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At least 37 records · Page 2

Upgrade of the gated laser entrance hole imager G-LEH-2 on the National Ignition Facility

A major upgrade has been implemented for the ns-gated laser entrance hole imager on the National Ignition Facility (NIF) to obtain high-quality data for Hohlraum physics study. In this upgrade, the single “Furi” hCMOS sensor (1024 × 448 pixel arrays with two-frame capability) is replaced with dual “Icarus” sensors (1024 × 512 pixel arrays with four-frame capability). Both types of sensors were developed by Sandia National Laboratories for high energy density physics experiments. With the new Icarus sensors, the new diagnostic provides twice the detection area with improved uniformity, wider temporal coverage, flexible timing setup, and greater sensitivity to soft x rays (<2 keV). These features, together with the fact that the diagnostic is radiation hardened and can be operated on the NIF for high neutron yield deuterium–triterium experiments, enable significantly greater return of data per experiment.

47 OTHER INSTRUMENTATION↗

Test results and prospects for RD53A, a large scale 65 nm CMOS chip for pixel readout at the HL-LHC

The CERN RD53 collaboration was founded to tackle the extraordinary challenges associated with the design of pixel readout chips for the innermost layers of particle trackers at future high energy physics experiments. Around 20 institutions are involved in the collaboration, which has the support of both ATLAS and CMS experiments. The goals of the collaboration include the comprehensive understanding of radiation effects in the 65 nm technology, the development of tools and methodology to efficiently design large complex mixed signal chips and, ultimately, the development of a full size readout chip featuring a 400 × 400 pixel array with 50μm pitch. In August 2017, the collaboration submitted the large scale chip RD53A, integrating a matrix of 400 × 192 pixels and embodying three different analog front-end designs. Here, this work discusses the characteristic of the RD53A chip, with some emphasis on the analog processors, and presents the first test results on the pixel array.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

A Low Power, High Speed Readout for Pixel Detectors Based on an Arbitration Tree

A low-power, high-speed arbitration tree for pixel detector readout is presented. The synchronized, binary tree priority encoder establishes a position dependent priority list at the start of every time frame. Pixels that indicate the presence of data for readout, are sequentially granted access to a shared bus for data transfer to the periphery, without the use of an additional global strobe signal. It can be used for either full frame imaging or zero-suppressed readout, in which case it can simultaneously generate the pixel address. To increase the readout frame rate, the pixel array is subdivided into two halves, which allows interleaved latching of data at the output serializer. The design was implemented in a 65 nm LP-CMOS process for the readout of a 64 x 64 pixel array. Measurement results demonstrate a deadtime-less, full frame imaging rate of ~50 kfps, achieved with a dedicated output for every (32 x 32) 1024 pixels and for a pixel data packet of 11 bits, with no bit errors detected over 1000 frames. The measured energy per bit is 0.94 pJ.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Pixelated plastic scintillator array manufacturing using fast-, photo-curable resin

Pixelated plastic scintillator arrays can serve as high efficiency and high resolution neutron imaging detectors. Manufacturing these arrays is intensive in both time and labor. This article presents a fabrication method based on additive manufacturing for two-dimensional plastic organic scintillator arrays using a custom-built automated assembly machine and a custom photocurable resin that has significant non-aromatic acrylate oligomer content. The process involves two main stages: fully autonomous production of one-dimensional layered arrays, followed by semi-autonomous cutting and stacking to form two-dimensional pixel arrays. One-dimensional arrays were manufactured at a rate of around 4 layers per hour with minimal defects and tight dimensional tolerances, while two-dimensional arrays up to 7 x 7 pixels and 70 mm in length were completed in approximately 3.5 hours. Final arrays exhibited dimensional deviations of less than 0.5 mm. Two-dimensional arrays read out by a multi-anode photomultiplier tube demonstrated per-pixel position resolution and pulse-shape discrimination, enabling gamma–neutron interaction separation in mixed radiation environments.

