neutrino observation, we find that final state radiation increases the overall detectable energy by as much as 20%, affects flavor measurements, and decreases the energy of both Earth-emergent tau leptons and regenerated tau neutrinos. Many of these have significant impacts on measuring neutrino fluxes and spectra. Finally, for the LHC’s Forward Physics Facility, we find that final state radiation will impact future extractions of strange quark parton distribution functions. Final state radiation should be included in future analyses at neutrino telescopes and the Forward Physics Facility. Published by the American Physical Society 2025
Feldspathic granulitic impactites and pre-final bombardment lunar evolution
It is suggested that feldspathic granulitic impactites, which are characterized by a high model plagioclase content of between 70 and 80%, all formed in the period after consolidation of the lunar crust and before the final bombardment. The granulitic impactites contain essentially no KREEP component, which suggests that KREEP appeared on the lunar surface mostly after the formation of the granulitic impactites, at about the start of the final bombardment. The granulite metamorphism indicated by the matrix textures of these samples requires 1000 C temperatures for prolonged periods of time. The apparent sequence of formation is granulitic impactites before the final bombardment, crystalline-matrix breccias during the final bombardment, and vitric-matrix breccias after the final bombardment. The sequence is consistent with a described thermal model of breccia lithification and with characteristics of the decay of the meteorite flux rate.
The final warming and polar vortex disappearance during the Southern Hemisphere spring
Seven years (1979-1985) of NMC data are used to analyze Southern Hemisphere middle stratosphere winter-to-summer circulation transitions. These transitions are classified into two extreme categories: (1) a mid-October final warming accompanied by a major mid-October wave event (1979 and 1982), and (2) a mid-November final warming with no strong October wave event (1980 and 1981). After the final warming a wave event in late November-early December results in the disappearance of the polar vortex. All of these wave events in conjunction with zonal mean mass motions act to reduce zonal mean gradients of potential vorticity and ozone through horizontal mixing, and hence they act to destroy the vortex and fill the ozone hole. Additionally, it is noted that the final warming and the vortex breakdown are two distinct events separated by 15-40 days. Finally, past studies show that the time of these events has not radically changed.
Diving Deeper: Exploring the Feasibility of Lowering Cassini’s Final Orbits
During the final five orbits of Cassini’s mission, the spacecraft will get closer to Saturn than it has ever been. These five orbits were designed to be as deep in the atmosphere as Cassini could safely fly; however, recent occultation data of Saturn’s atmosphere suggest that it is contracting. Given this contraction, the primary concern during these orbits has shifted from spacecraft health and safety to loss of science value. This paper explores a scenario for modifying the Cassini spacecraft’s trajectory, during these final orbits, such that it dips deeper into Saturn’s atmosphere. This scenario describes the method for in-situ detection of Saturn’s atmospheric state, the locations and sizes of maneuvers that would reduce the final periapsis altitudes, the effects of such maneuvers on the remaining trajectory, and the risks involved. The result is that a periapsis-lowering, “pop-down” maneuver is feasible during Cassini’s final orbits. Risk to the spacecraft is minimized by using the attitude control thrusters as density detectors during the first three atmospheric transits of the final five orbits. Should these transits reveal sufficiently low density and should sufficient propellant remain, then the Cassini project will consider performing the maneuver.
Emulation of the calculations of final r -process abundance patterns with a neural network
This work explores the construction of a fast emulator for the calculation of the final pattern of nucleosynthesis in the rapid neutron capture process (the r-process). An emulator is built using a feed-forward artificial neural network (ANN). We train the ANN with nuclear data and relative abundance patterns. We take as input the β-decay half-lives and the one-neutron separation energy of the nuclei in the rare-earth region. The output is the final isotopic abundance pattern. In this work, we focus on the nuclear data and abundance patterns in the rare-earth region to reduce the dimension of the input and output space. We show that the ANN can capture the effect of the changes in the nuclear physics inputs on the final r-process abundance pattern in the adopted astrophysical conditions. We employ the deep ensemble method to quantify the prediction uncertainty of the neural network emulator. The emulator achieves a speed-up by a factor of about 20 000 in obtaining a final abundance pattern in the rare-earth region. The emulator may be utilized in statistical analyses such as uncertainty quantification, inverse problems, and sensitivity analysis.