36 MATERIALS SCIENCE↗

Wide Dynamic Range, 10 kHz Framing Detector for 4D-STEM

Hybrid pixel array detectors (PADs) have expanded the fidelity, frame rate and dynamic range for diffractive imaging in electron microscopes. With their high detective quantum efficiencies (DQE), the noise performance limited is by counting statistics. Consequently, improving the precision and quality of high-speed images requires increasing the linear dynamic range and the maximum usable beam current. Here we describe a new prototype hybrid PAD, our next-generation electron microscope pixel array detector (NG-EMPAD) that expands both the framing speed and dynamic range of our earlier EMPAD design. Like the EMPAD, electrons are detected directly in a 500 μm thick silicon sensor bonded pixel-by-pixel to a custom signal processing integrated circuit (IC). Each pixel in the IC integrates charge carriers produced by the high-energy incident electrons. Here, in-pixel circuitry uses a combination of techniques to extend the dynamic range, including adaptive gain switching and the quantitative excess charge dumping similar to the EMPAD. In-pixel buffering of signals during readout allows acquiring a new image while reading out the previously collected image, yielding an image collection duty cycle of nearly 100%.

36 MATERIALS SCIENCE↗

Plasmonic photoconductive terahertz focal-plane array with pixel super-resolution

Abstract Imaging systems operating in the terahertz part of the electromagnetic spectrum are attractive due to their ability to penetrate many opaque materials and provide unique spectral signatures of various chemicals. However, the use of terahertz imagers in real-world applications has been limited by the slow speed, large size, high cost and complexity of present systems, largely due to the lack of suitable terahertz focal-plane array detectors. Here we report a terahertz focal-plane array that can directly provide the spatial amplitude and phase distributions, along with the ultrafast temporal and spectral information of an imaged object. It consists of a two-dimensional array of ~0.3 million plasmonic photoconductive nanoantennas optimized to rapidly detect broadband terahertz radiation with a high signal-to-noise ratio. We utilized the multispectral nature of the amplitude and phase data captured by these plasmonic nanoantennas to image different objects, including super-resolved etched patterns in a silicon substrate and defects in battery electrodes. By eliminating the need for raster scanning and spatial terahertz modulation, our terahertz focal-plane array offers more than a 1,000-fold increase in the imaging speed compared with the state of the art and potentially suits a broad range of applications in industrial inspection, security screening and medical diagnosis, among others.

Optics↗

Pixelated scintillator array response to relativistic electrons

In order to make time resolved measurements of the gamma spectra on DARHT Axis 2 using the Compton Spectrometer (CS), the electron detector in the focal plane must be a scintillator that is optically coupled to a gated or streak camera. There are several issues we would like to address with experiments at Idaho Accelerator Center (IAC) before committing to a full size array (7”x2”), which would cost at least $100k. Two candidates for this application are organic (Bicron 422 or equivalent) or inorganic (LYSO) scintillator. Monte Carlo calculations were performed by Rachel Morneau, P-21, using MCNP to compare the two materials each 1.5mm thick for an energy range of 0.1 to 20MeV. The energy loss per particle in LYSO is much larger (100x) than in the plastic scintillator. We confirmed, by performing experiments with the CS on the Microton, that sensitivity of the LYSO was much larger (10x) than the plastic scintillator. Therefore, we have selected LYSO as the scintillator of choice. However, interest in the response of other organic and plastic scintillators prompted an increase in scope of the project. The goals of this experiment were as follows. First, we need to understand the optical response of the scintillators to electrons as a function of thickness, energy, and deposited charge. We also need to verify level of saturation in the scintillation process. Second, compare the scintillators’ response to an image plate (the current CS detector). Third, we need to quantify the effect of signal bleed through to adjacent pixels.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

A Paris-Edinburgh Cell for High-Pressure and High-Temperature Structure Studies on Silicate Liquids Using Monochromatic Synchrotron Radiation

A Paris-Edinburgh press combined with a multi-channel collimator assembly has been commissioned at the GeoSoilEnviro Center for Advanced Radiation Sources (GSECARS) beamline for monochromatic X-ray scattering, with an emphasis on studying low-Z liquids, especially silicate liquids at high pressure. The Paris-Edinburgh press is mounted on a general-purpose diffractometer, with a pixel array detector mounted on the detector arm. The incident monochromatic undulator beam with energies up to 60 keV is focused both horizontally and vertically to a beam size about 30 &times; 30 &micro;m. With this setup, background scattering from the surrounding pressure media is completely removed at 2&theta; angles above 10&deg; for samples larger than 1.05 mm in diameter. Thirty minutes is typically sufficient to collect robust X-ray scattering signals from a 1.6 mm diameter amorphous silicate sample. Cell assemblies for the standard Paris-Edinburgh anvils have been developed and pressures and temperatures up to 7 GPa and 2300 K, respectively, have been maintained steadily over hours. We have also developed a cupped-toroidal Drickamer anvil to further increase pressure and temperature capabilities. The cupped-toroidal Drickamer anvil combines features of a modified Drickamer anvil and the traditional Paris-Edinburgh anvil. Pressures up to 12 GPa have been generated at temperatures up to 2100 K.

58 GEOSCIENCES↗

Development of the microcalorimeter and anticoincidence detector for the Line Emission Mapper x-ray probe

The Line Emission Mapper (LEM) is an x-ray probe mission concept that is designed to provide unprecedented insight into the physics of galaxy formation, including stellar and black-hole feedback and flows of baryonic matter into and out of galaxies. LEM incorporates a light-weight x-ray optic with a large-format microcalorimeter array. The LEM detector utilizes a 14k pixel array of transition-edge sensors (TESs) that will provide <2.5 eV spectral resolution over the energy range 0.2 to 2 keV, along with a field-of-view of 30 arcmin. The microcalorimeter array and readout builds upon the technology developed for the European Space Agency’s (ESA’s) Athena/x-ray Integral Field Unit. Here, we present a detailed overview of the base- line microcalorimeter design, its performance characteristics, including a detailed energy resolution budget and the expected count-rate capability. In addition, we outline the current status and plan for continued technology maturation. Behind the LEM array sits a high-efficiency TES-based anticoincidence (antico) detector that will reject cosmic-ray background events. We will briefly describe the design of the antico and plan for continued development.

47 OTHER INSTRUMENTATION↗

Characterizing electron-collecting CdTe for use in a 77 ns burst-rate imager

The Keck-PAD (pixel array detector) was developed at Cornell as a burst-rate imager capable of recording images from successive electron bunches (153 ns period) from the Advanced Photon Source (APS). Both Si and hole-collecting Schottky CdTe have been successfully bonded to this ASIC (application-specific integrated circuit) and used with this frame rate. The facility upgrades at the APS will lower the bunch period to 77 ns, which will require modifications to the Keck-PAD electronics to image properly at this reduced period. In addition, operation at high X-ray energies will require a different sensor material having a shorter charge collection time. For the target energy of 40 keV for this project, simulations have shown that electron-collecting CdTe should allow >90% charge collection within 35 ns. This collection time will be sufficient to sample the signal from one frame and prepare for the next. 750 µm-thick electron-collecting Schottky CdTe has been obtained from Acrorad and bonded to two different charge-integrating ASICs developed at Cornell, the Keck-PAD and the CU-APS-PAD. Carrier mobility has been investigated using the detector response to single X-ray bunches at the Cornell High Energy Synchrotron Source and to a pulsed optical laser. The tests indicate that the collection time will meet the requirements for 77 ns imaging.

36 MATERIALS SCIENCE↗

Spatial calibration and synthetic diagnostic of a multi-energy hard x-ray camera at WEST tokamak

WEST (tungsten environment in steady-state tokamak) is starting operation for the first time with a water-cooled full tungsten divertor, enabling long pulse operation. Heating is provided by radiofrequency systems, including lower hybrid current drive (LHCD). In this context, a compact multi-energy hard x-ray camera has been installed for energy and space-resolved measurements of the electron temperature, the fast electron tail density produced by LHCD and runaway electrons, and the beam–target emission of tungsten at the target due to fast electron losses interacting with the divertor plates. The diagnostic is a pinhole camera based on a 2D pixel array detector (Pilatus 3 CdTe CMOS Hybrid-Pixel detector produced by DECTRIS). The novelty of this diagnostic technique is the detector’s capability of adjusting the threshold energy at pixel level. This innovation provides great flexibility in the energy configuration, allowing simultaneous space and energy-resolved x-ray measurements. This contribution details two important steps in the preparation of the diagnostic operation. First, the in-vessel spatial calibration that was carried out with a radioactive source. Second, the synthetic diagnostic is obtained by the suite of codes ALOHA/C3PO/LUKE/R5-X2, which simulates LH wave propagation and absorption, as well as the fast electron bremsstrahlung production.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Linear fitting of multi-threshold counting data