Measurement of post-disruption runaway electron kinetic energy and pitch angle during final loss instability in DIII-D
Post-disruption runaway electron (RE) kinetic energy K and pitch angle sin$\vartheta$ are critical parameters for determining resulting first wall material damage during wall strikes, but are very challenging to measure experimentally. During the final loss instability, confined RE K and sin$\vartheta$ are reconstructed during center-post wall strikes for both high impurity (high-Z) and low impurity (low-Z) plasmas by combining soft x-ray, hard x-ray, synchrotron emission, and total radiated power measurements. Deconfined (wall impacting) RE sin$\vartheta$ is then reconstructed for these shots by using time-decay analysis of infra-red imaging. Additionally, deconfined RE K and sin$\vartheta$ are reconstructed for a low-Z downward loss shot by analyzing resulting damage to a sacrificial graphite dome limiter. The damage analysis uses multi-step modeling simulating plasma instability, RE loss orbits, energy deposition, and finally material expansion (MARS-F, KORC, GEANT-4, and finally COMSOL). Overall, mean kinetic energies are found to be in the range $\langle$$K$$\rangle$ $≈ 3-4$ MeV for confined REs. KORC simulations indicate that the final loss instability process does not change individual RE kinetic energy K. In conclusion, confined RE pitch angles are found to be fairly low initially pre-instability, $\langle$sin$\vartheta$$\rangle$ $≈ 0.1 – 0.2$, but appear to increase roughly 2x, to $\langle$sin$\vartheta$$\rangle$ $≈ 0.3 – 0.4$ for both confined and deconfined REs during instability onset in the low-Z case; this increase is not observed in the high-Z case.
Initial energy-momentum to final flow: A general framework for heavy-ion collisions
The evolution of a relativistic heavy-ion collision is typically understood as a process that transmutes the initial geometry of the system into the final momentum distribution of observed hadrons, which can be described via a cumulant expansion of the initial distribution of energy density and is represented at leading order as the well-known eccentricity scaling of anisotropic flow. We extend this framework to include the contribution from initial momentum-space properties, as encoded in other components of the energy-momentum tensor. Furthermore, we confirm the validity of the framework in state-of-the-art hydrodynamic simulations of large and small systems. With this framework, it is possible to separate the effects of early time dynamics from those of final-state evolution, even in the case when the distribution of energy does not fully determine subsequent evolution, as for example, in small systems. Specifically, we answer the question of when and how azimuthal correlations from the initial state survive to the final state. In very small systems such as 𝑝−𝑝, for example, initial momentum degrees of freedom dominate over energy. Thus, even if the system forms a quark-gluon plasma that is well described by hydrodynamics, the usual hydrodynamic picture of the transmutation of initial geometry to final momentum anisotropy is broken. Nevertheless, we show that the hydrodynamic response to the full energy-momentum tensor can be well understood in a similar manner as larger systems. Additionally, this framework elucidates the generic features of the system's evolution that are responsible for the impressive success of hydrodynamic simulations, but which may still hold even in cases where hydrodynamics is not applicable.
Integrated Application of Active Controls (IAAC) technology to an advanced subsonic transport project: Final ACT configuration evaluation
The Final ACT Configuration Evaluation Task of the Integrated Application of Active Controls (IAAC) technology project within the energy efficient transport program is summarized. The Final ACT Configuration, through application of Active Controls Technology (ACT) in combination with increased wing span, exhibits significant performance improvements over the conventional baseline configuration. At the design range for these configurations, 3590 km, the block fuel used is 10% less for the Final ACT Configuration, with significant reductions in fuel usage at all operational ranges. Results of this improved fuel usage and additional system and airframe costs and the complexity required to achieve it were analyzed to determine its economic effects. For a 926 km mission, the incremental return on investment is nearly 25% at 1980 fuel prices. For longer range missions or increased fuel prices, the return is greater. The technical risks encountered in the Final ACT Configuration design and the research and development effort required to reduce these risks to levels acceptable for commercial airplane design are identified.
Mixing processes following the final stratospheric warming
An investigation is made of the dynamics responsible for the mixing and dissolution of the polar vortex during the final stratospheric warmings. The dynamics and transport during a Northern Hemisphere final stratospheric warming are simulated via a GCM and an associated offline N2O transport model. The results are compared with those obtained from LIMS data for the final warming of 1979, with emphasis on the potential vorticity evolution in the two datasets, the modeled N2O evolution, and the observed O3 evolution. Following each warming, the remnants of the originally intact vortex are found to gradually homogenize with the atmosphere at large. Two processes leading to this homogenization are identified following the final warmings, namely, the potential vorticity field becomes decorrelated from that of the chemical tracer, and the vortex remnants begin to tilt dramatically in a vertical direction.