The present disclosure provides a system and method for efficiently mining multi-threshold measurements acquired using photon counting pixel-array detectors for spectral imaging and diffraction analyses. Images of X-ray intensity as a function of X-ray energy were recorded on a 6 megapixel X-ray photon counting array detector through linear fitting of the measured counts recorded as a function of counting threshold. An analytical model is disclosed for describing the probability density of detected voltage, utilizing fractional photon counting to account for edge/corner effects from voltage plumes that spread across multiple pixels. Three-parameter fits to the model were independently performed for each pixel in the array for X-ray scattering images acquired for 13.5 keV and 15.0 keV X-ray energies. From the established pixel responses, multi-threshold composite images produced from the sum of 13.5 keV and 15.0 keV data can be analytically separated to recover the monochromatic images through simple linear fitting.

47 OTHER INSTRUMENTATION↗

Characterization of high-flux cadmium zinc telluride detectors coupled to MM-PAD readout ASICs for high-flux X-ray applications

High-flux cadmium zinc telluride (HF-CZT) is a promising material for next-generation X-ray imaging due to its high stopping power, wide bandgap, and improved resistance to radiation-induced polarization [1]. We bonded 2 mm thick HF-CZT sensors with Cornell's Mixed-Mode Pixel Array ASICs, which combine analog charge integration and in-pixel digital counting to achieve single X-ray sensitivity, large full well capacity, and frame rates up to 10 kHz [2,3]. Detector characterization showed stable electron collection above 150 V bias, while hole collection remained limited by trapping even at 700 V. Temporal studies revealed non-negligible afterglow, with an unexpected increase in afterglow at higher biases, which was reduced by infrared illumination, suggesting that injected carriers reduce trapping near contact interfaces. Polarization measurements confirmed improved stability compared to conventional CZT, though polarization effects persisted, particularly with hole collection, with up to 5% signal loss and spatial distortion at high doses.

36 MATERIALS SCIENCE↗

Characterization of 128 × 128 MM-PAD-2.1 ASIC: a fast framing hard x-ray detector with high dynamic range

Here, we characterize a new x-ray Mixed-Mode Pixel Array Detector (MM-PAD-2.1) Application Specific Integrated Circuit (ASIC). Using an integrating pixel front-end with dynamic charge removal architecture, the MM-PAD-2.1 ASIC extends the maximum measurable x-ray signal (in 20 keV photon units) to > 10 7 x-rays/pixel/frame while maintaining a low read noise across the full dynamic range, all while imaging continuously at a frame rate of up to 10 kHz. The in-pixel dynamic charge removal mechanism prevents saturation of the input amplifier and proceeds in parallel with signal integration to achieve deadtime-less measurements with incident x-ray rates of > 10 10 x-rays/pixel/s. The ASIC format consists of 128 × 128 square pixels each 150 μm on a side and is designed to be 3-side buttable so large arrays can be effectively tiled. Here we use both laboratory x-ray sources and the Cornell High Energy Synchrotron Source (CHESS) to characterize two single ASIC prototype detectors for both low (single x-ray) and high incident flux detection. In the first detector the ASIC was solder bump-bonded to a 500 μm thick Si sensor for efficient detection of x-rays below 20 keV, whereas the second detector used a 750 μm thick CdTe sensor for x-rays above ~20 keV.

36 MATERIALS SCIENCE↗

Design and engineering challenges of a multi-energy hard x-ray camera for long-pulse profile measurements at WEST tokamak

The WEST tokamak has recently been prepared for long pulse operation with a water-cooled full first wall. Heating is provided by radiofrequency systems, including Lower Hybrid Current Drive (LHCD). The Princeton Plasma Physics Laboratory has developed a multi-energy hard x-ray camera for profile measurements at WEST. The camera is based on a new generation of 2D pixel array detectors that allow the energy threshold to be independently set for each pixel. The diagnostic will provide spatial, temporal and energy resolved measurements of the hard x-ray emission from the full plasma cross-section, investigating several physical quantities such as the electron temperature from continuum emission, the fast electron tail density produced by radiofrequency current drive and runaway electrons, as well as characteristic tungsten x-rays due to beam-target emission at the edge. Overall, this work describes the engineering challenges that the WEST long pulse scenario poses for this diagnostic and how the design addresses and solves them. Vacuum, thermal stress and heat transfer calculations are presented and discussed.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Super-Resolution Ptychography with Small Segmented Detectors

To overcome the spatial resolution limit set by aperture-limited diffraction in traditional scanning transmission electron microscopy, microscopists have developed ptychography enabled by iterative phase retrieval algorithms and high-dynamic-range pixel array detectors. Current detector designs are limited by the data rate off chip, so a high-pixel-count detector has a proportionally lower frame rate than the few-segment detectors used for differential phase contrast (DPC) imaging. This slower acquisition speed leads to heightened vulnerability to scan noise, drift, and potential sample damage. This creates opportunities for repurposing fast segmented detectors for ptychography by trading a reduction in reciprocal space pixels for an increase in real space pixels. Here, we explore a strategy of oversampling in real space and instead apply detector pixel upsampling during the reconstruction process. Further, we demonstrate the viability of achieving super-resolution ptychography on thin objects using only 2 × 2 detector pixels, surpassing the resolution of integrated DPC (iDPC) imaging. With optimization using simulated datasets and experiments on MoTe 2 /WSe 2 bilayer moiré superlattices, we achieved super-resolution ptychography reconstructions under rapid acquisition conditions (37.5 pA, 1 μs dwell time), yielding over 50% improvements in contrast and information limit compared to annular dark field and iDPC imaging on the same detectors.

2D materials↗

Ultra low background time projection alpha particle detector ( Phase II Final Scientific/Technical Report)

When alpha particles are emitted into a gas they create an ionization track of gas ions and electrons. In our commercial UltraLo instrument we apply a voltage between a planar sample and an anode, integrate the anode signal as it collects the electrons, and distinguish between alphas emitted from the sample and elsewhere (anode, sidewalls) by the duration and shape of the resultant signal. The major contributors limiting the instrument’s lower detection limit are cosmic rays that pass through the detector close to the sample and Rn decays that produce charge tracks the originate in the gas and end on the sample. In this work we proposed to identify and reject these events by converting the anode into a multi-pixel array and operating in time projection mode. Cosmic rays would be eliminated by generating charge on many pixels, while charge collection asymmetry would distinguish between sample events (Bragg curve up) and Rn events (Bragg curve down). We therefore proposed to modify an UltraLo by pixilating its anode, developing low noise, low power multiplexed electronics to track each pixel’s signal individually, and develop analysis software to make the required discriminations.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

High spatial resolution direct conversion amorphous selenium X-ray detectors with monolithically integrated CMOS readout

Recent progress in the field of micron-scale spatial resolution direct conversion X-ray detectors for high-energy synchrotron light sources serve applications ranging from nondestructive and noninvasive microscopy techniques which provide insight into the structure and morphology of crystals, to medical diagnostic measurement devices. Amorphous selenium ( a -Se) as a wide-bandgap thermally evaporated photoconductor exhibits ultra-low thermal generation rates for dark carriers and has been extensively used in X-ray medical imaging. Being an amorphous material, it can further be deposited over large areas at room temperatures and at substantially lower costs as compared to crystalline semiconductors. Here, to address the demands for a high-energy and high spatial resolution X-ray detector for synchrotron light source applications, we have thermally evaporated a -Se on a Mixed-Mode Pixel Array Detector (MM-PAD) Application Specific Integrated Circuit (ASIC). The ASIC format consists of 128 × 128 square pixels each 150 μm on a side. A 200 μm a -Se layer was directly deposited on the ASIC followed by a metal top electrode. The completed detector assembly was tested with 45 kV Ag and 23 kV Cu X-ray tube sources. The detector fabrication, performances, Modulation Transfer Function (MTF) measurements, and simulations are reported.

36 MATERIALS SCIENCE↗