Final STS-35 Columbia descent BET products and results for LaRC OEX investigations
Final STS-35 'Columbia' descent Best Estimate Trajectory (BET) products have been developed for Langley Research Center (LaRC) Orbiter Experiments (OEX) investigations. Included are the reconstructed inertial trajectory profile; the Extended BET, which combines the inertial data and, in this instance, the National Weather Service atmospheric information obtained via Johnson Space Center; and the Aerodynamic BET. The inertial BET utilized Inertial Measurement Unit 1 (IMU1) dynamic measurements for deterministic propagation during the ENTREE estimation process. The final estimate was based on the considerable ground based C-band tracking coverage available as well as Tracking Data and Relay Satellite System (TDRSS) Doppler data, a unique use of the latter for endo-atmospheric flight determinations. The actual estimate required simultaneous solutions for the spacecraft position and velocity, spacecraft attitude, and six IMU parameters - three gyro biases and three accelerometer scale factor correction terms. The anchor epoch for this analysis was 19,200 Greenwich Mean Time (GMT) seconds which corresponds to an initial Shuttle altitude of approximately 513 kft. The atmospheric data incorporated were evaluated based on Shuttle derived considerations as well as comparisons with other models. The AEROBET was developed based on the Extended BET, the measured spacecraft configuration information, final mass properties, and the final Orbiter preoperation databook. The latter was updated based on aerodynamic consensus incrementals derived by the latest published FAD. The rectified predictions were compared versus the flight computed values and the resultant differences were correlated versus ensemble results for twenty-two previous STS entry flights.
Cassini's Grand Finale: A Mission Planning Retrospective
On September 15, 2017, Cassini plunged deep into Saturn, down to where the atmosphere was sufficiently dense to destroy the spacecraft, making it part of Saturn forever. In the five months leading up to its destruction, Cassini flew between Saturn and its rings 22 times, collecting data from the never before-explored region of the Kronian system. These orbits, the Grand Finale of Cassini, were the culmination of years of planning by the Cassini flight team. This paper looks back upon the mission planning effort in particular, comparing the baseline operational scenarios and contingency plans to the as flown Grand Finale. The bulk of the Grand Finale mission planning effort was focused on the environmental hazards present in the region between Saturn and its rings: the dust and the atmosphere. Dust hazard and atmospheric transit contingency plans were in place to help ensure spacecraft health and maximize science data return. The dust hazard plan gave the operations team the option to turn the spacecraft to a safe attitude during ring-plane crossings had the dust environment proved more threatening than anticipated. The atmospheric transit plan would have made use of an orbital trim maneuver in order to raise or lower periapsis depending on the density of the atmosphere. The proximal environment did have its surprises, though they were good surprises. The dust was significantly less hazardous than predicted. So much so that elements of the contingency plan were leveraged in order to remove a dust hazard protection from the baseline plan, rather than add one to it. While the atmosphere was substantially denser than predicted, it was not dense enough to warrant a periapsis-raise maneuver and actually meant that better in-situ data was gathered. Ultimately, from a mission planning perspective, the Grand Finale went better than expected.
Skimming through Saturn's Atmosphere: The Climax of the Cassini Grand Finale Mission
On September 15, 2017, the long-lived Cassini Mission to Saturn came to a triumphant end as the Cassini orbiter plunged deep into Saturn’s atmosphere, all the while transmitting engineering and science data back to Earth before Saturn’s atmosphere destroyed the orbiter. Even before the final plunge, the Cassini spacecraft became the first spacecraft to successfully skim Saturn’s atmosphere and collect atmospheric data during its final five complete orbits around Saturn (Rev-288 through Rev-292). During those five final orbits, the spacecraft was flying in Reaction Control Subsystem (RCS) control in order to maintain greater control authority. Therefore, by analyzing the thruster on-time flight data telemetered back to Earth after each orbit, atmospheric density estimates can be extracted. This paper proposes a method of using Cassini Attitude Control Flight Data to reconstruct Saturn atmospheric density profiles for each of the five final orbits around Saturn.